CN107810954A - A kind of white mosquito-repellent incense and preparation method thereof - Google Patents
A kind of white mosquito-repellent incense and preparation method thereof Download PDFInfo
- Publication number
- CN107810954A CN107810954A CN201711007766.2A CN201711007766A CN107810954A CN 107810954 A CN107810954 A CN 107810954A CN 201711007766 A CN201711007766 A CN 201711007766A CN 107810954 A CN107810954 A CN 107810954A
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- Prior art keywords
- mosquito
- repellent incense
- dry body
- white
- disks
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Links
- 239000000077 insect repellent Substances 0.000 title claims abstract description 96
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000843 powder Substances 0.000 claims abstract description 19
- 244000017020 Ipomoea batatas Species 0.000 claims abstract description 17
- 235000002678 Ipomoea batatas Nutrition 0.000 claims abstract description 17
- 238000002485 combustion reaction Methods 0.000 claims abstract description 15
- 239000000945 filler Substances 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 14
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 13
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 13
- 239000002699 waste material Substances 0.000 claims abstract description 13
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 12
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 12
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims abstract description 12
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 claims abstract description 11
- 239000001863 hydroxypropyl cellulose Substances 0.000 claims abstract description 11
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 claims abstract description 11
- 239000000203 mixture Substances 0.000 claims abstract description 11
- 229940088417 precipitated calcium carbonate Drugs 0.000 claims abstract description 11
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims abstract description 9
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims abstract description 9
- 239000002374 bone meal Substances 0.000 claims abstract description 9
- 229940036811 bone meal Drugs 0.000 claims abstract description 9
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims abstract description 9
- 229920003086 cellulose ether Polymers 0.000 claims abstract description 8
- 239000001923 methylcellulose Substances 0.000 claims abstract description 8
- 235000010981 methylcellulose Nutrition 0.000 claims abstract description 8
- 229920000609 methyl cellulose Polymers 0.000 claims abstract description 7
- LNAZSHAWQACDHT-XIYTZBAFSA-N (2r,3r,4s,5r,6s)-4,5-dimethoxy-2-(methoxymethyl)-3-[(2s,3r,4s,5r,6r)-3,4,5-trimethoxy-6-(methoxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6r)-4,5,6-trimethoxy-2-(methoxymethyl)oxan-3-yl]oxyoxane Chemical compound CO[C@@H]1[C@@H](OC)[C@H](OC)[C@@H](COC)O[C@H]1O[C@H]1[C@H](OC)[C@@H](OC)[C@H](O[C@H]2[C@@H]([C@@H](OC)[C@H](OC)O[C@@H]2COC)OC)O[C@@H]1COC LNAZSHAWQACDHT-XIYTZBAFSA-N 0.000 claims abstract description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 17
- 241000607479 Yersinia pestis Species 0.000 claims description 16
- 241000723353 Chrysanthemum Species 0.000 claims description 10
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 10
- 150000002148 esters Chemical class 0.000 claims description 10
- 239000003350 kerosene Substances 0.000 claims description 10
- HXELGNKCCDGMMN-UHFFFAOYSA-N [F].[Cl] Chemical compound [F].[Cl] HXELGNKCCDGMMN-UHFFFAOYSA-N 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- OOWCJRMYMAMSOH-UHFFFAOYSA-N [2,3,5,6-tetrafluoro-4-(methoxymethyl)phenyl]methyl 2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical group FC1=C(F)C(COC)=C(F)C(F)=C1COC(=O)C1C(C)(C)C1C=C(C)C OOWCJRMYMAMSOH-UHFFFAOYSA-N 0.000 claims description 5
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 claims description 3
- 239000005871 repellent Substances 0.000 claims description 3
- 229920002472 Starch Polymers 0.000 claims description 2
- 238000009837 dry grinding Methods 0.000 claims description 2
- 230000003760 hair shine Effects 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims 2
- 229910052731 fluorine Inorganic materials 0.000 claims 2
- 239000011737 fluorine Substances 0.000 claims 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- GQNBIMLHUAWKHJ-UHFFFAOYSA-N [4-(methoxymethyl)phenyl]methyl 2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound C1=CC(COC)=CC=C1COC(=O)C1C(C)(C)C1C=C(C)C GQNBIMLHUAWKHJ-UHFFFAOYSA-N 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- YREQHYQNNWYQCJ-UHFFFAOYSA-N etofenprox Chemical compound C1=CC(OCC)=CC=C1C(C)(C)COCC1=CC=CC(OC=2C=CC=CC=2)=C1 YREQHYQNNWYQCJ-UHFFFAOYSA-N 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract description 10
- 229910052799 carbon Inorganic materials 0.000 abstract description 10
