CN107156407A - A kind of threeleaf akebia pressed candy and preparation method thereof - Google Patents

Abstract

The invention belongs to the field of food technology, and in particular relates to a pressed Akebia candy and a preparation method thereof. Akebia clover candy is composed of aketo hydrolyzate, calcium D-pantothenate, β-carotene, seaweed powder, docosahexaenoic acid, calcium saccharin, black safflower extract, calcium sorbate, rutin, Composition of pregelatinized starch, hypromellose, cross-linked polyvinylpyrrolidone, magnesium stearate, purified water, and ethanol. In the hydrolysis of Akebia clover, the present invention decomposes the macromolecular protein in the pulp of Akebia clover into small molecular amino acids, which is beneficial for human body to absorb; no components harmful to the human body are introduced during the hydrolysis of Akebia clover, and the hydrolyzate is directly spray-dried, and the maximum The beneficial ingredients in the pulp of Akebia clover are retained to the maximum extent.

Description

A kind of Sanye Akebia compressed tablet candy and preparation method thereof

technical field

The invention belongs to the field of food technology, and in particular relates to a pressed Akebia candy and a preparation method thereof.

Background technique

Compared with traditional candies, plant-pressed candies add medicinal and edible plants or plant extracts as raw materials. Through reasonable formula combination, they have certain health care and beauty effects, and plant-pressed candies have a pleasant flavor and are portable. , easy to eat and other features, you can enjoy a lazy and beautiful health care mode anytime, anywhere.

Akebia trifoliate is an important medicinal plant, its roots, vines, fruits and seeds can be used as medicine. The pulp of Akebia clover is rich in nutrients, rich in protein, fat, starch and various soluble sugars, calcium, phosphorus, iron, organic acids, vitamins B1, BZ, B6, etc. It can be eaten fresh, brewed, and made into beverages. Akebia seeds are rich in oils and fats, with high nutritional value, good medicinal value, and ornamental value.

At present, the extraction and processing of the effective components of Akebia trifoliata has been extensively studied. CN 104068137 A discloses a kind of edible oil made from the seeds of Akebia trifoliata and its preparation method. The seeds of the fresh fruit of Akebia trifoliata are used, and the seeds are fried, crushed, Steaming base, tempering, pressing on cakes, and pressing, the oil color is light yellow, translucent, and edible oil with strong aroma; "Food Research and Development" 2016, 37 (19): 100-104 pages disclose The processing technology of making preserved fruit through the peel, adopts blanching, color protection, bitterness removal, sugaring, and drying processes to make the finished product with golden color, sweet and sour taste, and good plumpness.

Akebia clover belongs to the deciduous woody vine of Akebia genus. The fruit skin is thick, the seeds are many, and the edible rate is low. The fresh peel accounts for 69.1% of the total fruit weight. Therefore, it is of great significance to develop beneficial components in the peel of Akebia clover. "Anhui Agricultural Science" 2007,35(16):4757-4759 discloses the research of extracting pectin from the peel of Akebia trifoliata by acid hydrolysis, and 2008,29, (01):154-17 of "Food Science" also discloses Aketobia peel pectin extraction process research, but in the above-mentioned Akebia trifoliate pectin extraction process, all adopt inorganic acid such as hydrochloric acid, sulfuric acid, nitric acid etc. to carry out acidolysis and extraction, but too much sulfuric acid will produce a large amount of acid waste water, not It is beneficial to environmental protection; and during acid extraction, the raw materials are smashed and heated to form a viscous paste, which makes it difficult to filter the extract and is easy to corrode the equipment.

There is no literature report on the compressed candy prepared with the extract of Akebia trifoliata.

Contents of the invention

The object of the present invention is to provide a kind of Akebia compressed candy and its preparation method. The Akebia compressed candy prepared by the present invention is rich in protein, fat, starch and various soluble sugars, calcium, phosphorus, iron, organic Nutrients such as acid, vitamin B1, vitamin B2, and vitamin B6 have physiological effects such as soothing the liver and strengthening the spleen, harmonizing the stomach, promoting body fluid and quenching thirst, relaxing tendons and activating collaterals, and anti-cancer.

