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CN107021813A - A kind of late rice plantation herb fermenting organic slow-release fertilizer and preparation method thereof - Google Patents

A kind of late rice plantation herb fermenting organic slow-release fertilizer and preparation method thereof Download PDF

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Publication number
CN107021813A
CN107021813A CN201710244360.XA CN201710244360A CN107021813A CN 107021813 A CN107021813 A CN 107021813A CN 201710244360 A CN201710244360 A CN 201710244360A CN 107021813 A CN107021813 A CN 107021813A
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parts
herb fermenting
powder
late rice
sustained release
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高青山
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/02Superphosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/90Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/30Layered or coated, e.g. dust-preventing coatings
    • C05G5/36Layered or coated, e.g. dust-preventing coatings layered or coated with sulfur

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of late rice plantation herb fermenting organic slow-release fertilizer, its raw material includes human and animal excreta, stalk, flyash, soybean skin, oil cake, powdered rice hulls, bean dregs, bentonite in powder, daghestan sweet clover, pale reddish brown lucerne place, lignin, cocoa pod shell powder, illite powder, banana skin powder, calcium superphosphate, urea, potassium sulfate, potassium chloride, calcium magnesium phosphate, white clay, careless carbon, kaolin, gangue, quartz, coal slime, ammonium hydrogen carbonate, nitro humic acid, herb fermenting thing and modified sustained release agent.The invention also discloses a kind of above-mentioned preparation method of late rice plantation herb fermenting organic slow-release fertilizer.Organic slow-release fertilizer of the present invention is applied in late rice plantation, using the nutriment after herb fermenting, with closing organic material and inorganic material, and pass through sustained release agent coating, abundant nutriment is provided for the growth of late rice, and the release of nutriment is efficiently high-quality, effectively increases the yield and quality of late rice.

Description

A kind of late rice plantation herb fermenting organic slow-release fertilizer and preparation method thereof
Technical field
The present invention relates to the technical field of fertilizer, more particularly to a kind of plantation of late rice with herb fermenting organic slow-release fertilizer and its Preparation method.
Background technology
China is natural resources of Chinese medicinal materials consumption big country, thus also produces substantial amounts of Chinese medicine dreg, Chinese medicine dreg is mainly derived from respectively The process of class Chinese medicine production, wherein the dregs of a decoction remained in the production process of Chinese patent drug are at most, these dregs of a decoction are also just in One of pollution sources of most serious in medicine enterprise, if handled not in time, these dregs of a decoction will become morally degenerate, and distribute stench, grow Bacterium, the hotbed as multiple infectious disease, and traditional processing mode is stacked or buried to concentrate, and can not only take substantial amounts of soil Ground, produces substantial amounts of harmful corrupt gas, and also has pollution to underground water, if can be produced after being burned after Chinese medicine slag is dried big The pollutants such as flue dust, the carbon dioxide of amount, cause the pollution of atmospheric environment.
The active constituent content of Chinese medicine is often relatively low, and Chinese medicine will produce a large amount of dregs of a decoction after extracting and decocting, and the dregs of a decoction In there is typically further a variety of organic nutrients and a certain amount of active component, mainly including amino acid, crude protein, crude fibre, thick A variety of inorganic elements and a small amount of vitamin such as fat and nitrogen, phosphorus, potassium, silicon, zinc, chromium, magnesium, iron.
Current late rice plantation fertilizer type used is a lot, and wherein late rice special fertilizer is mostly using commercially available NPK composite fertilizers, it is mainly made up of the big inorganic elements of N, P, K tri-, and the growth needs of late rice can be met in a short time.But it is long-term Using that can be destroyed soil granular structure, easily cause soil hardening, soil property and be hardened, so as to influence late rice to grow, to late rice Growth-promoting effect is not obvious, though while simple organic fertilizer is rich in organic matter, nutrients release is slow, and late rice absorbs slow, fertilizer Effect is low, and the mirror of various available nutrients does not reach active balance, so it is organic slow to need a kind of late rice plantation herb fermenting of design badly Fertilizer is released to solve the problems of the prior art.
The content of the invention
To solve technical problem present in background technology, the present invention proposes that a kind of late rice plantation is organic slow with herb fermenting Fertilizer and preparation method thereof is released, the organic slow-release fertilizer prepared is applied in late rice plantation, utilizes the nutrients after herb fermenting Matter, with organic material and inorganic material, and process sustained release agent coating is closed, abundant nutriment is provided for the growth of late rice, and The release of nutriment is efficiently high-quality, effectively increases the yield and quality of late rice.
