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CN107550819A - A kind of preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving - Google Patents

A kind of preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving Download PDF

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Publication number
CN107550819A
CN107550819A CN201710916811.XA CN201710916811A CN107550819A CN 107550819 A CN107550819 A CN 107550819A CN 201710916811 A CN201710916811 A CN 201710916811A CN 107550819 A CN107550819 A CN 107550819A
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CN
China
Prior art keywords
parts
wet tissue
chinese medicine
sterilizing
itch
Prior art date
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Pending
Application number
CN201710916811.XA
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Chinese (zh)
Inventor
郑磊
张辉
李继龙
汪青
李继春
何金林
陶续
贺佳
孙晓莉
张国庆
徐国庆
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Anhui Hanbon Daily Chemical Co Ltd
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Anhui Hanbon Daily Chemical Co Ltd
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Priority to CN201710916811.XA priority Critical patent/CN107550819A/en
Publication of CN107550819A publication Critical patent/CN107550819A/en
Pending legal-status Critical Current

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  • Cosmetics (AREA)

Abstract

The invention discloses a kind of preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving, domestic silkworm silk is soaked into Na2CO3In solution, it is placed in 95 100 DEG C of water-baths and handles 30 40min, obtain fibroin fiber;Prepare the mixed solution of calcium chloride and acetic acid;The spunlace non-woven cloth folded after cutting is placed in the silk fibroin aqueous solution that S2 is obtained, soaks 2 4h;Nonwoven after being soaked in S3 is arranged in 30 DEG C of hot air driers and dries 7 8h;Prepare Chinese medicine extract;The dried nonwovens of S4 are arranged in the wet tissue liquid and soak 3 4h, are passed through ozone, sealed, sterile is taken out and is packaged to be wet tissue.The invention discloses a kind of preparation method of traditional Chinese medicine wet tissue, silk fibroin aqueous solution is added in wet tissue, lifts the tensile property and ductility of wet tissue, while plurality of Chinese medicinal material is added in wet tissue, does not produce damage to skin, while there is the effect of sterilizing and itch-relieving.

