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CN106903302A - A kind of metal powder degassing, encapsulation, pincers envelope integration apparatus - Google Patents

A kind of metal powder degassing, encapsulation, pincers envelope integration apparatus Download PDF

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Publication number
CN106903302A
CN106903302A CN201710114614.6A CN201710114614A CN106903302A CN 106903302 A CN106903302 A CN 106903302A CN 201710114614 A CN201710114614 A CN 201710114614A CN 106903302 A CN106903302 A CN 106903302A
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CN
China
Prior art keywords
powder
vacuum
jacket
encapsulation
transitional storehouse
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Granted
Application number
CN201710114614.6A
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Chinese (zh)
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CN106903302B (en
Inventor
马乐
贾庆功
王锦群
方向明
张嘉
杜亚宁
孙斌
黄金亮
张磊
张弛
丁锋钰
王亚滨
李扬扬
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Xi'an Cumulative Equipment Technology Co Ltd
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Xi'an Cumulative Equipment Technology Co Ltd
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Priority to CN201710114614.6A priority Critical patent/CN106903302B/en
Publication of CN106903302A publication Critical patent/CN106903302A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/14Treatment of metallic powder

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  • Basic Packing Technique (AREA)

Abstract

A kind of metal powder degassing, encapsulation, pincers envelope integration apparatus, including powder tank, powder tank are connected by powder mass flow flow speed control valve one, vacuum corrugated pipe one with transitional storehouse;The bottom of transitional storehouse is connected by vacuum pipe one with dress powder jacket;The right-hand member of transitional storehouse is connected by filter with vacuum valve, and vacuum valve is connected with vacuum pump set;After the vacuum of transitional storehouse, dress powder jacket reaches requirement, powder tank and transitional storehouse are connected, powder flows into dress powder jacket;Transitional storehouse powder overflows, the alarm of powder level detecting apparatus;Pipeline heating system convection current heats degasification through the powder of transitional storehouse;Not enough, weighing system alarm more renews powder tank to the powder of powder tank 1;Tube wall vibration device prevents the blocking of vacuum pipe one;After loading a certain amount of powder, powder mass flow flow speed control valve is closed, open shaking platform and realize powder in jacket middle-high density jolt ramming;After having been charged into the powder jolt ramming of jacket, continue to fill powder;With easy to operate, degassing effect it is good, tap density is high the characteristics of.