According to one aspect of the present invention, the present invention provides a kind of Akebia clover compressed tablet candy, which consists of the following ingredients in parts by weight:

15-16 parts by weight of akebia hydrolyzate; 18-19 parts by weight of D-calcium pantothenate; 7-9 parts by weight of β-carotene; 11-13 parts by weight of seaweed powder; 4-6 parts by weight of docosahexaene acid; 15-17 parts by weight of calcium saccharin; 7-9 parts by weight of black safflower extract; 4-6 parts by weight of calcium sorbate; 2-3 parts by weight of rutin; 18-19 parts by weight of pregelatinized starch; 21- 22 parts by weight of hypromellose; 11-13 parts by weight of cross-linked polyvinylpyrrolidone; 4-6 parts by weight of magnesium stearate; 23-24 parts by weight of purified water; 3-5 parts by weight of ethanol;

The extraction process of the hydrolyzate of Akebia trifoliata, comprises the following steps:

1) Wash the akebia fruit with deionized water, then beat the pulp, filter through a microporous membrane with a pore size of 0.5 microns, filter out impurities and aketo seeds to obtain aketo juice, add hydrochloric acid to adjust the pH of the akebia juice 4.0-4.5 to get acidic akebia juice;

2) Add amylase, pectinase, cellulase, lactobacillus and gibberellic acid to acid akebia fruit juice and ferment at 15-20°C in the dark for one week to obtain a fermentation broth; calculated based on the volume of acid akebia juice, The dosages of amylase, pectinase, cellulase, lactobacillus and gibberellic acid are 0.3g/L, 0.4g/L, 3.1g/L, 0.2g/L, 0.6g/L respectively;

3) Use magnesium carbonate to adjust the pH of the fermentation broth to 6.0-6.5, and then concentrate at low temperature; the volume after concentration is half of that before concentration;

4) The concentrated fermented liquid is spray-dried to obtain Akebia trifoliate hydrolyzate.

In the present invention, amylase, pectinase, cellulase and lactobacillus are used as fermentation agents in the processing process of Akebia clover fruit, and gibberellic acid is used as an enzyme activator to ferment and decompose Akebia clover fruit juice, and three The macromolecular protein in the Akebia fruit juice is decomposed into small molecule amino acids, which is beneficial to human body absorption; in order to ensure the activity of the enzyme, the present invention uses hydrochloric acid to adjust the pH of the Akebia fruit juice to acidity before fermentation, which fully ensures the activity of the enzyme; In order to retain all the beneficial components of Akebia to the greatest extent, after the fermentation is finished, adjust the pH of the fermented liquid, concentrate the fermented liquid, and then spray dry it to obtain the hydrolyzate of Akebia clover, and retain all the components after fermentation.

According to the present invention, the Akebia compressed tablet candy is preferably further technically prepared as follows:

16 parts by weight of Akebia hydrolyzate; 19 parts by weight of D-calcium pantothenate; 8 parts by weight of beta-carotene; 12 parts by weight of seaweed powder; 5 parts by weight of docosahexaenoic acid; 16 parts by weight of calcium saccharin; 8 parts by weight 5 parts by weight of calcium sorbate; 3 parts by weight of rutin; 19 parts by weight of pregelatinized starch; 22 parts by weight of hypromellose; 12 parts by weight of cross-linked polyvinylpyrrolidone; Magnesium fatty acid; 24 parts by weight of purified water; 4 parts by weight of ethanol;

According to another aspect of the present invention, the present invention provides a kind of preparation method of Akebia japonicus compressed tablet candy, comprising the following steps:

1) Akebia trifoliate hydrolyzate, calcium D-pantothenate, β-carotene, seaweed powder, and calcium saccharin were crushed, sieved, and then mixed to obtain the first mixture;

2) Add rutin, black safflower extract, and docosahexaenoic acid to the first mixture for 20-30 minutes, then add calcium sorbate, pregelatinized starch and purified water for mixing to obtain wetting The second mixture of the second mixture; in the process of making the second mixture, if the materials are not premixed, the second mixture obtained is easy to form balls, the materials are not uniform, and there is sticking phenomenon in the subsequent tableting process;

3) Sieving the second mixture to obtain wet granules, drying the wet granules by a fluidized bed dryer to obtain second mixture granules, and then granulating the second mixture granules with a swinging granulator, After processing, the third mixture is obtained;

4) Mechanically mix the third mixture with hypromellose, cross-linked polyvinylpyrrolidone, and magnesium stearate, then add ethanol and ultrasonically mix it evenly, and finally press it through a tablet machine to obtain Akebia candy .

The preparation method of the Akebia trifoliate compressed candy of the present invention, its further technical solution is that the aperture of the sieve plate for sieving described in step 1) is 200 mesh;

The further technical scheme of the preparation method of Akebia clover tablet candy of the present invention is that the drying temperature in step 3) is 45-50°C, and the drying is carried out until the moisture content is 1.0-2.0wt%; the moisture content after drying is greater than 3.0 Wt% will cause the material to agglomerate during the granulation process of the swinging granulator in the later stage, making it difficult to process; when the moisture content is lower than 0.5wt%, the prepared Akebia candy is prone to splitting in a humid environment .