- 238000004519 manufacturing process Methods 0.000 abstract description 9
- 241000255925 Diptera Species 0.000 abstract description 6
- 229920002678 cellulose Polymers 0.000 abstract description 6
- 235000010980 cellulose Nutrition 0.000 abstract description 6
- 239000001913 cellulose Substances 0.000 abstract description 5
- 229920002261 Corn starch Polymers 0.000 abstract description 4
- 239000008120 corn starch Substances 0.000 abstract description 4
- 229940099112 cornstarch Drugs 0.000 abstract description 4
- 239000000853 adhesive Substances 0.000 abstract description 3
- 230000001070 adhesive effect Effects 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 239000000779 smoke Substances 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 description 8
- 229940071676 hydroxypropylcellulose Drugs 0.000 description 8
- 244000045947 parasite Species 0.000 description 8
- 239000000047 product Substances 0.000 description 8
- 239000000463 material Substances 0.000 description 7
- 239000003814 drug Substances 0.000 description 6
- 239000000428 dust Substances 0.000 description 6
- 239000007921 spray Substances 0.000 description 4
- 239000003905 agrochemical Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 238000004806 packaging method and process Methods 0.000 description 3
- 230000001846 repelling effect Effects 0.000 description 3
- ZCVAOQKBXKSDMS-AQYZNVCMSA-N (+)-trans-allethrin Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(CC=C)C(=O)C1 ZCVAOQKBXKSDMS-AQYZNVCMSA-N 0.000 description 2
- FMTFEIJHMMQUJI-NJAFHUGGSA-N 102130-98-3 Natural products CC=CCC1=C(C)[C@H](CC1=O)OC(=O)[C@@H]1[C@@H](C=C(C)C)C1(C)C FMTFEIJHMMQUJI-NJAFHUGGSA-N 0.000 description 2
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 2
- 235000017491 Bambusa tulda Nutrition 0.000 description 2
- 244000082204 Phyllostachys viridis Species 0.000 description 2
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 2
- 229940024113 allethrin Drugs 0.000 description 2
- 239000011425 bamboo Substances 0.000 description 2
- 235000019504 cigarettes Nutrition 0.000 description 2
- 235000012054 meals Nutrition 0.000 description 2
- 238000007493 shaping process Methods 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 description 1
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 1
- 239000005995 Aluminium silicate Substances 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- DPXJVFZANSGRMM-UHFFFAOYSA-N acetic acid;2,3,4,5,6-pentahydroxyhexanal;sodium Chemical compound [Na].CC(O)=O.OCC(O)C(O)C(O)C(O)C=O DPXJVFZANSGRMM-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 229920006184 cellulose methylcellulose Polymers 0.000 description 1
- 239000003610 charcoal Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000002817 coal dust Substances 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- -1 hydroxypropyl Chemical group 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 230000001172 regenerating effect Effects 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 235000019812 sodium carboxymethyl cellulose Nutrition 0.000 description 1
- 229920001027 sodium carboxymethylcellulose Polymers 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/34—Shaped forms, e.g. sheets, not provided for in any other sub-group of this main group
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/20—Combustible or heat-generating compositions
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N53/00—Biocides, pest repellants or attractants, or plant growth regulators containing cyclopropane carboxylic acids or derivatives thereof
Landscapes
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
The invention discloses a kind of white mosquito-repellent incense and preparation method thereof, belong to mosquito repellent technical field.The mosquito-repellent incense includes mosquito-repellent incense dry body and is sprayed at the anophelifuge composition on mosquito-repellent incense dry body surface, and mosquito-repellent incense dry body is made up of the raw material of following mass percent：Binding and combustion carrier 30 60% and filler 40 70%, the one or more of binding and combustion carrier in cellulose ether, methylcellulose, hydroxypropyl cellulose, hydroxyethyl cellulose and carboxymethyl cellulose, one or more of the filler in bone meal, precipitated calcium carbonate, talcum powder and sweet potato waste powder.The present invention replaces the powdered carbon in conventional mosquito coil as burner body using high molecular cellulose, while cancels the use of other adhesives such as cornstarch, and its outward appearance is white.White mosquito-repellent incense provided by the invention has the advantages that raw material environmental protection is easy to get, simple production process, product weight and burning time stablize, while product smoke content reaches smokeless level.
