CN107201065A - A kind of diatom ooze ornament materials and preparation method thereof - Google Patents
A kind of diatom ooze ornament materials and preparation method thereof Download PDFInfo
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- CN107201065A CN107201065A CN201710589056.9A CN201710589056A CN107201065A CN 107201065 A CN107201065 A CN 107201065A CN 201710589056 A CN201710589056 A CN 201710589056A CN 107201065 A CN107201065 A CN 107201065A
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- 239000000463 material Substances 0.000 title claims abstract description 82
- 238000002360 preparation method Methods 0.000 title claims description 11
- 239000000843 powder Substances 0.000 claims abstract description 101
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 52
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 47
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 47
- 241001330002 Bambuseae Species 0.000 claims abstract description 47
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 47
- 239000011425 bamboo Substances 0.000 claims abstract description 47
- 239000003610 charcoal Substances 0.000 claims abstract description 47
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 42
- 229910052613 tourmaline Inorganic materials 0.000 claims abstract description 41
- 239000011032 tourmaline Substances 0.000 claims abstract description 41
- 229940070527 tourmaline Drugs 0.000 claims abstract description 41
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 39
- 239000000835 fiber Substances 0.000 claims abstract description 39
- 239000000654 additive Substances 0.000 claims abstract description 34
- 230000000996 additive effect Effects 0.000 claims abstract description 34
- 239000002270 dispersing agent Substances 0.000 claims abstract description 33
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 29
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 29
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 29
- 239000003054 catalyst Substances 0.000 claims abstract description 28
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 27
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000440 bentonite Substances 0.000 claims abstract description 26
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 26
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229910021389 graphene Inorganic materials 0.000 claims abstract description 26
- 239000010445 mica Substances 0.000 claims abstract description 26
- 229910052618 mica group Inorganic materials 0.000 claims abstract description 26
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 26
- 239000011230 binding agent Substances 0.000 claims abstract description 25
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims abstract description 24
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims abstract description 24
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims abstract description 24
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims abstract description 24
- 125000000129 anionic group Chemical group 0.000 claims abstract description 19
- 239000002994 raw material Substances 0.000 claims abstract description 16
- 238000000034 method Methods 0.000 claims description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 150000001450 anions Chemical class 0.000 claims description 15
- 238000000227 grinding Methods 0.000 claims description 15
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 14
- 238000001914 filtration Methods 0.000 claims description 14
- 238000005406 washing Methods 0.000 claims description 14
- 230000004048 modification Effects 0.000 claims description 12
- 238000012986 modification Methods 0.000 claims description 12
- 230000000694 effects Effects 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 239000002202 Polyethylene glycol Substances 0.000 claims description 7
- 229960000583 acetic acid Drugs 0.000 claims description 7
- 239000004744 fabric Substances 0.000 claims description 7
- 239000012362 glacial acetic acid Substances 0.000 claims description 7
- 150000002500 ions Chemical class 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 229920001223 polyethylene glycol Polymers 0.000 claims description 7
- -1 polypropylene Polymers 0.000 claims description 7
- 239000004743 Polypropylene Substances 0.000 claims description 5
- 229920002678 cellulose Polymers 0.000 claims description 5
- 239000001913 cellulose Substances 0.000 claims description 5
- 229920002401 polyacrylamide Polymers 0.000 claims description 5
- 229920001155 polypropylene Polymers 0.000 claims description 5
- 239000002689 soil Substances 0.000 claims description 5
- 229920000049 Carbon (fiber) Polymers 0.000 claims description 4
- 238000001354 calcination Methods 0.000 claims description 4
- 239000004917 carbon fiber Substances 0.000 claims description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 4
- 229920003091 Methocel™ Polymers 0.000 claims 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
- 230000008961 swelling Effects 0.000 claims 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract description 9