Herb fermenting organic slow-release fertilizer is used in a kind of late rice plantation proposed by the present invention, and its raw material includes by weight:People and animals 80-120 parts of excrement, 2-8 parts of stalk, 1-5 parts of flyash, 3-6 parts of soybean skin, 4-8 parts of oil cake, 1-8 parts of powdered rice hulls, bean dregs 2-8 Part, 2-6 parts of bentonite in powder, 1-5 parts of daghestan sweet clover, pale reddish brown lucerne place 2-6 parts, 3-9 parts of lignin, 4-8 parts of cocoa pod shell powder, illite 2-5 parts of powder, 4-5 parts of banana skin powder, 2-6 parts of calcium superphosphate, 4-8 parts of urea, 1-4 parts of potassium sulfate, 2-6 parts of potassium chloride, calcium and magnesium phosphorus Fertile 3-9 parts, 1-5 parts of white clay, careless 3-8 parts of carbon, 1-5 parts of kaolin, 1-6 parts of gangue, 2-8 parts of quartz, 3-9 parts of coal slime, carbonic acid 4-8 parts of hydrogen ammonium, 1-5 parts of nitro humic acid, 4-12 parts of herb fermenting thing, modified 10-20 parts of sustained release agent.
Preferably, herb fermenting thing is prepared by following technique:By Echinacea, red clover, the red sage root, Radix Angelicae Sinensis, radix scutellariae, The fruit of Chinese magnoliavine, ganoderma lucidum, giant knotweed and the fruit of glossy privet are well mixed after crushing and obtain material a, then mix material a, cellulase and water, 35-45 DEG C of enzymolysis 2-5h obtains material b, and material b then is filtered to take into filtrate, then arrives material c by what filtrate concentrated, then will Material c is mixed with fermented bacterium, and the 5-10d that fermented in 55-65 DEG C obtains material d, and material d then is cooled into room temperature is put into granulation 20-60 mesh granular material f are made in machine, material f then is placed in into 80-90 DEG C of dry 2-6h obtains herb fermenting thing.
Preferably, in the preparation technology of herb fermenting thing, Echinacea, red clover, the red sage root, Radix Angelicae Sinensis, radix scutellariae, the fruit of Chinese magnoliavine, Ganoderma lucidum, giant knotweed, the fruit of glossy privet, cellulase, the weight ratio of water and fermented bacterium are 2-5:1-3:2-6:1-4:3-5:4-8:1-4: 3-6:2-5:2-4:1-4:3-5.
Preferably, in the preparation technology of herb fermenting thing, fermented bacterium by saccharomycete, actinomyces and acetic acid bacteria by weight 1-3:2-4:1-5 is mixed.
Preferably, the raw material of modified sustained release agent includes by weight:5-15 parts of Chinese medicine dreg, 2-6 parts of zinc chloride, fish scale 3- 6 parts, 4-5 parts of dimethyl diallyl ammonium chloride, 2-4 parts of cetyl trimethyl amine, 3-5 parts of potassium dihydrogen phosphate, acrylic acid 1-5 Part, 2-5 parts of N,N methylene bis acrylamide, 4-8 parts of ammonium persulfate.
Preferably, modified sustained release agent is prepared by following technique:Chinese medicine dreg and zinc chloride are well mixed, in 80- 90 DEG C of drying are subsequently placed in stainless steel reactor to constant weight, 50-70 DEG C, control pressure are warming up to 5 DEG C/min programming rates For 28-32kPa, room temperature is cooled to, it is 6.0-7.0 then to wash to pH, and material a is obtained after drying;Dried after fish scale is cleaned, 20-40 mesh granular materials are ground into, material a, dimethyl diallyl ammonium chloride and cetyl trimethyl amine is then added It is well mixed, in 650-850r/min rotating speed magnetic agitation 10-20min, 70-90 DEG C is then heated to, 1-3h is incubated, is cooled to 50-70 DEG C, potassium dihydrogen phosphate, acrylic acid, N are added, N- methylene-bisacrylamides and ammonium persulfate are well mixed, are warming up to 60-70 DEG C, 3-4h is incubated, is then stayed overnight with soaked in absolute ethyl alcohol, after washing, be placed in 70-80 DEG C of baking oven and dry to constant weight, warp Pulverize and sieve and obtain being modified sustained release agent.
A kind of late rice plantation preparation method of herb fermenting organic slow-release fertilizer of the present invention, comprises the following steps:
S1, human and animal excreta, stalk, flyash, soybean skin, oil cake, powdered rice hulls, bean dregs, daghestan sweet clover and pale reddish brown lucerne place mixed Close it is uniform after, be ground into 30-50 mesh materials, room temperature be cooled to after drying, then add nitro humus acid and herb fermenting thing in Ferment 2-4d at room temperature, be subsequently added into bentonite in powder, lignin, cocoa pod shell powder, illite powder, banana skin powder, calcium superphosphate, Urea, potassium sulfate, potassium chloride, calcium magnesium phosphate, white clay, careless carbon, kaolin, gangue, quartz, coal slime and ammonium hydrogen carbonate mixing are equal It is even, 50-70 DEG C is warming up to, slurry is stirred into 3500-5500r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 25-30rpm, forms fertilizer Expect particle;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 50-60 DEG C, deliver to sustained release agent bag Coating is carried out in film machine and using the modification sustained release agent of proportioning, the sustained release agent coating machine rotating speed is 10-15rpm;
S5, the fertiliser granulates that will pass through coating are dried by dispelling, are cooled to room temperature and obtain late rice plantation herb fermenting Organic slow-release fertilizer.