Description

A kind of preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving
Technical field
The invention belongs to wet tissue processing technique field, more particularly to a kind of preparation side of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving Method.
Background technology
With the continuous improvement of social and economic level, people, which are no longer only satisfied with, to have enough to eat and wear, and more starts to focus on life Taste, improves the quality of living.Increasingly severe pollution problem causes the enough attention of people, more focuses on safety therewith and defends Raw, sterilizing, then there have been easy to carry, safety and sanitation Sanitary products based on pasteurization towelette.
Especially in recent years, the application of hygenic towelette and disinfection wet tissue gradually increases, but traditional wet tissue is mostly with poly- Ethene, polypropylene, polyester and polyamide are the non-woven cloth of material as matrix, although cheap, its maximum Shortcoming videlicet can not be biodegradable, is difficult to reclaim again, a large amount of uses can cause white pollution.It is in addition, wet for manufacture feature Towel, it is also necessary to prepare the reagent for including many chemical compositions, easy polluted source.
In addition, currently used disinfected paper napkin is typically all to have volatilization containing alcohol, essence and preservative, alcohol Property, skin surface water loss easily make it that after wiping, essence has stimulation component, there is injury to human skin, easy allergy, separately Outer preservative also easily causes allergy, easily carcinogenic.
Therefore, one kind effectively can either will not produce stimulation by cleaning-sterilizing again, and can voluntarily degrade, non-environmental-pollution Pasteurization towelette be consumer there is an urgent need to.
The content of the invention
It is an object of the invention to provide a kind of preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving, the draftability of wet tissue is lifted Energy and ductility, have the effect of sterilizing and itch-relieving.
The present invention is achieved by the following technical solutions:
A kind of preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving, this method comprise the following steps:
S1, domestic silkworm silk is soaked into Na2CO3In solution, it is placed in 95-100 DEG C of water-bath and handles 30-40min, obtain fibroin Fiber;
S2, the mixed solution for preparing calcium chloride and acetic acid;
S3, by fold cut after spunlace non-woven cloth be placed in the silk fibroin aqueous solution that S2 is obtained, soak 2-4h;
S4, the nonwoven after being soaked in S3 is arranged in 30 DEG C of hot air driers and dries 7-8h;
S5, prepare Chinese medicine extract;
S6, the dried nonwovens of S4 are arranged in the wet tissue liquid and soak 3-4h, be passed through ozone, take out sealed, sterile It is packaged to be wet tissue.
Further, the volume ratio of calcium chloride, acetic acid and water is in the mixed solution of the calcium chloride and acetic acid, by fibroin Fibrinolysis is in the mixed solution, 75-80 DEG C of magnetic agitation 30-60min, and room temperature is cooled to after stirring, and dialyse 64- 72h obtains silk fibroin aqueous solution.
Further, the non-woven fabrics is spunlace non-woven cloth.
Further, described Chinese medicine extract includes following raw material:Radix Angelicae Sinensis 8-10 parts, peppermint 16-18 parts, Pu Public 14 parts of English, matrimony vine 30-35 parts, Asiatic plantain 12-14 parts, 16 parts of cassia seed, 18 parts of melia toosendan, radix glycyrrhizae 22-25 parts, 15 parts of tendril-leaved fritillary bulb, 3 parts of radix scrophulariae, Semen Cuscutae 5-9 parts, root of herbaceous peony 2-4 parts, pungent 8 parts of sprout, great burdock achene 5-7 parts, deionized water 200-250 parts.
The invention has the advantages that:
The invention discloses a kind of preparation method of traditional Chinese medicine wet tissue, silk fibroin aqueous solution is added in wet tissue, lifts the drawing of wet tissue Performance and ductility are stretched, while plurality of Chinese medicinal material is added in wet tissue, does not produce damage to skin, while there is sterilizing and itch-relieving Effect.
Certainly, any product for implementing the present invention it is not absolutely required to reach all the above advantage simultaneously.
Embodiment
Technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is only Part of the embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art The all other embodiment obtained under the premise of creative work is not made, belongs to the scope of protection of the invention.
Embodiment 1
S1, domestic silkworm silk is soaked into Na2CO3In solution, it is placed in 95-100 DEG C of water-bath and handles 30-40min, obtain fibroin Fiber;
S2, configuration calcium chloride and acetic acid mixed solution, the volume ratio of wherein calcium chloride, acetic acid and water are, fibroin is fine Dimension is dissolved in the mixed solution, 75 DEG C of magnetic agitation 30min, and room temperature is cooled to after stirring, and dialysis 64h obtains fibroin The aqueous solution;
S3, by fold cut after spunlace non-woven cloth be placed in the silk fibroin aqueous solution that S2 is obtained, soak 2-4h;
S4, the nonwoven after being soaked in S3 is arranged in 30 DEG C of hot air driers and dries 7-8h;
S5, Chinese medicine extract is prepared, described Chinese medicine extract includes following raw material:8 parts of Radix Angelicae Sinensis, peppermint 16 Part, 14 parts of dandelion, 30 parts of matrimony vine, 12 parts of Asiatic plantain, 16 parts of cassia seed, 18 parts of melia toosendan, 22 parts of radix glycyrrhizae, 15 parts of tendril-leaved fritillary bulb, radix scrophulariae 3 Part, 5 parts of Semen Cuscutae, 2 parts of the root of herbaceous peony, pungent 8 parts of sprout, 5 parts of great burdock achene, 200 parts of deionized water;
S6, the dried nonwovens of S4 are arranged in the wet tissue liquid and soak 3h, be passed through ozone, take out sealed, sterile bag Dress obtains wet tissue.
Embodiment 2
S1, domestic silkworm silk is soaked into Na2CO3In solution, it is placed in 100 DEG C of water-baths and handles 40min, obtain fibroin fiber;
S2, configuration calcium chloride and acetic acid mixed solution, the volume ratio of wherein calcium chloride, acetic acid and water are, fibroin is fine Dimension is dissolved in the mixed solution, 80 DEG C of magnetic agitation 60min, and room temperature is cooled to after stirring, and dialysis 72h obtains fibroin The aqueous solution;
S3, by fold cut after spunlace non-woven cloth be placed in the silk fibroin aqueous solution that S2 is obtained, soak 2-4h;
S4, the nonwoven after being soaked in S3 is arranged in 30 DEG C of hot air driers and dries 7-8h;
S5, Chinese medicine extract is prepared, described Chinese medicine extract includes following raw material:10 parts of Radix Angelicae Sinensis, peppermint 18 Part, 14 parts of dandelion, 35 parts of matrimony vine, 14 parts of Asiatic plantain, 16 parts of cassia seed, 18 parts of melia toosendan, 25 parts of radix glycyrrhizae, 15 parts of tendril-leaved fritillary bulb, radix scrophulariae 3 Part, 9 parts of Semen Cuscutae, 4 parts of the root of herbaceous peony, pungent 8 parts of sprout, 7 parts of great burdock achene, 250 parts of deionized water;
S6, the dried nonwovens of S4 are arranged in the wet tissue liquid and soak 4h, be passed through ozone, take out sealed, sterile bag Dress obtains wet tissue.
Embodiment 3
S1, domestic silkworm silk is soaked into Na2CO3In solution, it is placed in 98 DEG C of water-baths and handles 35min, obtain fibroin fiber;
S2, configuration calcium chloride and acetic acid mixed solution, the volume ratio of wherein calcium chloride, acetic acid and water are, fibroin is fine Dimension is dissolved in the mixed solution, 78 DEG C of magnetic agitation 45min, and room temperature is cooled to after stirring, and dialysis 68h obtains fibroin The aqueous solution;
S3, by fold cut after spunlace non-woven cloth be placed in the silk fibroin aqueous solution that S2 is obtained, soak 2-4h;
S4, the nonwoven after being soaked in S3 is arranged in 30 DEG C of hot air driers and dries 7-8h;
S5, Chinese medicine extract is prepared, described Chinese medicine extract includes following raw material:9 parts of Radix Angelicae Sinensis, peppermint 17 Part, 14 parts of dandelion, matrimony vine 30-35 parts, Asiatic plantain 12-14 parts, 16 parts of cassia seed, 18 parts of melia toosendan, 24 parts of radix glycyrrhizae, tendril-leaved fritillary bulb 15 Part, 3 parts of radix scrophulariae, 7 parts of Semen Cuscutae, 3 parts of the root of herbaceous peony, pungent 8 parts of sprout, 6 parts of great burdock achene, 230 parts of deionized water;
S6, the dried nonwovens of S4 are arranged in the wet tissue liquid and soak 3.5h, be passed through ozone, take out sealed, sterile It is packaged to be wet tissue.
Above content is only citing made for the present invention and explanation, and affiliated those skilled in the art are to being retouched The specific embodiment stated is made various modifications or supplement or substituted using similar mode, without departing from invention or super More scope defined in the claims, protection scope of the present invention all should be belonged to.