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract description 6
- 239000010432 diamond Substances 0.000 abstract description 4
- 229910003460 diamond Inorganic materials 0.000 abstract description 4
- 230000002265 prevention Effects 0.000 abstract description 4
- 239000005416 organic matter Substances 0.000 abstract description 3
- 230000004202 respiratory function Effects 0.000 abstract description 3
- 238000001179 sorption measurement Methods 0.000 abstract description 2
- 239000000839 emulsion Substances 0.000 description 6
- 238000001238 wet grinding Methods 0.000 description 6
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
- 240000007594 Oryza sativa Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 239000011787 zinc oxide Substances 0.000 description 2
- 239000005909 Kieselgur Substances 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 230000001458 anti-acid effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 238000005341 cation exchange Methods 0.000 description 1
- 229920003086 cellulose ether Polymers 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000019646 color tone Nutrition 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010292 electrical insulation Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 229920002689 polyvinyl acetate Polymers 0.000 description 1
- 239000011118 polyvinyl acetate Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
- Catalysts (AREA)
Abstract
The invention discloses a kind of diatom ooze ornament materials, include the raw material of following parts by weight：30~50 parts of diatomite, 7~13 parts of bentonite, 10~20 parts of calcined kaolin, 3~8 parts of modified Nano bamboo charcoal powder, 6~14 parts of mica powder, 5~10 parts of titanium dioxide, 1~2 part of hydroxypropyl methyl cellulose ether, 3~5 parts of anti-crack fiber, 4~9 parts of graphene oxide, 2~3 parts of tourmaline powder anionic additive, 7~11 parts of modifying agent, 1.5~2.5 parts of dispersant, 6~13 parts of inorganic binder, catalyst 0.5~1.5 part of nano zine oxide of level.The diatom ooze ornament materials has a variety of functions such as Diamond Search, heatproof fire prevention, organic matter wear-resistant, with respiratory function, energy formaldehyde adsorption, toluene etc, and performance is stable, and Acceptable life is long.
Description
Technical field
The invention belongs to building material technical field, and in particular to a kind of diatom ooze ornament materials and preparation method thereof.
Background technology
Decorative material for internal wall on the market is mainly aqueous emulsion paint at present, is called emulsion paint, is divided into polyvinyl acetate
Emulsion and the major class of acrylic emulsion two, interior wall coating advantage are that construction is simple, have multiple color tones, various decorations are preferably interspersed thereon
Product, decorative effect simplicity generosity, are widely used.China's development and production since the eighties, existing tens kind models so far,
Its basic performance is identical, is substantially made up of water, pigment, emulsion, filler and various auxiliary agents.But it is this by emulsion, auxiliary agent
Etc. the interior wall coating being made, there are VOC emission, heatproof of not preventing fires, containing heavy metal.
The content of the invention
The invention provides a kind of diatom ooze ornament materials and preparation method thereof, asking in above-mentioned background technology is solved
Topic, the diatom ooze ornament materials have Diamond Search, heatproof fire prevention, it is wear-resistant, with respiratory function, can formaldehyde adsorption, toluene it
A variety of functions such as the organic matter of class, performance is stable, and Acceptable life is long.
In order to solve the problem of prior art is present, adopt the following technical scheme that：
A kind of diatom ooze ornament materials, includes the raw material of following parts by weight：30~50 parts of diatomite, 7~13 parts of bentonite, calcining
10~20 parts of kaolin, 3~8 parts of modified Nano bamboo charcoal powder, 6~14 parts of mica powder, 5~10 parts of titanium dioxide, hydroxypropyl methyl
1~2 part of cellulose ether, 3~5 parts of anti-crack fiber, 4~9 parts of graphene oxide, 2~3 parts of tourmaline powder anionic additive, change
Property 7~11 parts of agent, 1.5~2.5 parts of dispersant, 6~13 parts of inorganic binder, catalyst level 0.5~1.5 part of nano zine oxide.
It is preferred that, the diatom ooze ornament materials includes the raw material of following parts by weight：35~45 parts of diatomite, bentonite 9
~12 parts, 13~18 parts of calcined kaolin, 4~7 parts of modified Nano bamboo charcoal powder, 8~12 parts of mica powder, 7~9 parts of titanium dioxide,
1.3~1.8 parts of hydroxypropyl methyl cellulose ether, 3.2~4.6 parts of anti-crack fiber, 6~8 parts of graphene oxide, tourmaline powder bear from
Sub- 2.4~2.9 parts of additive, 8~10 parts of modifying agent, 1.7~2.2 parts of dispersant, 8~12 parts of inorganic binder, catalyst level are received
0.9~1.4 part of zinc oxide of rice.