Herb fermenting organic slow-release fertilizer use in a kind of late rice plantation proposed by the present invention, its raw material including human and animal excreta, stalk, Flyash, soybean skin, oil cake, powdered rice hulls, bean dregs, bentonite in powder, daghestan sweet clover, pale reddish brown lucerne place, lignin, cocoa pod shell powder, she Sharp stone flour, banana skin powder, calcium superphosphate, urea, potassium sulfate, potassium chloride, calcium magnesium phosphate, white clay, careless carbon, kaolin, gangue, Quartz, coal slime, ammonium hydrogen carbonate, nitro humic acid, herb fermenting thing and modified sustained release agent.Wherein with human and animal excreta, stalk, fine coal Ash, soybean skin, oil cake, powdered rice hulls, bean dregs and herb fermenting thing are organic material, with bentonite in powder, daghestan sweet clover, pale reddish brown lucerne place, wood Quality, cocoa pod shell powder, illite powder and banana skin powder as Controlled-release filler, with calcium superphosphate, urea, potassium sulfate, potassium chloride, Calcium magnesium phosphate, ammonium hydrogen carbonate and nitro humic acid are that inorganic nutritive element supplements material, with white clay, careless carbon, kaolin, gangue, Quartz and coal slime supplement the cooperation of material by organic material, Controlled-release filler and inorganic nutritive element, by modification as hole filler is increased The coating of sustained release agent, the late rice plantation prepared disclosure satisfy that the nutritional need of late rice plantation with organic slow-release fertilizer, with excellent Different sustained release performance, is capable of the release nutriment of uniform high-efficiency, improves the yield and quality of paddy rice.Wherein, herb fermenting Thing after crushing Echinacea, red clover, the red sage root, Radix Angelicae Sinensis, radix scutellariae, the fruit of Chinese magnoliavine, ganoderma lucidum, giant knotweed and the fruit of glossy privet by being well mixed Material a is obtained, then material a, cellulase and water is mixed, enzymolysis obtains material b, and material b then is filtered to take into filtrate, connect And arrive material c by what filtrate concentrated, then mix material c with fermented bacterium, fermentation obtains material d, then cools down material d It is put into room temperature in comminutor and granular material f is made, then material f is dried to obtain in herb fermenting thing, utilization in spice Organic matter and inorganic nutritive element, by fermentation obtain late rice be more easy to absorb material, for late rice growth provide it is rich Rich nutriment and microorganism species, improves the yield and quality of late rice.Wherein, modified sustained release agent is by by Chinese medicine dreg It is well mixed with zinc chloride, dry to constant weight, be subsequently placed in stainless steel reactor, room temperature is cooled to after heating, is then washed, Material a is obtained after drying;Granular material is dry, pulverize into after fish scale is cleaned, material a, the allyl of dimethyl two is then added Ammonium chloride and cetyl trimethyl amine are well mixed, in magnetic agitation, then heat up, and are incubated, and cooling adds biphosphate Potassium, acrylic acid, N, N- methylene-bisacrylamides and ammonium persulfate are well mixed, and are heated up, and soaked in absolute ethyl alcohol is then used in insulation Overnight, after washing, it is placed in baking oven and dries to constant weight, size-reduced sieving obtains being modified sustained release agent, in the plantation for applying to paddy rice, The sustained release performance of paddy rice is effectively increased, is coordinated with herb fermenting thing, release nutriment that can be efficiently high-quality, water supply rice gives birth to It is long to absorb, effectively increase the yield and quality of paddy rice.
Embodiment
The present invention is described in detail with reference to specific embodiment, it should be appreciated that embodiment is served only for illustrating this hair It is bright, rather than for limiting the invention, any modification made on the basis of the present invention, equivalent substitution etc. are in this hair In bright protection domain.
In embodiment, the parts by weight of human and animal excreta can for 80 parts, 85 parts, 90 parts, 95 parts, 100 parts, 105 parts, 110 parts, 115 parts, 120 parts;The parts by weight of stalk can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts;The weight of flyash Part can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts;The parts by weight of soybean skin can for 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 Part, 6 parts;The parts by weight of oil cake can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;Powdered rice hulls Parts by weight can for 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;The parts by weight of bean dregs can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts;The parts by weight of bentonite in powder can be with For 2 parts, 3 parts, 4 parts, 5 parts, 6 parts;The parts by weight of daghestan sweet clover can for 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The parts by weight of pale reddish brown lucerne place can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts; The parts by weight of lignin can for 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 Part, 9 parts;The parts by weight of cocoa pod shell powder can be 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;She The parts by weight of sharp stone flour can be 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts;The parts by weight of banana skin powder can be 4 Part, 4.1 parts, 4.2 parts, 4.3 parts, 4.4 parts, 4.5 parts, 4.6 parts, 4.7 parts, 4.8 parts, 4.9 parts, 5 parts;The parts by weight of calcium superphosphate It can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts;The parts by weight of urea can for 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 Part, 7.5 parts, 8 parts;The parts by weight of potassium sulfate can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts;The weight of potassium chloride It can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts to measure part;The parts by weight of calcium magnesium phosphate can for 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 Part;The parts by weight of white clay can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts;The parts by weight of careless carbon can for 3 parts, 3.5 parts, 4 parts, 4.5 Part, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;Kaolinic parts by weight can be 1 part, 2 parts, 3 parts, 4 parts, 5 parts; The parts by weight of gangue can be 1 part, 1.5 parts, 2 parts, 2.5 parts, 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts;Stone The parts by weight of English can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts;The parts by weight of coal slime can for 3 parts, 3.5 parts, 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts, 8.5 parts, 9 parts;The parts by weight of ammonium hydrogen carbonate can for 4 parts, 4.5 parts, 5 parts, 5.5 parts, 6 parts, 6.5 parts, 7 parts, 7.5 parts, 8 parts;The parts by weight of nitro humic acid can for 1 part, 2 parts, 3 parts, 4 Part, 5 parts;The parts by weight of herb fermenting thing can be 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts, 10 parts, 11 parts, 12 parts;It is modified slow The parts by weight for releasing agent can be 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts.