Claims (4)

1. a kind of preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving, it is characterised in that this method comprises the following steps:
S1, domestic silkworm silk is soaked into Na2CO3In solution, it is placed in 95-100 DEG C of water-bath and handles 30-40min, obtain fibroin fiber;
S2, the mixed solution for preparing calcium chloride and acetic acid;
S3, by fold cut after spunlace non-woven cloth be placed in the silk fibroin aqueous solution that S2 is obtained, soak 2-4h;
S4, the nonwoven after being soaked in S3 is arranged in 30 DEG C of hot air driers and dries 7-8h;
S5, prepare Chinese medicine extract;
S6, the dried nonwovens of S4 are arranged in the wet tissue liquid and soak 3-4h, be passed through ozone, take out sealed, sterile packaging Obtain wet tissue.
A kind of 2. preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving according to claim 1, it is characterised in that:The chlorination The volume ratio of calcium chloride, acetic acid and water is that fibroin fiber is dissolved in the mixed solution in the mixed solution of calcium and acetic acid, 75-80 DEG C of magnetic agitation 30-60min, is cooled to room temperature after stirring, dialysis 64-72h obtains silk fibroin aqueous solution.
A kind of 3. preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving according to claim 1, it is characterised in that:The nonwoven Cloth is spunlace non-woven cloth.
A kind of 4. preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving according to claim 1, it is characterised in that:In described Medicament extracting solution includes following raw material:Radix Angelicae Sinensis 8-10 parts, peppermint 16-18 parts, 14 parts of dandelion, matrimony vine 30-35 parts, Chinese herbaceous peony Careless 12-14 parts, 16 parts of cassia seed, 18 parts of melia toosendan, radix glycyrrhizae 22-25 parts, 15 parts of tendril-leaved fritillary bulb, 3 parts of radix scrophulariae, Semen Cuscutae 5-9 parts, root of herbaceous peony 2- 4 parts, it is pungent sprout 8 parts, great burdock achene 5-7 parts, deionized water 200-250 parts.
CN201710916811.XA 2017-09-30 2017-09-30 A kind of preparation method of the traditional Chinese medicine wet tissue of sterilizing and itch-relieving Pending CN107550819A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012067032A (en) * 2010-09-22 2012-04-05 Arimino Kagaku Kk Hair cosmetic preparation to fill up non-aerosol foamer for use
CN103361885A (en) * 2013-06-28 2013-10-23 上海纳米技术及应用国家工程研究中心有限公司 Preparation method of antibacterial silk fibroin fibrous membrane
CN104324204A (en) * 2014-10-08 2015-02-04 青岛叁鼎卫生制品有限公司 Wet tissue liquid of wet toilet tissue
CN104606083A (en) * 2013-11-04 2015-05-13 天津市蓟县岐山科技有限公司 Traditional Chinese medicine disinfection wet tissue

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2012067032A (en) * 2010-09-22 2012-04-05 Arimino Kagaku Kk Hair cosmetic preparation to fill up non-aerosol foamer for use
CN103361885A (en) * 2013-06-28 2013-10-23 上海纳米技术及应用国家工程研究中心有限公司 Preparation method of antibacterial silk fibroin fibrous membrane
CN104606083A (en) * 2013-11-04 2015-05-13 天津市蓟县岐山科技有限公司 Traditional Chinese medicine disinfection wet tissue
CN104324204A (en) * 2014-10-08 2015-02-04 青岛叁鼎卫生制品有限公司 Wet tissue liquid of wet toilet tissue

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
苏州丝绸工学院: "《制丝化学》", 30 June 1996, 中国纺织出版社 *
谢光银等: "《机织物设计基础学》", 30 August 2010, 东华大学出版社 *

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Application publication date: 20180109