It is preferred that, the diatom ooze ornament materials includes the raw material of following parts by weight：40 parts of diatomite, 11 parts of bentonite,
16 parts of calcined kaolin, 5 parts of modified Nano bamboo charcoal powder, 10 parts of mica powder, 8 parts of titanium dioxide, hydroxypropyl methyl cellulose ether 1.4
Part, 3.9 parts of anti-crack fiber, 7 parts of graphene oxide, 2.8 parts of tourmaline powder anionic additive, 9 parts of modifying agent, 2 parts of dispersant,
10 parts of inorganic binder, catalyst 1.2 parts of nano zine oxide of level.
It is preferred that, the anti-crack fiber is any of polypropylene fibre, wood-fibred, carbon fiber or a variety of mixing
Thing.
It is preferred that, the preparation method of the modified Nano bamboo charcoal powder is as follows：Bamboo charcoal is put into glacial acetic acid solution and soaks 4
After~5 hours, take out washing, calcined 4~6 hours then at 400~450 DEG C, then grind to form nanometer powder produce it is described
Modified Nano bamboo charcoal powder.
It is preferred that, the tourmaline anion additive is made by following methods：Selection is electric with negative ion effect
Stone, carries out attrition grinding, is then dispersed in water miberal powder, wet grinding, with 1000 mesh filter-cloth filterings, and filtration is expected after drying,
The tourmaline anion additive is made.
It is preferred that, the dispersant be any of cellulose derivative, polyacrylamide, polyethoxy alkylphenol or
The a variety of mixture of person.
It is preferred that, the modifying agent is polyethylene glycol.
A kind of method for preparing the diatom ooze ornament materials, comprises the following steps：
（1）By above-mentioned formula weigh diatomite, bentonite, calcined kaolin, modified Nano bamboo charcoal powder, mica powder, titanium dioxide,
Hydroxypropyl methyl cellulose ether, anti-crack fiber, graphene oxide, tourmaline powder anionic additive, modifying agent, dispersant, nothing
Machine binding agent, catalyst level nano zine oxide, it is standby；
（2）Diatomite is first placed in microwave environment and shakes washing, then calcined 10~20 hours under the conditions of being placed in 400~600 DEG C,
Then it is mixed evenly with modifying agent, is first placed in closed container and stands 20~30 hours, then be placed in 50~60 DEG C of environment
Middle roasting 30~50 minutes, is washed with water unnecessary modifying agent, dries, and grinding crosses 1000~2000 mesh sieves, obtains being modified diatom
Soil；
（3）Bentonite and calcined kaolin and mica powder are respectively placed in grinder and ground, 1000~2000 mesh sieves are crossed, then
It is placed in high speed dispersor, adds dispersant and modified Nano bamboo charcoal powder, it is scattered 20~30 minutes at a high speed, obtain mixed material A；
（4）Titanium dioxide, hydroxypropyl methyl cellulose ether, anti-crack fiber and graphene oxide are added in modification infusorial earth,
It is placed in high-speed mixer, mixing obtains mixed material B in 5~10 minutes under 800~1000 revs/min of speed；
（5）Mixed material A, mixed material B and inorganic binder, catalyst level nano zine oxide are mixed evenly, Ran Houchao
Sound is scattered 5~10 minutes, obtains the diatom ooze ornament materials.