Description
Technical field
The present invention relates to mosquito repellent technical field, and in particular to a kind of white mosquito-repellent incense and preparation method thereof.
Background technology
Mosquito-repellent incense, it is a kind of mosquito repellent thing, the cigarette that medicine therein is ignited being sent afterwards can mosquitoes or smoked dead mosquito.I
The mosquito-repellent incense of state has long history, and traditional mosquito-repellent incense separated time is fragrant and two kinds of incense coil, with the development of technology, nowadays on the market
There are the novel mosquito repellent incenses such as piece type electric mosquito repellent, Electric liquid mosquito-repellent incense extensively, people can carry out multiple choices as needed.
Conventional mosquito coil is using coal dust, carbon dust（Trees charing powdered carbon, string charing powdered carbon）, wood powder etc. carries for burning
Body, cornstarch, carboxymethyl cellulose etc. is that adhesive, precipitated calcium carbonate, clay etc. is filler, above material is blended,
Mosquito-repellent incense dry body is made after shaping, baking operation, mosquito-repellent incense is made after mosquito-repellent incense dry body spray.
Patent such as Application No. CN 201210210521.0 discloses a kind of smokeless mosquito-repellent incense, its dry body constitutive material
Percentage by weight is：Carbon dust 78-82%, pre-gelatinized starch 4-6%, sodium carboxymethylcellulose 4-6%, cornstarch 4-6% and fine particle calcium carbonate
4-6%；Dry body surface is sprayed with liquid medicine, and liquid medicine is made up of following composition：Agricultural chemicals, deodorized kerosine and mosquito-repellent incense essence composition, its weight
Part it is：Agricultural chemicals 50-60, deodorized kerosine 40-45, mosquito-repellent incense essence 1.8-2.2, described agricultural chemicals are allethrin, tetrafluoro methyl ether chrysanthemum
Ester or fluorine chlorine ether.
Patent such as Application No. 201410492717.2 discloses a kind of smokeless mosquito-repellent incense, by the raw material of following weight proportion
It is made：Charcoal powder 50-60 parts, anchracite duff 10-20 parts, cellulose 5-10 parts, acrylic polyester 1-2 parts, kaolin 3-13 parts, carbon
Sour calcium 5-10 parts, sodium alginate 5-15 parts, spices 1-2 parts and water 1-2 parts.
Problems be present when using existing mosquito-repellent incense in applicant：
First, the carbon dust used in existing mosquito-repellent incense is the carbonization such as trees, bamboo, it is necessary to consume a large amount of green resources；
2nd, the carbon dust that the trees of unlike material or bamboo are fired, proportion and combustibility are different, cause product weight and burning time
It is difficult stabilization etc. index（Such as the mosquito-repellent incense of same formula and thickness, because carbon dust material different weight may differ by more than 10%, combustion
The burning time may differ by more than 25%）, thus directly result in the unstable and product drug effect of active ingredient degree not
It is stable；
3rd, traditional product is black, and production environment is severe, generally there is a larger airborne dust, product also easy dirty hand when in use.
The content of the invention
To solve problem above, through many experiments, the invention provides one kind to use high molecular cellulose as combustion carrier
White smokeless coiled mosquito-repellent incense.The technical scheme is as follows：
On the one hand, the embodiments of the invention provide a kind of white mosquito-repellent incense, including mosquito-repellent incense dry body and it is sprayed at mosquito-repellent incense dry body surface
Anophelifuge is formed.Wherein, mosquito-repellent incense dry body is made up of the raw material of following mass percent：Binding and combustion carrier 30-60% and
Filler 40-70%, a certain proportion of water is added in preparation process, moisture removal is gone by drying after the shaping of mosquito-repellent incense dry body.Wherein.