Embodiment 1
Herb fermenting organic slow-release fertilizer is used in a kind of late rice plantation proposed by the present invention, and its raw material includes by weight:People and animals 100 parts of excrement, 5 parts of stalk, 3 parts of flyash, 4.5 parts of soybean skin, 6 parts of oil cake, 4.5 parts of powdered rice hulls, 5 parts of bean dregs, bentonite in powder 4 Part, 3 parts of daghestan sweet clover, 4 parts of pale reddish brown lucerne place, 6 parts of lignin, 6 parts of cocoa pod shell powder, 3.5 parts of illite powder, 4.5 parts of banana skin powder, 4 parts of calcium superphosphate, 6 parts of urea, 2.5 parts of potassium sulfate, 4 parts of potassium chloride, 6 parts of calcium magnesium phosphate, 3 parts of white clay, careless 5.5 parts of carbon, kaolinite 3 parts of soil, 3.5 parts of gangue, 5 parts of quartz, 6 parts of coal slime, 6 parts of ammonium hydrogen carbonate, 3 parts of nitro humic acid, 8 parts of herb fermenting thing, change 15 parts of sustained release agent of property.
Embodiment 2
Herb fermenting organic slow-release fertilizer is used in a kind of late rice plantation proposed by the present invention, and its raw material includes by weight:People and animals 80 parts of excrement, 8 parts of stalk, 1 part of flyash, 6 parts of soybean skin, 4 parts of oil cake, 8 parts of powdered rice hulls, 2 parts of bean dregs, 6 parts of bentonite in powder, grass 1 part of wooden slippers, 6 parts of pale reddish brown lucerne place, 3 parts of lignin, 8 parts of cocoa pod shell powder, 2 parts of illite powder, 5 parts of banana skin powder, calcium superphosphate 2 Part, 8 parts of urea, 1 part of potassium sulfate, 6 parts of potassium chloride, 3 parts of calcium magnesium phosphate, 5 parts of white clay, careless 3 parts of carbon, 5 parts of kaolin, gangue 1 Part, 8 parts of quartz, 3 parts of coal slime, 8 parts of ammonium hydrogen carbonate, 1 part of nitro humic acid, 12 parts of herb fermenting thing, modified 10 parts of sustained release agent.
Herb fermenting thing is prepared by following technique:By weight by 2 parts of Echinaceas, 3 parts of red clovers, 2 parts of reds sage root, 4 parts of Radix Angelicae Sinensis, 3 parts of radix scutellariaes, 8 portions of fruit ofs Chinese magnoliavine, 1 portion of ganoderma lucidum, 6 parts of giant knotweeds and 2 portions of fruit of glossy privets are well mixed after crushing and obtain material a, Then material a, 4 parts of cellulases and 1 part of water are mixed, 45 DEG C of enzymolysis 2h obtain material b, and material b then is filtered to take into filtrate, Then material c is arrived by what filtrate concentrated, then mixes material c with 5 parts of fermented bacteriums, the 10d that fermented in 55 DEG C obtains material d, Then material d is cooled to room temperature and be put into comminutor and 20 mesh granular material f are made, material f is then placed in 90 DEG C of dryings 2h obtains herb fermenting thing.
In the preparation technology of herb fermenting thing, fermented bacterium is by saccharomycete, actinomyces and acetic acid bacteria by weight 1:4:1 mixes Conjunction is formed.
Modified sustained release agent is prepared by following technique:5 parts of Chinese medicine dregs and 6 parts of zinc chloride are mixed equal by weight It is even, in 80 DEG C of drying to constant weight, it is subsequently placed in stainless steel reactor, 70 DEG C, control pressure is warming up to 5 DEG C/min programming rates Power is 28kPa, is cooled to room temperature, and it is 7.0 then to wash to pH, and material a is obtained after drying;Dried after 3 parts of fish scales are cleaned, powder 40 mesh granular materials are broken into, material a, 4 parts of dimethyl diallyl ammonium chlorides and 4 parts of cetyl trimethyl amine are then added It is well mixed, in 650r/min rotating speed magnetic agitation 20min, 70 DEG C are then heated to, 3h is incubated, 50 DEG C are cooled to, 5 parts are added Potassium dihydrogen phosphate, 1 part of acrylic acid, 5 parts of N, N- methylene-bisacrylamides and 4 parts of ammonium persulfates are well mixed, and are warming up to 70 DEG C, 3h is incubated, is then stayed overnight with soaked in absolute ethyl alcohol, after washing, is placed in 80 DEG C of baking ovens and dries to constant weight, size-reduced sieving is obtained Modified sustained release agent.