Compared with prior art, it has the advantages that the present invention：
Diatom ooze ornament materials of the present invention have Diamond Search, heatproof fire prevention, it is wear-resistant, with respiratory function, first can be adsorbed
A variety of functions such as the organic matter of aldehyde, toluene etc, performance is stable, and Acceptable life is long, specific as follows：
（1）Diatom ooze ornament materials addition calcined kaolin of the present invention is as raw material, and the kaolin after calcining has white
Degree is high, matter is soft, it is easily scattered suspend in water, good plasticity and high caking property, excellent electrical insulation capability, effectively improve
The caking property and insulating properties of the diatom ooze ornament materials, at the same the kaolin after calcining have good antiacid dissolubility,
The physicochemical properties such as very low cation exchange capacity (CEC), preferable fire resistance, improve the heatproof fire prevention of the diatom ooze ornament materials
Performance；
（2）Diatom ooze ornament materials of the present invention with the addition of diatomite, tourmaline powder anionic additive and catalyst level and receive
Rice zinc oxide is as raw material, and diatomite is the porous material of self-assembling formation, and silicon is further increased by the method for chemical reaction
The number of the nanoaperture of diatomaceous earth, and add diatomaceous specific surface area so that the diatom ooze ornament materials adsorbs first
The ability of aldehyde is greatly improved, while with the addition of tourmaline powder anionic additive and catalyst level nano zine oxide, improves institute
State the antibacterial ability of diatom ooze ornament materials；
（3）Diatom ooze ornament materials of the present invention with the addition of bentonite and anti-crack fiber as raw material, effectively improve its resistance to
Mill property；
（4）Mutually acted synergistically between the raw material that diatom ooze ornament materials of the present invention is used, the diatom ooze prepared
Ornament materials Diamond Search, green non-pollution.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1
The present embodiment is related to a kind of diatom ooze ornament materials, includes the raw material of following parts by weight：30 parts of diatomite, 7 parts of bentonite,
10 parts of calcined kaolin, 3 parts of modified Nano bamboo charcoal powder, 6 parts of mica powder, 5 parts of titanium dioxide, 1 part of hydroxypropyl methyl cellulose ether,
It is 3 parts of anti-crack fiber, 4 parts of graphene oxide, 2 parts of tourmaline powder anionic additive, 7 parts of modifying agent, 1.5 parts of dispersant, inorganic
6 parts of binding agent, catalyst 0.5 part of nano zine oxide of level.
Wherein, the anti-crack fiber is polypropylene fibre.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows：Bamboo charcoal is put into immersion 4 in glacial acetic acid solution small
Shi Hou, takes out washing, is calcined 4 hours then at 400 DEG C, then grinds to form nanometer powder and produce the modified Nano bamboo charcoal powder.
Wherein, the tourmaline anion additive is made by following methods：Tourmaline of the selection with negative ion effect,
Attrition grinding is carried out, is then dispersed in water miberal powder, wet grinding, with 1000 mesh filter-cloth filterings, after filtration material is dried, is made
The tourmaline anion additive.
Wherein, the dispersant is cellulose derivative.
Wherein, the modifying agent is polyethylene glycol.
A kind of method for preparing the diatom ooze ornament materials, comprises the following steps：
（1）By above-mentioned formula weigh diatomite, bentonite, calcined kaolin, modified Nano bamboo charcoal powder, mica powder, titanium dioxide,
Hydroxypropyl methyl cellulose ether, anti-crack fiber, graphene oxide, tourmaline powder anionic additive, modifying agent, dispersant, nothing
Machine binding agent, catalyst level nano zine oxide, it is standby；
（2）Diatomite is first placed in microwave environment and shakes washing, then calcine 10 hours under the conditions of being placed in 400 DEG C, then and changed
Property agent be mixed evenly, be first placed in closed container stand 20 hours, then be placed in 50 DEG C of environment be calcined 30 minutes, use water
Unnecessary modifying agent is washed away, is dried, grinding crosses 1000~2000 mesh sieves, obtains modification infusorial earth；
（3）Bentonite and calcined kaolin and mica powder are respectively placed in grinder and ground, 1000~2000 mesh sieves are crossed, then
It is placed in high speed dispersor, adds dispersant and modified Nano bamboo charcoal powder, it is scattered 20 minutes at a high speed, obtain mixed material A；
（4）Titanium dioxide, hydroxypropyl methyl cellulose ether, anti-crack fiber and graphene oxide are added in modification infusorial earth,
It is placed in high-speed mixer, mixing obtains mixed material B in 5 minutes under 800 revs/min of speed；
（5）Mixed material A, mixed material B and inorganic binder, catalyst level nano zine oxide are mixed evenly, Ran Houchao
Sound is scattered 5 minutes, obtains the diatom ooze ornament materials.
Embodiment 2
The present embodiment is related to a kind of diatom ooze ornament materials, includes the raw material of following parts by weight：50 parts of diatomite, bentonite 13
Part, 20 parts of calcined kaolin, 8 parts of modified Nano bamboo charcoal powder, 14 parts of mica powder, 10 parts of titanium dioxide, hydroxypropyl methyl cellulose
2 parts of ether, 5 parts of anti-crack fiber, 9 parts of graphene oxide, 3 parts of tourmaline powder anionic additive, 11 parts of modifying agent, dispersant 2.5
Part, 13 parts of inorganic binder, catalyst 1.5 parts of nano zine oxide of level.