Binding and combustion carrier are selected from cellulose ether, methylcellulose, hydroxypropyl cellulose, hydroxyethyl cellulose and carboxymethyl cellulose
One or more in the high molecular celluloses such as element, filler are selected from bone meal, precipitated calcium carbonate, talcum powder and sweet potato waste powder etc.
In one or more.Wherein, cellulose ether, methylcellulose, hydroxypropyl cellulose, hydroxyethyl cellulose, carboxymethyl cellulose
Element, bone meal, precipitated calcium carbonate, talcum powder and sweet potato waste powder are colourless or white, make final product for white, it is attractive in appearance and
Will not dry linting.
Wherein, the anophelifuge in the embodiment of the present invention includes the component of following mass percent：Pest repellant 1-30%, perfume (or spice)
Smart 2-5% and deodorized kerosine 60-95% etc..Wherein, pest repellant is selected from fluorine chlorine ether chrysanthemum ester, dimefluthrin and Es- biology allyls
One or more in chrysanthemum ester etc..
Specifically, in the present invention, if pest repellant is fluorine chlorine ether chrysanthemum ester, fluorine chlorine ether chrysanthemum ester accounts for the quality of mosquito-repellent incense dry body
Percentage is 0.05-0.10%（Preferably 0.08%）.If pest repellant is dimefluthrin, dimefluthrin accounts for mosquito-repellent incense
The mass percent of dry body is 0.01-0.05%（Preferably 0.03%）.If pest repellant is Es- bioallethrins, Es- lifes
The mass percent that thing allethrin accounts for mosquito-repellent incense dry body is 0.2-1.0%（Preferably 0.5%）.
Wherein, the molecular weight of the binding in the embodiment of the present invention and combustion carrier is more than 200,000 to ensure its viscosity and combustion
Burning property, can be obtained by regenerative raw materials industrial-scale production.
Wherein, the composition of the binding in the embodiment of the present invention and combustion carrier is in terms of the mass percent of mosquito-repellent incense dry body,
Including in carboxymethyl cellulose 12-15%, hydroxypropyl cellulose 5-10% and cellulose ether, methylcellulose and hydroxyethyl cellulose
One or more（30-60% is gathered together enough with carboxymethyl cellulose and hydroxypropyl cellulose）.
Wherein, the filler in the embodiment of the present invention, which is crushed to 80 mesh and the above, makes its particle more carefully ensure its flammability simultaneously
The not dry linting after mosquito-repellent incense is made.
Wherein, the composition of the filler in the embodiment of the present invention is in terms of the mass percent of mosquito-repellent incense dry body, including sweet potato waste
Powder 13-17%, talcum powder 25-30% and one or both of bone meal and precipitated calcium carbonate（With sweet potato waste powder and talcum powder
Gather together enough 40-70%）.
Wherein, the sweet potato waste powder in the present embodiment, which is prepared the residue after starch by sweet potato and shines dry grinding, forms, by adopting
With cleaning and renewable resource, can not only reduce solid discharge can also reduce cost.In addition, sweet potato waste powder has preferably
Flammability and its there is certain delicate fragrance and repelling effect.
On the other hand, the embodiment of the present invention additionally provides the preparation method of aforementioned white mosquito-repellent incense, and the preparation method includes：
(1) raw material binding and combustion carrier and filler are mixed in agitating device by proportioning（Premixing）15-45 minutes
（Preferably 30 minutes）, then add 0.4-0.8 times of weight of raw material water（Preferably 0.6 times）Wet feed stirring is carried out, wet feed stirs
Mix 10-25 minutes（Preferably 15 minutes）After send mosquito-repellent incense dry body be made in shaper of mosquitor-repellent incense（Including mould it is compressing with it is dry
Dry process）It is standby.
(2) pest repellant, essence and deodorized kerosine mix in stirred tank to be made anophelifuge standby by proportioning, stirs
Mix minute time 15-50（Preferably 30 minutes）.
(3) by proportioning by step (2) prepare anophelifuge be sprayed at step (1) preparation mosquito-repellent incense dry body surface be made it is white
Color mosquito-repellent incense.
Wherein, in step (1), filler is sent into reducing mechanism crushed before mixing, screen size is big
In 80 mesh and its powder of the above as raw material.