Compared with prior art, the present invention has following advantage:

1) The present invention provides a kind of Akebia clover tablet candy, because the akebia clover in the candy is rich in a large amount of beneficial substances, so the prepared candy has the functions of soothing the liver and invigorating the spleen, harmonizing the stomach and qi, promoting body fluid and quenching thirst, and relaxing tendons Physiological functions such as activating collaterals and anti-cancer;

2) The present invention decomposes the macromolecular protein in the pulp of Akebia clover into small molecule amino acids in the hydrolysis of Akebia clover, which is beneficial for human body to absorb;

3) The present invention does not introduce harmful components to the human body during the hydrolysis process of Akebia clover, directly sprays and dries the hydrolyzate, and retains the beneficial components in the pulp of Akebia clover to the greatest extent;

4) The Sanye Akebia compressed candy prepared by the present invention has no cracks, loose pieces and the like.

detailed description

In order to make the object, technical solution and advantages of the present invention clearer, the present invention will be further described in detail below in conjunction with specific embodiments. It should be understood that these descriptions are exemplary only, and are not intended to limit the scope of the present invention.

Example 1

1. Preparation of Akebia trifoliate hydrolyzate:

1) Wash the akebia fruit with deionized water, beat the pulp, filter through a microporous membrane with a pore size of 0.5 micron, filter out impurities and aketo seeds to obtain aketo juice, add hydrochloric acid to adjust the pH of the akebia juice 4.2 to get acid Akebia fruit juice;

2) Add amylase, pectinase, cellulase, lactobacillus and gibberellic acid to acid akebia fruit juice and ferment for one week in the dark at 15-20°C to obtain a fermentation liquid; calculated based on the volume of acid akebia juice, The dosages of amylase, pectinase, cellulase, lactobacillus and gibberellic acid are 0.3g/L, 0.4g/L, 3.1g/L, 0.2g/L, 0.6g/L respectively;

3) Use magnesium carbonate to adjust the pH of the fermentation broth to 6.3, and then concentrate at 45°C; the volume after concentration is half of that before concentration;

4) The concentrated fermented liquid is spray-dried by a spray dryer to obtain Akebia trifoliate hydrolyzate. The air inlet temperature of the spray dryer is 260°C, and the outlet air temperature of the spray dryer is 85°C.

2. Preparation of Akebia Tablet Candy

1) Grind 15 parts by weight of Akebia trifoliate hydrolyzate, 18 parts by weight of D-calcium pantothenate, 7 parts by weight of β-carotene, 11 parts by weight of seaweed powder, and 15 parts by weight of calcium saccharin, pass through a 200-mesh sieve, and then mix to obtain the first mixture;

2) Add 2 parts by weight of rutin, 7 parts by weight of Mosafflower extract, and 4 parts by weight of docosahexaenoic acid to the first mixture for premixing for 20-30 minutes, then add 4 parts by weight of calcium sorbate, 18 Parts by weight of pregelatinized starch and 23 parts by weight of purified water are mixed to obtain a moistened second mixture;

3) Sieve the second mixture to obtain wettable granules, and dry the wettable granules through a fluidized bed dryer to obtain the second mixture granules. The drying temperature is 45-50°C, and the moisture content is 1.0-2.0wt%; then the particles of the second mixture are granulated by a swinging granulator, and the third mixture is obtained after processing;

4) Mechanically mix the third mixture with 21 parts by weight of hypromellose, 11 parts by weight of cross-linked polyvinylpyrrolidone, and 4 parts by weight of magnesium stearate, then add 3 parts by weight of ethanol and ultrasonically mix them uniformly, and finally press Tablet machine is used for tableting to obtain Akebia shamrock tablet candy.

The weight of Sanye Ketong compressed tablet candy is 5.6g±0.1g.

Example 2

Akebia trifoliate hydrolyzate is the same as embodiment 1.

2. Preparation of Akebia Tablet Candy

1) 16 parts by weight of Akebia trifoliate hydrolyzate, 19 parts by weight of D-calcium pantothenate, 9 parts by weight of β-carotene, 13 parts by weight of seaweed powder, and 17 parts by weight of calcium saccharin were crushed and passed through a 200-mesh sieve, and then mixed to obtain the first mixture;

2) Add 3 parts by weight of rutin, 9 parts by weight of Mosafflower extract, and 6 parts by weight of docosahexaenoic acid to the first mixture for premixing for 20-30 minutes, then add 6 parts by weight of calcium sorbate, 19 Parts by weight of pregelatinized starch and 24 parts by weight of purified water are mixed to obtain a wetting second mixture;