Wherein, the anti-crack fiber is wood-fibred.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows：Bamboo charcoal is put into immersion 5 in glacial acetic acid solution small
Shi Hou, takes out washing, is calcined 6 hours then at 450 DEG C, then grinds to form nanometer powder and produce the modified Nano bamboo charcoal powder.
Wherein, the tourmaline anion additive is made by following methods：Tourmaline of the selection with negative ion effect,
Attrition grinding is carried out, is then dispersed in water miberal powder, wet grinding, with 1000 mesh filter-cloth filterings, after filtration material is dried, is made
The tourmaline anion additive.
Wherein, the dispersant is polyacrylamide.
Wherein, the modifying agent is polyethylene glycol.
A kind of method for preparing the diatom ooze ornament materials, comprises the following steps：
（1）By above-mentioned formula weigh diatomite, bentonite, calcined kaolin, modified Nano bamboo charcoal powder, mica powder, titanium dioxide,
Hydroxypropyl methyl cellulose ether, anti-crack fiber, graphene oxide, tourmaline powder anionic additive, modifying agent, dispersant, nothing
Machine binding agent, catalyst level nano zine oxide, it is standby；
（2）Diatomite is first placed in microwave environment and shakes washing, then calcine 20 hours under the conditions of being placed in 600 DEG C, then and changed
Property agent be mixed evenly, be first placed in closed container stand 30 hours, then be placed in 60 DEG C of environment be calcined 50 minutes, use water
Unnecessary modifying agent is washed away, is dried, grinding crosses 1000~2000 mesh sieves, obtains modification infusorial earth；
（3）Bentonite and calcined kaolin and mica powder are respectively placed in grinder and ground, 1000~2000 mesh sieves are crossed, then
It is placed in high speed dispersor, adds dispersant and modified Nano bamboo charcoal powder, it is scattered 30 minutes at a high speed, obtain mixed material A；
（4）Titanium dioxide, hydroxypropyl methyl cellulose ether, anti-crack fiber and graphene oxide are added in modification infusorial earth,
It is placed in high-speed mixer, mixing obtains mixed material B in 10 minutes under 1000 revs/min of speed；
（5）Mixed material A, mixed material B and inorganic binder, catalyst level nano zine oxide are mixed evenly, Ran Houchao
Sound is scattered 5~10 minutes, obtains the diatom ooze ornament materials.
Embodiment 3
The present embodiment is related to a kind of diatom ooze ornament materials, includes the raw material of following parts by weight：35 parts of diatomite, 9 parts of bentonite,
13 parts of calcined kaolin, 4 parts of modified Nano bamboo charcoal powder, 8 parts of mica powder, 7 parts of titanium dioxide, hydroxypropyl methyl cellulose ether 1.3
Part, 3.2 parts of anti-crack fiber, 6 parts of graphene oxide, 2.4 parts of tourmaline powder anionic additive, 8 parts of modifying agent, dispersant 1.7
Part, 8 parts of inorganic binder, catalyst 0.9 part of nano zine oxide of level.
Wherein, the anti-crack fiber is carbon fiber.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows：Bamboo charcoal is put into glacial acetic acid solution and soaks 4.5
After hour, washing is taken out, is calcined 5 hours then at 430 DEG C, is then ground to form nanometer powder and produce the modified Nano bamboo charcoal
Powder.
Wherein, the tourmaline anion additive is made by following methods：Tourmaline of the selection with negative ion effect,
Attrition grinding is carried out, is then dispersed in water miberal powder, wet grinding, with 1000 mesh filter-cloth filterings, after filtration material is dried, is made
The tourmaline anion additive.
Wherein, the dispersant is polyethoxy alkylphenol.
Wherein, the modifying agent is polyethylene glycol.