Specifically, preparation method provided by the invention includes：
(1) carboxymethyl cellulose 12-15% is pressed（It is rear same in terms of mosquito-repellent incense dry body weight）, hydroxypropyl cellulose 5-10%, cellulose
One or more in ether, methylcellulose and hydroxyethyl cellulose（30- is gathered together enough with carboxymethyl cellulose and hydroxypropyl cellulose
60%）, sweet potato waste powder 13-17%, talcum powder 25-30% and one or both of bone meal and precipitated calcium carbonate（With destarched sweet potato meal
End and talcum powder gather together enough 40-70%）（All raw materials gather together enough 100%）Mixed in agitating device（Premixing）15-45 minutes（It is preferred that
For 30 minutes）, then add 0.4-0.8 times of weight of raw material water（Preferably 0.6 times）Carry out wet feed stirring, wet feed stirring 10-
25 minutes（Preferably 15 minutes）After send that mosquito-repellent incense dry body is made in shaper of mosquitor-repellent incense is standby.
(2) pest repellant 1-30% is pressed（It is rear same in terms of anophelifuge weight）, essence 2-5% and deodorized kerosine 60-95% be sent into
In stirred tank, 15-50 minutes are stirred（It is preferred that 30 minutes）It is standby that anophelifuge is made.
(3) by proportioning by step (2) prepare anophelifuge be sprayed at step (1) preparation mosquito-repellent incense dry body surface be made it is white
Color mosquito-repellent incense.
The present invention replaces the powdered carbon in conventional mosquito coil as burner body using high molecular cellulose, while cancels cornstarch
Etc. the use of other adhesives, its outward appearance is white.There is white mosquito-repellent incense provided by the invention raw material environmental protection to be easy to get, production technology
Simply, the advantages that product weight and burning time stablize, while product smoke content reaches smokeless level.
Embodiment
The invention will be further elaborated by the following examples, but is not limited to content as described below.
Embodiment one
Embodiment 1 provides the preparation process of white mosquito-repellent incense, comprises the following steps：
1st, the making of mosquito-repellent incense dry body：Respectively by weight than the cellulose ether for 5%, 8% methylcellulose, 5% hydroxy propyl cellulose
Element, 12% carboxymethyl cellulose, 10% bone meal, 17% precipitated calcium carbonate, 28% talcum powder and 15% sweet potato waste powder,
Add in fine material mixer and carry out premix 30 minutes, the water for then adding powder 0.6 times of weight of weight carries out wet feed stirring, stirring
Time general control was at 15 minutes or so.Wet feed is subjected to punch forming by mosquito-repellent incense former after the completion of stirring, then entered again
Row drying just obtains white smokeless mosquito-repellent incense dry body.
2nd, the configuration of mosquito-repellent incense medicament：Respectively by weight fluorine chlorine ether chrysanthemum ester active compound, 4% essence and 91% deodorization for being 5%
Kerosene adds stirring 30 minutes in stirred tank, just completes the preparation of decoction.
3rd, spray packaging：The dry body every made in advance is sprayed 0.6 gram, then packs and just completes the smokeless disk of white
The making of formula mosquito-repellent incense.
Sample survey result：
Table 1
Wherein, table 1 is the detection data of the mosquito-repellent incense of the present embodiment production.In addition, by range estimation, the mosquito-repellent incense of this implementation production is white
Color, during hand-held will not dry linting, hand is clean and free from extraneous odour, and smokeless during burning, indices meet or more than professional standard.