Embodiment 3
Herb fermenting organic slow-release fertilizer is used in a kind of late rice plantation proposed by the present invention, and its raw material includes by weight:People and animals 120 parts of excrement, 2 parts of stalk, 5 parts of flyash, 3 parts of soybean skin, 8 parts of oil cake, 1 part of powdered rice hulls, 8 parts of bean dregs, 2 parts of bentonite in powder, 5 parts of daghestan sweet clover, 2 parts of pale reddish brown lucerne place, 9 parts of lignin, 4 parts of cocoa pod shell powder, 5 parts of illite powder, 4 parts of banana skin powder, peroxophosphoric acid 6 parts of calcium, 4 parts of urea, 4 parts of potassium sulfate, 2 parts of potassium chloride, 9 parts of calcium magnesium phosphate, 1 part of white clay, careless 8 parts of carbon, 1 part of kaolin, bastard coal 6 parts of stone, 2 parts of quartz, 9 parts of coal slime, 4 parts of ammonium hydrogen carbonate, 5 parts of nitro humic acid, 4 parts of herb fermenting thing, modified 20 parts of sustained release agent.
A kind of late rice plantation preparation method of herb fermenting organic slow-release fertilizer of the present invention, comprises the following steps:
S1, human and animal excreta, stalk, flyash, soybean skin, oil cake, powdered rice hulls, bean dregs, daghestan sweet clover and pale reddish brown lucerne place mixed After closing uniformly, 50 mesh materials are ground into, room temperature is cooled to after drying, nitro humus acid and herb fermenting thing are then added in room temperature Lower fermentation 2d, be subsequently added into bentonite in powder, lignin, cocoa pod shell powder, illite powder, banana skin powder, calcium superphosphate, urea, Potassium sulfate, potassium chloride, calcium magnesium phosphate, white clay, careless carbon, kaolin, gangue, quartz, coal slime and ammonium hydrogen carbonate are well mixed, rise Temperature stirs into slurry to 70 DEG C in 3500r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 30rpm, forms fertilizer Particle;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 50 DEG C, deliver to sustained release agent coating machine Interior and using proportioning modification sustained release agent carries out coating, and the sustained release agent coating machine rotating speed is 15rpm;
S5, the fertiliser granulates that will pass through coating are dried by dispelling, are cooled to room temperature and obtain late rice plantation herb fermenting Organic slow-release fertilizer.
Embodiment 4
Herb fermenting organic slow-release fertilizer is used in a kind of late rice plantation proposed by the present invention, and its raw material includes by weight:People and animals 85 parts of excrement, 7 parts of stalk, 2 parts of flyash, 5 parts of soybean skin, 5 parts of oil cake, 7 parts of powdered rice hulls, 3 parts of bean dregs, 5 parts of bentonite in powder, grass 2 parts of wooden slippers, 5 parts of pale reddish brown lucerne place, 4 parts of lignin, 7 parts of cocoa pod shell powder, 3 parts of illite powder, 4.8 parts of banana skin powder, peroxophosphoric acid 3 parts of calcium, 7 parts of urea, 2 parts of potassium sulfate, 5 parts of potassium chloride, 4 parts of calcium magnesium phosphate, 4 parts of white clay, careless 4 parts of carbon, 4 parts of kaolin, bastard coal 2 parts of stone, 7 parts of quartz, 4 parts of coal slime, 7 parts of ammonium hydrogen carbonate, 2 parts of nitro humic acid, 11 parts of herb fermenting thing, modified sustained release agent 12 Part.
Herb fermenting thing is prepared by following technique:By weight by 3 parts of Echinaceas, 2.5 parts of red clovers, 3 parts of pellets Ginseng, 3 parts of Radix Angelicae Sinensis, 3.5 parts of radix scutellariaes, 7 portions of fruit ofs Chinese magnoliavine, 2 portions of ganoderma lucidums, 5 parts of giant knotweeds and 3 portions of fruit of glossy privets are well mixed after crushing and obtain thing Expect a, then mix material a, 3.5 parts of cellulases and 2 parts of water, 42 DEG C of enzymolysis 3h obtain material b, then filter material b Filtrate is taken, then material c is arrived by what filtrate concentrated, then mixes material c with 4.5 parts of fermented bacteriums, the 9d that fermented in 58 DEG C is obtained To material d, material d is then cooled to room temperature be put into comminutor 30 mesh granular material f are made, be then placed in material f 88 DEG C of dry 3h obtain herb fermenting thing.