A kind of method for preparing the diatom ooze ornament materials, comprises the following steps：
（1）By above-mentioned formula weigh diatomite, bentonite, calcined kaolin, modified Nano bamboo charcoal powder, mica powder, titanium dioxide,
Hydroxypropyl methyl cellulose ether, anti-crack fiber, graphene oxide, tourmaline powder anionic additive, modifying agent, dispersant, nothing
Machine binding agent, catalyst level nano zine oxide, it is standby；
（2）Diatomite is first placed in microwave environment and shakes washing, then calcine 12 hours under the conditions of being placed in 450 DEG C, then and changed
Property agent be mixed evenly, be first placed in closed container stand 23 hours, then be placed in 52 DEG C of environment be calcined 35 minutes, use water
Unnecessary modifying agent is washed away, is dried, grinding crosses 1000~2000 mesh sieves, obtains modification infusorial earth；
（3）Bentonite and calcined kaolin and mica powder are respectively placed in grinder and ground, 1000~2000 mesh sieves are crossed, then
It is placed in high speed dispersor, adds dispersant and modified Nano bamboo charcoal powder, it is scattered 22 minutes at a high speed, obtain mixed material A；
（4）Titanium dioxide, hydroxypropyl methyl cellulose ether, anti-crack fiber and graphene oxide are added in modification infusorial earth,
It is placed in high-speed mixer, mixing obtains mixed material B in 6 minutes under 850 revs/min of speed；
（5）Mixed material A, mixed material B and inorganic binder, catalyst level nano zine oxide are mixed evenly, Ran Houchao
Sound is scattered 6 minutes, obtains the diatom ooze ornament materials.
Embodiment 4
The present embodiment is related to a kind of diatom ooze ornament materials, includes the raw material of following parts by weight：45 parts of diatomite, bentonite 12
Part, 18 parts of calcined kaolin, 7 parts of modified Nano bamboo charcoal powder, 12 parts of mica powder, 9 parts of titanium dioxide, hydroxypropyl methyl cellulose ether
1.8 parts, 4.6 parts of anti-crack fiber, 8 parts of graphene oxide, 2.9 parts of tourmaline powder anionic additive, 10 parts of modifying agent, dispersant
2.2 parts, 12 parts of inorganic binder, catalyst level 1.4 parts of nano zine oxide.
Wherein, the anti-crack fiber is polypropylene fibre, the mixture of wood-fibred.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows：Bamboo charcoal is put into glacial acetic acid solution and soaks 4.5
After hour, washing is taken out, is calcined 5 hours then at 420 DEG C, is then ground to form nanometer powder and produce the modified Nano bamboo charcoal
Powder.
Wherein, the tourmaline anion additive is made by following methods：Tourmaline of the selection with negative ion effect,
Attrition grinding is carried out, is then dispersed in water miberal powder, wet grinding, with 1000 mesh filter-cloth filterings, after filtration material is dried, is made
The tourmaline anion additive.
Wherein, the dispersant is cellulose derivative, polyacrylamide, the mixture of polyethoxy alkylphenol.
Wherein, the modifying agent is polyethylene glycol.
A kind of method for preparing the diatom ooze ornament materials, comprises the following steps：
（1）By above-mentioned formula weigh diatomite, bentonite, calcined kaolin, modified Nano bamboo charcoal powder, mica powder, titanium dioxide,
Hydroxypropyl methyl cellulose ether, anti-crack fiber, graphene oxide, tourmaline powder anionic additive, modifying agent, dispersant, nothing
Machine binding agent, catalyst level nano zine oxide, it is standby；
（2）Diatomite is first placed in microwave environment and shakes washing, then calcine 18 hours under the conditions of being placed in 550 DEG C, then and changed
Property agent be mixed evenly, be first placed in closed container stand 27 hours, then be placed in 58 DEG C of environment be calcined 45 minutes, use water
Unnecessary modifying agent is washed away, is dried, grinding crosses 1000~2000 mesh sieves, obtains modification infusorial earth；
（3）Bentonite and calcined kaolin and mica powder are respectively placed in grinder and ground, 1000~2000 mesh sieves are crossed, then
It is placed in high speed dispersor, adds dispersant and modified Nano bamboo charcoal powder, it is scattered 29 minutes at a high speed, obtain mixed material A；
（4）Titanium dioxide, hydroxypropyl methyl cellulose ether, anti-crack fiber and graphene oxide are added in modification infusorial earth,
It is placed in high-speed mixer, mixing obtains mixed material B in 9 minutes under 950 revs/min of speed；
（5）Mixed material A, mixed material B and inorganic binder, catalyst level nano zine oxide are mixed evenly, Ran Houchao
Sound is scattered 9 minutes, obtains the diatom ooze ornament materials.