Table 2
| This patent | Commercially available mosquito-repellent incense | |
| Quantity（Disk） | 200 disks | 200 disks |
| Disk average weight（g） | 36.1 | 36.3 |
| ＞ 10% | 0 | 3 disks |
| +8%—+10% | 0 | 3 disks |
| +6%—+8% | 0 | 4 disks |
| +4%—+6% | 1 disk | 9 disks |
| +2%—+4% | 2 disks | 13 disks |
| +1%—+2% | 19 disks | 20 disks |
| +0.5%—+1% | 35 disks | 26 disks |
| 0—+0.5% | 42 disks | 23 disks |
| +0% | 2 disks | 1 disk |
| -0.5%—0% | 41 disks | 25 disks |
| -1%—-0.5% | 37 disks | 25 disks |
| -2%—-1% | 17 disks | 19 disks |
| -4%—-2% | 3 disks | 10 disks |
| -6%—-4% | 1 disk | 9 disks |
| -8%—-6% | 0 | 5 disks |
| -10%—-8% | 0 | 2 disks |
| ＜ -10% | 0 | 3 disks |
Table 3
| This patent | Commercially available mosquito-repellent incense | |
| Quantity（Disk） | 200 disks | 200 disks |
| Expelling parasite agent content（wt%） | 0.08 | 0.10 |
| ＞ 40% | 0 | 3 disks |
| +30%—+40% | 0 | 5 disks |
| +20%—+30% | 0 | 6 disks |
| +15%—+20% | 0 | 9 disks |
| +10%—+15% | 3 disks | 12 disks |
| +5%—+10% | 7 disks | 22 disks |
| +2%—+5% | 47 disks | 21 disks |
| 0—+2% | 40 disks | 19 disks |
| +0% | 3 disks | 4 disks |
| -1%—0% | 17 disks | 9 disks |
| -2%—-1% | 24 disks | 11 disks |
| -4%—-2% | 38 disks | 20 disks |
| -8%—-4% | 10 disks | 24 disks |
| -12%—-8% | 7 disks | 15 disks |
| -16%—-12% | 3 disks | 9 disks |
| -20%—-16% | 1 disk | 5 disks |
| ＜ -20% | 0 | 6 disks |
Table 4
| This patent | Commercially available mosquito-repellent incense | |
| Quantity（Disk） | 200 disks | 200 disks |
| Burning time（h） | 8.3 | 7.8 |
| ＞ 10% | 0 | 1 disk |
| +8%—+10% | 0 | 4 disks |
| +6%—+8% | 0 | 8 disks |
| +4%—+6% | 4 disks | 13 disks |
| +2%—+4% | 10 disks | 17 disks |
| +1%—+2% | 18 disks | 19 disks |
| +0.5%—+1% | 33 disks | 21 disks |
| 0—+0.5% | 34 disks | 17 disks |
| +0% | 0 | 1 disk |
| -0.5%—0% | 35 disks | 16 disks |
| -1%—-0.5% | 35 disks | 24 disks |
| -2%—-1% | 17 disks | 18 disks |
| -4%—-2% | 9 disks | 18 disks |
| -6%—-4% | 5 disks | 12 disks |
| -8%—-4% | 0 | 6 disks |
| -10%—-8% | 0 | 5 disks |
| ＜ 10% | 0 | 0 |
Wherein, table 2-4 is the portioned product inspected by random samples as described in Example 1 and in a batch mosquito-repellent incense of proportioning production and commercially available mosquito
Fragrant contrast, and the percentage in table represents and the deviation of average value.Wherein, the mosquito-repellent incense date of manufacture of this patent is 2017
March, commercially available mosquito-repellent incense come from supermarket, and the date of manufacture is on March 16th, 2017, and its index marked weighs 35g, fluorine chlorine ether chrysanthemum ester for disk
Mass fraction is 0.08%, and burning time is a whole night, and color is black.From table 2 it can be seen that the disk weight of the mosquito-repellent incense of the present invention
It is mainly distributed in ± 2% deviation range, disk weight is highly stable, and the disk of commercially available prod is mainly distributed on ± 6% deviation again
In the range of, cause the more difficult control of disk weight, and then expelling parasite agent content and burning time are difficult to control, and cause unstable product quality.
From table 3 it can be seen that the expelling parasite agent content of the present invention is mainly distributed in ± 5% deviation range, expelling parasite agent content is relatively stable,
And the expelling parasite agent content of commercially available prod is mainly distributed in ± 15% deviation range, pest repellant content deviation is larger, in low expelling parasite
Repelling effect is unable to reach under agent content, and cost can be dramatically increased under high expelling parasite agent content, in the prior art in order to solve
The unstable situation of pest repellant, it will usually additionally increase 5-20% pest repellant dosage on standard content to ensure repelling effect,
In a disguised form add cost（Increased cost and the increased cost of this patent dry body are similar）.From table 4, it can be seen that the present invention
Burning time is mainly distributed in ± 2% deviation range, and burning time is highly stable, and the burning time of commercially available prod is main
It is distributed in ± 6% deviation range, burning time deviation is maximum up to 10%, and the burning deviation more than half an hour can cause user
Experience it is bad.