3) Sieve the second mixture to obtain wettable granules, and dry the wettable granules through a fluidized bed dryer to obtain the second mixture granules. The drying temperature is 45-50°C, and the moisture content is 1.0-2.0wt%; then the particles of the second mixture are granulated by a swinging granulator, and the third mixture is obtained after processing;

4) Mechanically mix the third mixture with 22 parts by weight of hypromellose, 13 parts by weight of cross-linked polyvinylpyrrolidone, and 6 parts by weight of magnesium stearate, and then add 5 parts by weight of ethanol for ultrasonic mixing, and finally press Tablet machine is used for tableting to obtain Akebia shamrock tablet candy. The weight of Sanye Ketong compressed tablet candy is 5.6g±0.1g.

Example 3

Akebia trifoliate hydrolyzate is the same as embodiment 1.

2. Preparation of Akebia Tablet Candy

1) Grind 15 parts by weight of Akebia trifoliate hydrolyzate, 19 parts by weight of D-calcium pantothenate, 8 parts by weight of β-carotene, 12 parts by weight of seaweed powder, and 16 parts by weight of calcium saccharin, pass through a 200-mesh sieve, and then mix to obtain the first mixture;

2) Add 3 parts by weight of rutin, 8 parts by weight of Mosafflower extract, and 5 parts by weight of docosahexaenoic acid to the first mixture for premixing for 20-30 minutes, then add 5 parts by weight of calcium sorbate, 19 Parts by weight of pregelatinized starch and 23 parts by weight of purified water are mixed to obtain a moistened second mixture;

3) Sieve the second mixture to obtain wettable granules, and dry the wettable granules through a fluidized bed dryer to obtain the second mixture granules, the drying temperature is 45-50°C, and the moisture content is 1.0-2.0wt%; then the particles of the second mixture are granulated by a swinging granulator, and the third mixture is obtained after processing;

4) Mechanically mix the third mixture with 22 parts by weight of hypromellose, 12 parts by weight of cross-linked polyvinylpyrrolidone, and 5 parts by weight of magnesium stearate, and then add 4 parts by weight of ethanol for ultrasonic mixing, and finally press Tablet machine is used for tableting to obtain Akebia shamrock tablet candy. The weight of Sanye Ketong compressed tablet candy is 5.6g±0.1g.

Comparative example 1

Compared with embodiment 1, used raw material and proportioning thereof are all identical:

The only difference is that step 2) in the preparation process of Akebia pressed tablet candy is: add 2 parts by weight of rutin, 7 parts by weight of Mosafflower extract, 4 parts by weight of docosahexaenoic acid, 4 parts by weight to the first mixture Parts by weight of calcium sorbate, 18 parts by weight of pregelatinized starch and 23 parts by weight of purified water are mixed to obtain the second mixture of wetting;

The second mixture is in a spherical aggregation state, and there is a sticking phenomenon in the subsequent tableting process.

Comparative example 2

Compared with embodiment 1, used raw material and proportioning thereof are all identical:

The only difference is that step 3) in the preparation process of Sanye Ketong tablet candy is: sieve the second mixture to obtain wet granules, and dry the wet granules through a fluidized bed dryer to obtain the second mixture granules. The drying temperature is 45-50°C, and the moisture content is dried to 0.5wt%; then the particles of the second mixture are granulated by a swinging granulator, and the third mixture is obtained after the treatment;

Comparative example 3

Compared with embodiment 1, used raw material and proportioning thereof are all identical:

The only difference is that step 3) in the preparation process of Sanye Ketong tablet candy is: sieve the second mixture to obtain wet granules, and dry the wet granules through a fluidized bed dryer to obtain the second mixture granules. The drying temperature is 45-50°C, and the moisture content is 3.0wt% after drying; then, the particles of the second mixture are granulated by a swinging granulator, and the third mixture is obtained after the treatment;

The phenomenon of sticking and punching occurs in the subsequent tableting process.

Carry out the detection of loose slices and cracks (all taking 100 pieces for detection) of the Sanyeketo pressed candy prepared in Examples 1-3 and its comparative examples 1-3, wherein the inspection method of the loose slices is: put the Sanyekeke pressed candy in Between the middle finger and the index finger, use the thumb to gently press to see if it is broken; the inspection method for the lobes is: take 10 pieces of candy in the palm of your hand, and shake them vigorously with both hands; the results are shown in Table 1:

Table 1 Test results of Akebia clover candy loose slices and splits

Loose flakes rate/% Fragmentation rate/% Example 1 2 1 Example 2 1 1 Example 3 1 1 Comparative example 1 5 6 Comparative example 2 11 13 Comparative example 3 6 8

The above results show that the present invention strictly controls the premixing in the wetting process and controls the moisture in the fluidized bed drying process in the preparation process of the Akebia clover compressed tablet candy to solve the problem of loose flakes and splits.