Embodiment 5
The present embodiment is related to a kind of diatom ooze ornament materials, includes the raw material of following parts by weight：40 parts of diatomite, bentonite 11
Part, 16 parts of calcined kaolin, 5 parts of modified Nano bamboo charcoal powder, 10 parts of mica powder, 8 parts of titanium dioxide, hydroxypropyl methyl cellulose ether
1.4 parts, 3.9 parts of anti-crack fiber, 7 parts of graphene oxide, 2.8 parts of tourmaline powder anionic additive, 9 parts of modifying agent, dispersant 2
Part, 10 parts of inorganic binder, catalyst 1.2 parts of nano zine oxide of level.
Wherein, the anti-crack fiber is polypropylene fibre, wood-fibred, the mixture of carbon fiber.
Wherein, the preparation method of the modified Nano bamboo charcoal powder is as follows：Bamboo charcoal is put into glacial acetic acid solution and soaks 4.5
After hour, washing is taken out, is calcined 4.5 hours then at 410 DEG C, is then ground to form nanometer powder and produce the modified Nano bamboo charcoal
Powder.
Wherein, the tourmaline anion additive is made by following methods：Tourmaline of the selection with negative ion effect,
Attrition grinding is carried out, is then dispersed in water miberal powder, wet grinding, with 1000 mesh filter-cloth filterings, after filtration material is dried, is made
The tourmaline anion additive.
Wherein, the dispersant is cellulose derivative, polyacrylamide, the mixture of polyethoxy alkylphenol.
Wherein, the modifying agent is polyethylene glycol.
A kind of method for preparing the diatom ooze ornament materials, comprises the following steps：
（1）By above-mentioned formula weigh diatomite, bentonite, calcined kaolin, modified Nano bamboo charcoal powder, mica powder, titanium dioxide,
Hydroxypropyl methyl cellulose ether, anti-crack fiber, graphene oxide, tourmaline powder anionic additive, modifying agent, dispersant, nothing
Machine binding agent, catalyst level nano zine oxide, it is standby；
（2）Diatomite is first placed in microwave environment and shakes washing, then calcine 15 hours under the conditions of being placed in 500 DEG C, then and changed
Property agent be mixed evenly, be first placed in closed container stand 25 hours, then be placed in 55 DEG C of environment be calcined 40 minutes, use water
Unnecessary modifying agent is washed away, is dried, grinding crosses 1000~2000 mesh sieves, obtains modification infusorial earth；
（3）Bentonite and calcined kaolin and mica powder are respectively placed in grinder and ground, 1000~2000 mesh sieves are crossed, then
It is placed in high speed dispersor, adds dispersant and modified Nano bamboo charcoal powder, it is scattered 25 minutes at a high speed, obtain mixed material A；
（4）Titanium dioxide, hydroxypropyl methyl cellulose ether, anti-crack fiber and graphene oxide are added in modification infusorial earth,
It is placed in high-speed mixer, mixing obtains mixed material B in 7 minutes under 900 revs/min of speed；
（5）Mixed material A, mixed material B and inorganic binder, catalyst level nano zine oxide are mixed evenly, Ran Houchao
Sound is scattered 7 minutes, obtains the diatom ooze ornament materials.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (9)
1. a kind of diatom ooze ornament materials, it is characterised in that include the raw material of following parts by weight：30~50 parts of diatomite, swelling
7~13 parts of soil, 10~20 parts of calcined kaolin, 3~8 parts of modified Nano bamboo charcoal powder, 6~14 parts of mica powder, titanium dioxide 5~10
Part, 1~2 part of hydroxypropyl methyl cellulose ether, 3~5 parts of anti-crack fiber, 4~9 parts of graphene oxide, tourmaline powder anion add
Plus 2~3 parts of agent, 7~11 parts of modifying agent, 1.5~2.5 parts of dispersant, 6~13 parts of inorganic binder, catalyst level nano zine oxide
0.5~1.5 part.