To sum up, mosquito-repellent incense indices produced by the invention be can be seen that from table 1-4 and meets or exceeds industry index, and its
The parameters such as disk weight, expelling parasite agent content and burning time are relatively stable, by accurately controlling each parameter in a disguised form to reduce cost.
Embodiment two
Embodiment 2 provides the preparation process of white mosquito-repellent incense, comprises the following steps：
1st, the making of mosquito-repellent incense dry body：It is respectively that weight is more fine than the cellulose ether for 6%, 6% hydroxyethyl cellulose, 8% hydroxypropyl
Dimension element, 12% carboxymethyl cellulose, 12% bone meal, 18% precipitated calcium carbonate, 25% talcum powder and 13% destarched sweet potato meal
End, adding in fine material mixer and carry out premix 30 minutes, the water for then adding powder 0.7 times of weight of weight carries out wet feed stirring,
Mixing time general control was at 15 minutes or so.Wet feed is subjected to punch forming by mosquito-repellent incense former after the completion of stirring, then
Dried again and just obtain white smokeless mosquito-repellent incense dry body.
2nd, the configuration of mosquito-repellent incense medicament：Respectively by weight the dimefluthrin active compound for 1.8%, 4% essence and 94.2%
Deodorized kerosine add stirred tank in stirring 30 minutes, just complete decoction preparation.
3rd, spray packaging：The dry body every made in advance is sprayed 0.6 gram, then packs and just completes the smokeless disk of white
The making of formula mosquito-repellent incense.
Sample survey result is as shown in table 5：
Table 5
Embodiment three
1st, the making of mosquito-repellent incense dry body：Respectively by weight than hydroxyethyl cellulose for 15%, 10% hydroxypropyl cellulose, 15%
Carboxymethyl cellulose, 18% precipitated calcium carbonate, 25% talcum powder and 17% sweet potato waste powder, add in fine material mixer
Row premix 30 minutes, the water for then adding powder 0.6 times of weight of weight carry out wet feed stirring, and mixing time general control is at 15 points
Clock or so.Wet feed is subjected to punch forming by mosquito-repellent incense former after the completion of stirring, is then dried again and just obtains white nothing
Cigarette mosquito-repellent incense dry body.
2nd, the configuration of mosquito-repellent incense medicament：Respectively by weight the Es- bioallethrins active compound for 30%, 4% essence and 66%
Deodorized kerosine add stirred tank in stirring 30 minutes, just complete decoction preparation.
3rd, spray packaging：The dry body every made in advance is sprayed 0.6 gram, then packs and just completes the smokeless disk of white
The making of formula mosquito-repellent incense.
Sample survey result is as shown in table 6：
Table 6
Presently preferred embodiments of the present invention is the foregoing is only, is not intended to limit the invention, it is all in the spirit and principles in the present invention
Within, any modification, equivalent substitution and improvements made etc., it should be included in the scope of the protection.
Claims (9)
1. a kind of white mosquito-repellent incense, including mosquito-repellent incense dry body and the anophelifuge composition for being sprayed at mosquito-repellent incense dry body surface, its feature exist
In the mosquito-repellent incense dry body is made up of the raw material of following mass percent：Binding and combustion carrier 30-60% and filler 40-
70%, the binding and combustion carrier are selected from cellulose ether, methylcellulose, hydroxypropyl cellulose, hydroxyethyl cellulose and carboxylic
One or more in methylcellulose, the filler is in bone meal, precipitated calcium carbonate, talcum powder and sweet potato waste powder
It is one or more.
2. white mosquito-repellent incense according to claim 1, it is characterised in that the anophelifuge includes following mass percent
Component：Pest repellant 1-30%, essence 2-5% and deodorized kerosine 60-95%, the pest repellant are selected from fluorine chlorine ether chrysanthemum ester, tetrafluoro methyl ether chrysanthemum
One or more in ester and Es- bioallethrins.
3. white mosquito-repellent incense according to claim 2, it is characterised in that when the pest repellant is fluorine chlorine ether chrysanthemum ester, the chlorine
The mass percent that fluorine ethofenprox accounts for mosquito-repellent incense dry body is 0.05-0.10%；When the pest repellant is dimefluthrin, described four
The mass percent that fluorine methothrin accounts for mosquito-repellent incense dry body is 0.01-0.05%；When the pest repellant is Es- bioallethrins, institute
It is 0.2-1.0% to state Es- bioallethrins and account for the mass percent of mosquito-repellent incense dry body.