In the preparation technology of herb fermenting thing, fermented bacterium is by saccharomycete, actinomyces and acetic acid bacteria by weight 1.5: 3.5:2 mix.
Modified sustained release agent is prepared by following technique:8 parts of Chinese medicine dregs and 5 parts of zinc chloride are mixed equal by weight It is even, in 82 DEG C of drying to constant weight, it is subsequently placed in stainless steel reactor, 65 DEG C, control pressure is warming up to 5 DEG C/min programming rates Power is 29kPa, is cooled to room temperature, and it is 6.8 then to wash to pH, and material a is obtained after drying;Dried after 4 parts of fish scales are cleaned, powder 35 mesh granular materials are broken into, material a, 4.2 parts of dimethyl diallyl ammonium chlorides and 3.5 parts of cetyl front threes are then added Base amine is well mixed, in 680r/min rotating speed magnetic agitation 18min, then heats to 75 DEG C, is incubated 2.5h, is cooled to 55 DEG C, 4.5 parts of potassium dihydrogen phosphates, 2 parts of acrylic acid, 4 parts of N are added, N- methylene-bisacrylamides and 5 parts of ammonium persulfates are well mixed, risen Temperature is incubated 3.2h, then stayed overnight with soaked in absolute ethyl alcohol to 68 DEG C, after washing, is placed in 78 DEG C of baking ovens and dries to constant weight, through powder Broken sieving obtains being modified sustained release agent.
A kind of late rice plantation preparation method of herb fermenting organic slow-release fertilizer of the present invention, comprises the following steps:
S1, human and animal excreta, stalk, flyash, soybean skin, oil cake, powdered rice hulls, bean dregs, daghestan sweet clover and pale reddish brown lucerne place mixed After closing uniformly, 35 mesh materials are ground into, room temperature is cooled to after drying, nitro humus acid and herb fermenting thing are then added in room temperature Lower fermentation 3.5d, is subsequently added into bentonite in powder, lignin, cocoa pod shell powder, illite powder, banana skin powder, calcium superphosphate, urine Element, potassium sulfate, potassium chloride, calcium magnesium phosphate, white clay, careless carbon, kaolin, gangue, quartz, coal slime and ammonium hydrogen carbonate mixing are equal It is even, 55 DEG C are warming up to, slurry is stirred into 5200r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 26rpm, forms fertilizer Particle;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 58 DEG C, deliver to sustained release agent coating machine Interior and using proportioning modification sustained release agent carries out coating, and the sustained release agent coating machine rotating speed is 11rpm;
S5, the fertiliser granulates that will pass through coating are dried by dispelling, are cooled to room temperature and obtain late rice plantation herb fermenting Organic slow-release fertilizer.
Embodiment 5
Herb fermenting organic slow-release fertilizer is used in a kind of late rice plantation proposed by the present invention, and its raw material includes by weight:People and animals 115 parts of excrement, 3 parts of stalk, 4 parts of flyash, 4 parts of soybean skin, 7 parts of oil cake, 2 parts of powdered rice hulls, 7 parts of bean dregs, 3 parts of bentonite in powder, 4 parts of daghestan sweet clover, 3 parts of pale reddish brown lucerne place, 8 parts of lignin, 5 parts of cocoa pod shell powder, 4 parts of illite powder, excessively 4.2 parts of banana skin powder, phosphorus Sour 5 parts of calcium, 5 parts of urea, 3 parts of potassium sulfate, 3 parts of potassium chloride, 8 parts of calcium magnesium phosphate, 2 parts of white clay, careless 7 parts of carbon, 2 parts of kaolin, coal 5 parts of spoil, 3 parts of quartz, 8 parts of coal slime, 5 parts of ammonium hydrogen carbonate, 4 parts of nitro humic acid, 5 parts of herb fermenting thing, modified sustained release agent 18 Part.
Herb fermenting thing is prepared by following technique:By weight by 4 parts of Echinaceas, 1.5 parts of red clovers, 5 parts of pellets Ginseng, 2 parts of Radix Angelicae Sinensis, 4.5 parts of radix scutellariaes, 5 portions of fruit ofs Chinese magnoliavine, 3 portions of ganoderma lucidums, 4 parts of giant knotweeds and 4 portions of fruit of glossy privets are well mixed after crushing and obtain thing Expect a, then mix material a, 2.5 parts of cellulases and 3 parts of water, 38 DEG C of enzymolysis 4h obtain material b, then filter material b Filtrate is taken, then material c is arrived by what filtrate concentrated, then mixes material c with 3.5 parts of fermented bacteriums, the 6d that fermented in 62 DEG C is obtained To material d, material d is then cooled to room temperature be put into comminutor 50 mesh granular material f are made, be then placed in material f 82 DEG C of dry 5h obtain herb fermenting thing.
In the preparation technology of herb fermenting thing, fermented bacterium is by saccharomycete, actinomyces and acetic acid bacteria by weight 2.5: 2.5:4 mix.