Description

A kind of metal powder degassing, encapsulation, pincers envelope integration apparatus
Technical field
The invention belongs to powder metallurgical technology, and in particular to a kind of metal powder degassing, encapsulation, pincers envelope integration set It is standby.
Background technology
The preparation of metal powder degassing jacket is the critical process for obtaining high-quality powder metallurgy blank, and high-quality powder is closed The main purposes of golden blank is for manufacturing high performance aero-engine turbine disk, in order to ensure that aero-engine turbine disk has There are enough material properties, the equipment for obtaining metal powder degassing jacket needed for high-quality powder metallurgy blank is particularly critical.
Prepare during metal powder degassing sheathing process, metal powder granulates and jacket all easily adsorb outside in itself There is density gradient in jacket dress powder short transverse in powder density after water, hydrogen in environment, oxygen, and powder loading jacket Difference, two kinds of situations cause the powder metallurgy blank that degasification makes when being wrapped in follow-up high temperature insostatic pressing (HIP) to there is low density, gas to contain High defect is measured, finally cannot be used for making qualified aero-engine turbine disk.
The equipment of current existing metal powder degassing jacket, is all only to carry out degasification to jacket, have ignored powder in itself The removal of adsorbed gas, it is bad to ultimately result in overall degassing effect, additionally, due to lacked in equipment necessary environmental monitoring and Powder position detection, the final metal powder degassing jacket quality for obtaining is unstable, and integration of equipments degree is not high, it is numerous to operate It is trivial, subsequently also to carry out secondary degasification etc..
The present invention not only considers to carry out degasification to jacket body, it is also contemplated that powder surface gas in itself is removed, Environmental monitoring and the detection of powder position are increased simultaneously, it is final to ensure to obtain the reliable metal powder degassing jacket of steady quality, in addition, By the degasification of metal dust, encapsulation, pincers envelope it is integrated after, equipment integrated degree is high, easy to operate.
The content of the invention
To overcome above-mentioned the deficiencies in the prior art, it is an object of the invention to provide a kind of metal powder degassing, encapsulation, pincers Envelope integration apparatus, solve the shortcomings of existing equipment degassing effect is poor, quality is unstable, device integration is not high, finally obtain Obtain high-quality powder metallurgy blank.
To achieve the above object, the technical solution adopted by the present invention is:A kind of metal powder degassing, encapsulation, pincers envelope one Change equipment, including powder tank, powder tank are connected by powder mass flow flow speed control valve one, vacuum corrugated pipe one with transitional storehouse;The bottom of transitional storehouse Portion is connected by vacuum pipe one with dress powder jacket;The right-hand member of transitional storehouse is connected by filter with vacuum valve, vacuum valve with Vacuum pump set is connected.
Described powder pot bottom is equipped with weighing system.
Described transitional storehouse be provided with observation panel, vacuum detecting instrument, gas analysis instrument, powder level detecting apparatus one and Pipeline heating system.
On described vacuum pipe one by it is upper under be sequentially provided with powder mass flow flow speed control valve two, powder mass flow flow speed control valve three, Vacuum corrugated pipe two;
Tube wall vibration device is installed on the tube wall of described vacuum pipe one.
Vacuum pipe one between described tube wall vibration device and powder mass flow flow speed control valve three is provided with powder level detecting apparatus Two.
The powder inlet of described dress powder jacket is equipped with hydraulic tongs seal apparatus, treats that powder level detecting apparatus detection jacket powder loads After amount arrival powder position requires height, hydraulic tongs seal apparatus are sealed powder jacket powder inlet is filled.
Described dress powder jacket bottom is provided with shaking platform.
Described shaking platform is designed using three-dimensional vibrating direction.
Vacuum pipe two is provided between described vacuum valve and vacuum pump set;One section of vacuum ripple is provided with the middle of vacuum pipe two Line pipe three.
Described vacuum pump set includes one group of sliding vane rotary vacuum pump and one group of diffusion vacuum pump, and working vacuum reaches 5 × 10- 3Pa。
The beneficial effects of the invention are as follows:
The present invention be it is a set of by metal dust under vacuum conditions degasification, encapsulation, pincers inside back cover operation be combined it is complete, steady Fixed, efficient metal dust jacket Preparation equipment.Improve efficiency, the easy to operate, degasification of metal powder degassing jacket preparation Effect is good, tap density is high, meets the follow-up high temperature insostatic pressing (HIP) that carries out to filling the requirements such as powder jacket air content is low, consistency is high.Tool Body advantage is as follows:
Whole powder deaeration jacket preparation process realizes degasification under vacuum environment, encapsulation, pincers inside back cover operation and is combined, equipment Easy to operate, integrated degree is high.
Whole powder deaeration jacket preparation process realizes degasification while to jacket and powder, and degassing effect is good.
Whole powder deaeration jacket preparation process realizes the monitoring to environmental gas, including vacuum, water, oxygen, hydrogen Detection, it is ensured that quality prepared by degasification jacket.
Whole powder deaeration jacket preparation process realizes the detection of filling amount, including to the detection of powder amount in powder tank, with And the detection of the final filling amount of jacket, it is ensured that stabilization, the reliability of degasification jacket preparation process.
Brief description of the drawings
Fig. 1 is metal powder degassing of the present invention, encapsulation, the structural representation of pincers envelope integration apparatus.
Specific embodiment
Specific embodiment of the invention is described in detail below in conjunction with the accompanying drawings:
Referring to Fig. 1, a kind of metal powder degassing, encapsulation, pincers envelope integration apparatus, including powder tank 1, it is characterised in that powder tank 1 leads to Powder mass flow flow speed control valve 1, vacuum corrugated pipe 1 is crossed to be connected with transitional storehouse 6;The bottom of transitional storehouse 6 passes through vacuum pipe 1 It is connected with dress powder jacket 12;The right-hand member of transitional storehouse 6 is connected by filter 16 with vacuum valve 17, vacuum valve and vacuum pump set 18 It is connected.
The described bottom of powder tank 1 is equipped with weighing system 2, and weighing system 2 detects the powder of powder tank 1 at any time during powder is filled Surplus, such as powder are not enough, and powder tank 1 is changed in time.