2. diatom ooze ornament materials according to claim 1, it is characterised in that include the raw material of following parts by weight：Diatom
35~45 parts of soil, 9~12 parts of bentonite, 13~18 parts of calcined kaolin, 4~7 parts of modified Nano bamboo charcoal powder, mica powder 8~12
Part, 7~9 parts of titanium dioxide, 1.3~1.8 parts of hydroxypropyl methyl cellulose ether, 3.2~4.6 parts of anti-crack fiber, graphene oxide 6
~8 parts, 2.4~2.9 parts of tourmaline powder anionic additive, 8~10 parts of modifying agent, 1.7~2.2 parts of dispersant, inorganic bond
8~12 parts of agent, catalyst 0.9~1.4 part of nano zine oxide of level.
3. diatom ooze ornament materials according to claim 1, it is characterised in that include the raw material of following parts by weight：Diatom
40 parts of soil, 11 parts of bentonite, 16 parts of calcined kaolin, 5 parts of modified Nano bamboo charcoal powder, 10 parts of mica powder, 8 parts of titanium dioxide, hydroxyl
1.4 parts of propyl methocel ether, 3.9 parts of anti-crack fiber, 7 parts of graphene oxide, 2.8 parts of tourmaline powder anionic additive,
9 parts of modifying agent, 2 parts of dispersant, 10 parts of inorganic binder, catalyst 1.2 parts of nano zine oxide of level.
4. diatom ooze ornament materials according to claim 1, it is characterised in that the anti-crack fiber be polypropylene fibre,
Any of wood-fibred, carbon fiber or a variety of mixtures.
5. diatom ooze ornament materials according to claim 1, it is characterised in that the preparation side of the modified Nano bamboo charcoal powder
Method is as follows：Bamboo charcoal is put into after being soaked 4~5 hours in glacial acetic acid solution, takes out washing, then at 400~450 DEG C of calcinings 4
~6 hours, then grind to form nanometer powder and produce the modified Nano bamboo charcoal powder.
6. diatom ooze ornament materials according to claim 1, it is characterised in that the tourmaline anion additive by with
Lower section method is made：Tourmaline of the selection with negative ion effect, carries out attrition grinding, is then dispersed in water miberal powder, wet method
Grinding, with 1000 mesh filter-cloth filterings, after filtration material is dried, is made the tourmaline anion additive.
7. diatom ooze ornament materials according to claim 1, it is characterised in that the dispersant be cellulose derivative,
Any of polyacrylamide, polyethoxy alkylphenol or a variety of mixtures.
8. diatom ooze ornament materials according to claim 1, it is characterised in that the modifying agent is polyethylene glycol.
9. a kind of method for preparing any one of the claim 1~8 diatom ooze ornament materials, it is characterised in that including as follows
Step：
（1）By above-mentioned formula weigh diatomite, bentonite, calcined kaolin, modified Nano bamboo charcoal powder, mica powder, titanium dioxide,
Hydroxypropyl methyl cellulose ether, anti-crack fiber, graphene oxide, tourmaline powder anionic additive, modifying agent, dispersant, nothing
Machine binding agent, catalyst level nano zine oxide, it is standby；
（2）Diatomite is first placed in microwave environment and shakes washing, then calcined 10~20 hours under the conditions of being placed in 400~600 DEG C,
Then it is mixed evenly with modifying agent, is first placed in closed container and stands 20~30 hours, then be placed in 50~60 DEG C of environment
Middle roasting 30~50 minutes, is washed with water unnecessary modifying agent, dries, and grinding crosses 1000~2000 mesh sieves, obtains being modified diatom
Soil；
（3）Bentonite and calcined kaolin and mica powder are respectively placed in grinder and ground, 1000~2000 mesh sieves are crossed, then
It is placed in high speed dispersor, adds dispersant and modified Nano bamboo charcoal powder, it is scattered 20~30 minutes at a high speed, obtain mixed material A；
（4）Titanium dioxide, hydroxypropyl methyl cellulose ether, anti-crack fiber and graphene oxide are added in modification infusorial earth,
It is placed in high-speed mixer, mixing obtains mixed material B in 5~10 minutes under 800~1000 revs/min of speed；
（5）Mixed material A, mixed material B and inorganic binder, catalyst level nano zine oxide are mixed evenly, Ran Houchao
Sound is scattered 5~10 minutes, obtains the diatom ooze ornament materials.
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