Modified sustained release agent is prepared by following technique:12 parts of Chinese medicine dregs and 3 parts of zinc chloride are mixed equal by weight It is even, in 88 DEG C of drying to constant weight, it is subsequently placed in stainless steel reactor, 55 DEG C, control pressure is warming up to 5 DEG C/min programming rates Power is 31kPa, is cooled to room temperature, and it is 6.2 then to wash to pH, and material a is obtained after drying;Dried after 5 parts of fish scales are cleaned, powder 25 mesh granular materials are broken into, material a, 4.8 parts of dimethyl diallyl ammonium chlorides and 2.5 parts of cetyl front threes are then added Base amine is well mixed, in 820r/min rotating speed magnetic agitation 12min, then heats to 85 DEG C, is incubated 1.5h, is cooled to 65 DEG C, 3.5 parts of potassium dihydrogen phosphates, 4 parts of acrylic acid, 3 parts of N are added, N- methylene-bisacrylamides and 7 parts of ammonium persulfates are well mixed, risen Temperature is incubated 3.8h, then stayed overnight with soaked in absolute ethyl alcohol to 62 DEG C, after washing, is placed in 72 DEG C of baking ovens and dries to constant weight, through powder Broken sieving obtains being modified sustained release agent.
A kind of late rice plantation preparation method of herb fermenting organic slow-release fertilizer of the present invention, comprises the following steps:
S1, human and animal excreta, stalk, flyash, soybean skin, oil cake, powdered rice hulls, bean dregs, daghestan sweet clover and pale reddish brown lucerne place mixed After closing uniformly, 45 mesh materials are ground into, room temperature is cooled to after drying, nitro humus acid and herb fermenting thing are then added in room temperature Lower fermentation 2.5d, is subsequently added into bentonite in powder, lignin, cocoa pod shell powder, illite powder, banana skin powder, calcium superphosphate, urine Element, potassium sulfate, potassium chloride, calcium magnesium phosphate, white clay, careless carbon, kaolin, gangue, quartz, coal slime and ammonium hydrogen carbonate mixing are equal It is even, 65 DEG C are warming up to, slurry is stirred into 3800r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 29rpm, forms fertilizer Particle;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 52 DEG C, deliver to sustained release agent coating machine Interior and using proportioning modification sustained release agent carries out coating, and the sustained release agent coating machine rotating speed is 14rpm;
S5, the fertiliser granulates that will pass through coating are dried by dispelling, are cooled to room temperature and obtain late rice plantation herb fermenting Organic slow-release fertilizer.
By sample fertilizer before rice transplanting, by every 53kg/667m2Amount disposably apply, contrast groups are according to a conventional method Basal dressing and topdress, total fertilization amount is 70kg/667m2, fertilizer is nitrogen-phosphorus-potassium compound fertilizer, wherein, nitrogenous fertilizer and potash fertilizer are spread in two times Apply;
Yield-increasing efficiency=(experimental group yield/contrast groups yield -1) * 100%
Table 1:
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (7)

1. herb fermenting organic slow-release fertilizer is used in a kind of late rice plantation, it is characterised in that its raw material includes by weight:Human and animal excreta 80-120 parts, it is 2-8 parts of stalk, 1-5 parts of flyash, 3-6 parts of soybean skin, 4-8 parts of oil cake, 1-8 parts of powdered rice hulls, 2-8 parts of bean dregs, swollen Native 2-6 parts of the powder of profit, 1-5 parts of daghestan sweet clover, pale reddish brown lucerne place 2-6 parts, 3-9 parts of lignin, 4-8 parts of cocoa pod shell powder, illite powder 2-5 Part, 4-5 parts of banana skin powder, 2-6 parts of calcium superphosphate, 4-8 parts of urea, 1-4 parts of potassium sulfate, 2-6 parts of potassium chloride, calcium magnesium phosphate 3-9 Part, 1-5 parts of white clay, careless 3-8 parts of carbon, 1-5 parts of kaolin, 1-6 parts of gangue, 2-8 parts of quartz, 3-9 parts of coal slime, ammonium hydrogen carbonate 4- 8 parts, 1-5 parts of nitro humic acid, 4-12 parts of herb fermenting thing, modified 10-20 parts of sustained release agent.
2. herb fermenting organic slow-release fertilizer is used in late rice plantation according to claim 1, it is characterised in that herb fermenting thing is pressed It is prepared by following technique:By Echinacea, red clover, the red sage root, Radix Angelicae Sinensis, radix scutellariae, the fruit of Chinese magnoliavine, ganoderma lucidum, giant knotweed and ligustrum lucidum powder It is well mixed after broken to obtain material a, then material a, cellulase and water are mixed, 35-45 DEG C of enzymolysis 2-5h obtains material b, Then material b is filtered to take into filtrate, then arrives material c by what filtrate concentrated, then mix material c with fermented bacterium, in 55- 65 DEG C of fermentation 5-10d obtain material d, material d then is cooled into room temperature be put into comminutor 20-60 mesh granular materials are made F, is then placed in 80-90 DEG C of dry 2-6h by material f and obtains herb fermenting thing.