4. white mosquito-repellent incense according to claim 1, it is characterised in that the molecular weight of the binding and combustion carrier is more than
200000.
5. white mosquito-repellent incense according to claim 1, it is characterised in that the composition of the binding and combustion carrier is with mosquito-repellent incense
The mass percent meter of dry body, including carboxymethyl cellulose 12-15%, hydroxypropyl cellulose 5-10% and cellulose ether, methyl fibre
Dimension element and the one or more in hydroxyethyl cellulose.
6. white mosquito-repellent incense according to claim 1, it is characterised in that the filler be crushed to 80 mesh and more than.
7. white mosquito-repellent incense according to claim 1, it is characterised in that the composition of the filler is with the quality of mosquito-repellent incense dry body
Percentages, including sweet potato waste powder 13-17%, talcum powder 25-30% and one or both of bone meal and precipitated calcium carbonate.
8. the white mosquito-repellent incense according to claim 1 or 7, it is characterised in that the sweet potato waste powder prepares starch by sweet potato
Residue afterwards shines dry grinding and formed.
9. the preparation method of the white mosquito-repellent incense as described in claim any one of 1-8, it is characterised in that the preparation method bag
Include：
(1) raw material binding and combustion carrier and filler are mixed into 15-45 minutes in agitating device by proportioning, then added
The water of 0.4-0.8 times of weight of raw material carries out wet feed stirring, and wet feed send after stirring 10-25 minutes and mosquito-repellent incense is made in shaper of mosquitor-repellent incense
Dry body；
(2) pest repellant, essence and deodorized kerosine are mixed by proportioning and anophelifuge is made；
(3) anophelifuge is sprayed at mosquito-repellent incense dry body surface by proportioning and white mosquito-repellent incense is made.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108853168A (en) * | 2018-07-13 | 2018-11-23 | 滁州职业技术学院 | A kind of perfume (or spice) and preparation method thereof with chrysanthemum perfume |
| CN109381726A (en) * | 2018-12-17 | 2019-02-26 | 湖北瑞晟农业科技有限责任公司 | A kind of Lemon Basil Pelargonium composite fibre incense coil manufacturing technology |
| CN111296431A (en) * | 2019-11-04 | 2020-06-19 | 吉林省农业科学院 | Plant smoking agent for expelling insects and killing insects and use method thereof |
| CN111937867A (en) * | 2019-10-08 | 2020-11-17 | 田文长 | Method for making incense by adopting cellulose ether |
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| JPS4838348A (en) * | 1971-09-18 | 1973-06-06 | ||
| CN1273030A (en) * | 1999-05-07 | 2000-11-15 | 约翰逊父子公司 | Piece for diffusing volatile |
| CN102754658A (en) * | 2012-06-25 | 2012-10-31 | 安徽立康杀虫制品有限公司 | Smokeless mosquito coil and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| JPS4838348A (en) * | 1971-09-18 | 1973-06-06 | ||
| CN1273030A (en) * | 1999-05-07 | 2000-11-15 | 约翰逊父子公司 | Piece for diffusing volatile |
| CN102754658A (en) * | 2012-06-25 | 2012-10-31 | 安徽立康杀虫制品有限公司 | Smokeless mosquito coil and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108853168A (en) * | 2018-07-13 | 2018-11-23 | 滁州职业技术学院 | A kind of perfume (or spice) and preparation method thereof with chrysanthemum perfume |
| CN108853168B (en) * | 2018-07-13 | 2021-07-20 | 滁州职业技术学院 | A kind of fragrance with chrysanthemum fragrance and preparation method thereof |
| CN109381726A (en) * | 2018-12-17 | 2019-02-26 | 湖北瑞晟农业科技有限责任公司 | A kind of Lemon Basil Pelargonium composite fibre incense coil manufacturing technology |
| CN111937867A (en) * | 2019-10-08 | 2020-11-17 | 田文长 | Method for making incense by adopting cellulose ether |
| CN111296431A (en) * | 2019-11-04 | 2020-06-19 | 吉林省农业科学院 | Plant smoking agent for expelling insects and killing insects and use method thereof |
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