Although the embodiments of the present invention have been described in detail, it should be understood that the various changes, substitutions and alterations could be made hereto without departing from the spirit and scope of the invention.

Claims (6)

1. a kind of threeleaf akebia pressed candy, it is characterised in that：Count, consist of the following composition by weight：

15-16 parts by weight threeleaf akebia hydrolysates；18-19 parts by weight D-VB5 calcium；7-9 parts by weight beta carotenes；11-13 weights Measure part seawood meal；4-6 parts by weight docosahexaenoic acids；15-17 parts by weight calcium benzosulphimides；7-9 parts by weight concretes of rose crimson glory；4-6 Parts by weight calcium sorbate；2-3 parts by weight rutins；18-19 parts by weight pregelatinized starch；21-22 parts by weight hydroxypropyl methylcelluloses； 11-13 parts by weight PVPPs；4-6 parts by weight magnesium stearates；23-24 parts by weight purified waters；3-5 parts by weight second Alcohol；

The extraction process of the threeleaf akebia hydrolysate, comprises the following steps：

1）Deionized water cleans threeleaf akebia fruit, is then beaten, and is 0.5 micrometer Millipore membrane filtration by aperture, filters out impurity And its Akebia trifoliata seed obtains threeleaf akebia fruit juice, the pH for adding hydrochloric acid regulation threeleaf akebia fruit juice obtains acid three leaf for 4.0-4.5 Akebi fruit juice；

2）Amylase, pectase, cellulase, Bacillus acidi lactici and gibberellic acid are added in oxytropism threeleaf akebia fruit juice in 15-20 Lucifuge, which is fermented one week, at DEG C obtains zymotic fluid；

3）Use the pH of magnesium carbonate regulation zymotic fluid for 6.0-6.5, then low temperature is concentrated, and volume is one before concentration after concentration Half；

4）Zymotic fluid after concentration carries out being spray-dried to obtain threeleaf akebia hydrolysate.

2. threeleaf akebia pressed candy according to claim 1, it is characterised in that：Count by weight, by following component Composition：16 parts by weight threeleaf akebia hydrolysates；19 parts by weight D-VB5 calcium；8 parts by weight β-carrotene；12 parts by weight marine algas Powder；5 parts by weight docosahexaenoic acids；16 parts by weight calcium benzosulphimides；8 parts by weight concretes of rose crimson glory；5 parts by weight calcium sorbates；3 weights Measure part rutin；19 parts by weight pregelatinized starch；22 parts by weight hydroxypropyl methylcelluloses；12 parts by weight PVPPs； 6 parts by weight magnesium stearates；24 parts by weight purified waters；4 parts by weight of ethanol.

3. threeleaf akebia pressed candy according to claim 1 or 2, it is characterised in that：The extraction of threeleaf akebia hydrolysate Processing step 2）In calculated with acid threeleaf akebia fruit juice volume, wherein amylase, pectase, cellulase, Bacillus acidi lactici, red Mould sour consumption is respectively 0.3g/L, 0.4g/L, 3.1g/L, 0.2g/L, 0.6g/L.

4. a kind of preparation method of threeleaf akebia pressed candy, it is characterised in that：Comprise the following steps：

By threeleaf akebia hydrolysate, D-VB5 calcium, beta carotene, seawood meal, calcium benzosulphimide grinding and sieving, then mix One mixture；

Rutin, concrete of rose crimson glory, docosahexaenoic acid are added into the first mixture and carries out premix 20-30min, is then added Calcium sorbate, pregelatinized starch and purified water are mixed, and obtain the second mixture of wetting；

Second mixture is carried out to sieve to obtain wettable particles, by fluidized bed dryer wettable particles are dried the Then second compound particles are carried out pelletization treatment by two compound particles using oscillating granulator, and the 3rd is obtained after processing and is mixed Compound；

By the 3rd mixture and hydroxypropyl methylcellulose, PVPP, magnesium stearate mechanical mixture it is uniform after, then Add EtOH Sonicate to be well mixed, eventually pass tablet press machine progress tabletting and obtain threeleaf akebia pressed candy.

5. preparation method according to claim 4, it is characterised in that：Step 1）Described sieving hole diameter of sieve (perforated) plate is 200 Mesh.

6. preparation method according to claim 4, it is characterised in that：Step 3）The temperature of described drying is 45-50 DEG C, It is 1.0-2.0wt% to dry to moisture.