3. herb fermenting organic slow-release fertilizer is used in late rice plantation according to claim 1 or 2, it is characterised in that herb fermenting In the preparation technology of thing, Echinacea, red clover, the red sage root, Radix Angelicae Sinensis, radix scutellariae, the fruit of Chinese magnoliavine, ganoderma lucidum, giant knotweed, the fruit of glossy privet, cellulose The weight ratio of enzyme, water and fermented bacterium is 2-5:1-3:2-6:1-4:3-5:4-8:1-4:3-6:2-5:2-4:1-4:3-5.
4. the late rice plantation herb fermenting organic slow-release fertilizer according to claim any one of 1-3, it is characterised in that Chinese medicine In the preparation technology of fermentate, fermented bacterium is by saccharomycete, actinomyces and acetic acid bacteria by weight 1-3:2-4:1-5 mix and Into.
5. the late rice plantation herb fermenting organic slow-release fertilizer according to claim any one of 1-4, it is characterised in that modified The raw material of sustained release agent includes by weight:5-15 parts of Chinese medicine dreg, 2-6 parts of zinc chloride, 3-6 parts of fish scale, dimethyl diallyl 4-5 parts of ammonium chloride, 2-4 parts of cetyl trimethyl amine, 3-5 parts of potassium dihydrogen phosphate, 1-5 parts of acrylic acid, N, N- di-2-ethylhexylphosphine oxides third 2-5 parts of acrylamide, 4-8 parts of ammonium persulfate.
6. the late rice plantation herb fermenting organic slow-release fertilizer according to claim any one of 1-5, it is characterised in that modified Sustained release agent is prepared by following technique:Chinese medicine dreg and zinc chloride are well mixed, in 80-90 DEG C of drying to constant weight, then It is placed in stainless steel reactor, is warming up to 50-70 DEG C with 5 DEG C/min programming rates, control pressure is 28-32kPa, is cooled to room Temperature, it is 6.0-7.0 then to wash to pH, and material a is obtained after drying;20-40 mesh graininess is dry, pulverize into after fish scale is cleaned Material, then adds material a, dimethyl diallyl ammonium chloride and cetyl trimethyl amine and is well mixed, in 650-850r/ Min rotating speed magnetic agitation 10-20min, then heat to 70-90 DEG C, are incubated 1-3h, are cooled to 50-70 DEG C, add biphosphate Potassium, acrylic acid, N, N- methylene-bisacrylamides and ammonium persulfate are well mixed, and are warming up to 60-70 DEG C, are incubated 3-4h, then Stayed overnight with soaked in absolute ethyl alcohol, after washing, be placed in 70-80 DEG C of baking oven and dry to constant weight, size-reduced sieving obtains being modified sustained release Agent.
7. a kind of preparation method of late rice plantation herb fermenting organic slow-release fertilizer according to claim any one of 1-6, It is characterised in that it includes following steps:
S1, human and animal excreta, stalk, flyash, soybean skin, oil cake, powdered rice hulls, bean dregs, daghestan sweet clover and pale reddish brown lucerne place mixed equal After even, 30-50 mesh materials are ground into, room temperature is cooled to after drying, nitro humus acid and herb fermenting thing are then added in room temperature Lower fermentation 2-4d, is subsequently added into bentonite in powder, lignin, cocoa pod shell powder, illite powder, banana skin powder, calcium superphosphate, urine Element, potassium sulfate, potassium chloride, calcium magnesium phosphate, white clay, careless carbon, kaolin, gangue, quartz, coal slime and ammonium hydrogen carbonate mixing are equal It is even, 50-70 DEG C is warming up to, slurry is stirred into 3500-5500r/min;
S3, the slurry that S2 is obtained is delivered in comminutor granulated, the comminutor rotating speed is 25-30rpm, forms fertilizer Grain;
S4, the fertiliser granulates that S3 is obtained are delivered to cooler cooling, after temperature is down to 50-60 DEG C, deliver to sustained release agent coating machine Interior and using proportioning modification sustained release agent carries out coating, and the sustained release agent coating machine rotating speed is 10-15rpm;
S5, it will be dried by the fertiliser granulates of coating by dispelling, being cooled to room temperature, to obtain late rice plantation herb fermenting organic Slow-release fertilizer.
CN201710244360.XA 2017-04-14 2017-04-14 A kind of late rice plantation herb fermenting organic slow-release fertilizer and preparation method thereof Withdrawn CN107021813A (en)

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CN112079673A (en) * 2020-08-31 2020-12-15 贵州黔亨生态肥业有限公司 Organic fertilizer prepared from coal slime and agricultural products and preparation method thereof
CN118930366A (en) * 2024-08-23 2024-11-12 甘肃昊洲土壤修复科技有限责任公司 Attapulgite organic fertilizer and preparation method thereof
CN119684057A (en) * 2024-12-17 2025-03-25 黑龙江艾加生物技术有限公司 Water-retention yield-increasing liquid microbial fertilizer and preparation method thereof
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CN112079673A (en) * 2020-08-31 2020-12-15 贵州黔亨生态肥业有限公司 Organic fertilizer prepared from coal slime and agricultural products and preparation method thereof
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