Described transitional storehouse 6 is provided with observation panel 7, vacuum detecting instrument 14, gas analysis instrument 15, powder level detecting apparatus One 5 and pipeline heating system 8, the convection current of pipeline heating system 8 heats degasification through the powder of transitional storehouse 6.
On described vacuum pipe 1 powder mass flow flow speed control valve 2 19, powder mass flow flow speed control valve are sequentially provided with by upper under 3 20, vacuum corrugated pipe 2 21;
Tube wall vibration device 9 is installed on the tube wall of described vacuum pipe 1, the blocking in powder course of conveying is prevented.
Vacuum pipe 1 between described tube wall vibration device 9 and powder mass flow flow speed control valve 3 20 is provided with the detection of powder position Device 2 24.
The powder inlet of described dress powder jacket 12 is equipped with hydraulic tongs seal apparatus 11, treats that powder level detecting apparatus 24 detect jacket powder After last charge weight arrival powder position requires height, hydraulic tongs seal apparatus 11 will fill the powder inlet of powder jacket 12 and be sealed.
The described bottom of dress powder jacket 12 is provided with shaking platform 13, shaking platform 13 play fixed dress powder jacket 12 and The effect of jolt ramming powder.
Described shaking platform 13 is using the design of three-dimensional vibrating direction, the vibration by top to bottom, left and right, front and rear to jacket 12 Realize powder in jacket middle-high density jolt ramming.
Vacuum pipe 2 23 is provided between described vacuum valve 17 and vacuum pump set 18;One is provided with the middle of vacuum pipe 2 23 Section vacuum corrugated pipe 3 22.
Described vacuum pump set 18 includes one group of sliding vane rotary vacuum pump and one group of diffusion vacuum pump, and working vacuum reaches 5 × 10- 3Pa, vacuum pump set mainly carries out degasification to dress powder jacket 12 and vacuum pipe.
Water in the described detection of gas analysis instrument 15 transitional storehouse 6, oxygen, hydrogen content.
Powder level detecting apparatus 1 and powder level detecting apparatus 2 24, detect whether the powder of transitional storehouse 6 overflows and fill respectively The final dress powder powder position height of powder jacket 12, pipeline heating system 8 is arranged on the pipeline both sides that powder flows into transitional storehouse 6, convection current Heating degasification is carried out through the powder of transitional storehouse 6.Tube wall vibration device 9 is installed on the tube wall of vacuum pipe 1, prevents powder defeated Blocking during sending.The powder inlet of dress powder jacket 12 is equipped with hydraulic tongs seal apparatus 11, treats that powder level detecting apparatus 5 detect jacket powder After charge weight arrival powder position requires height, hydraulic tongs seal apparatus 11 will fill the powder inlet of powder jacket 12 and be sealed.Dress powder jacket 12 Bottom is provided with shaking platform 13, and shaking platform 13 plays a part of fixed jacket 12 and jolt ramming powder.Vacuum pump set 18 is wrapped One group of sliding vane rotary vacuum pump and one group of diffusion vacuum pump are included, working vacuum reaches 5 × 10-3Pa, vacuum pump set 18 is main to dress powder bag Set 12 and vacuum pipe carry out degasification.In addition filter 16 and vacuum valve 17 are installed in the front end of vacuum pump set 18.
Specific metal powder degassing, encapsulation, pincers envelope process are realized by following steps:
Powder tank 1 is arranged on weighing system 2, the powder of vacuum pump set 18 and connection jacket 12 and transitional storehouse 6 is first turned on Flow flow speed control valve 1, powder mass flow flow speed control valve 2 19, powder mass flow flow speed control valve 3 20, are carried out to transitional storehouse 6, dress powder jacket 12 Vacuum suction, treat vacuum vacuum detecting instrument 14 detection vacuum reach technological requirement and gas analysis instrument 15 detection water, After hydrogen, oxygen content reach technological requirement, the powder mass flow flow speed control valve 2 19, powder mass flow for opening powder tank 1 and the connection of transitional storehouse 6 is adjusted Fast valve 3 20, powder flows into dress powder jacket 12 by transitional storehouse 6, and transitional storehouse 6 is provided with observation window 7 and is easy to observation powder stream emotionally Condition.Transitional storehouse 6 is provided with powder level detecting apparatus 5, if overflowing occurs in the powder of transitional storehouse 6, powder level detecting apparatus 5 send alarm Signal.Pipeline heating system 8 is arranged on the pipeline both sides that powder flows into transitional storehouse 6, and during powder is filled, convection current is through transitional storehouse 6 Powder carry out heating degasification.Powder during dress powder such as fruit powder tank 1 is inadequate, and weighing system 2 sends alarm signal, now more The powder tank for renewing;In order to avoid powder is blocked at vacuum pipe 10, vacuum pipe 10 is provided with tube wall vibration device 9 and is aided in Powder feeding.Powder in arrangement of powder jacket 12 load it is a certain amount of after, close powder mass flow flow speed control valve 2 19, powder mass flow flow speed control valve three 20, shaking platform 13 is now opened, shaking platform 13 is designed using three-dimensional vibrating, by top to bottom, left and right, front and rear to dress powder jacket 12 vibration realizing powder is in jacket middle-high density jolt ramming.After having been charged into the powder jolt ramming of jacket, powder mass flow tune is continued on Fast valve 3, realizes dress powder, the circulation work of vibration.Treat that powder charge weight reaches powder in the detection dress powder jacket of powder level detecting apparatus 27 After position requires height, hydraulic tongs seal apparatus 11 will fill the powder inlet of powder jacket 12 and be sealed.So far, whole technological process terminates.

Claims (10)

1. a kind of metal powder degassing, encapsulation, pincers seal integration apparatus, including powder tank(1), it is characterised in that powder tank(1)Pass through Powder mass flow flow speed control valve one(3), vacuum corrugated pipe one(4)With transitional storehouse(6)It is connected;Transitional storehouse(6)Bottom pass through vacuum tube Road one(10)With dress powder jacket(12)It is connected;Transitional storehouse(6)Right-hand member pass through filter(16)With vacuum valve(17)It is connected, very Empty valve and vacuum pump set(18)It is connected.
2. a kind of metal powder degassing according to claim 1, encapsulation, pincers seal integration apparatus, it is characterised in that described Powder tank(1)Bottom is equipped with weighing system(2).
3. a kind of metal powder degassing according to claim 1, encapsulation, pincers seal integration apparatus, it is characterised in that described Transitional storehouse(6)It is provided with observation panel(7), vacuum detecting instrument(14), gas analysis instrument(15), powder level detecting apparatus one (5)And pipeline heating system(8).
4. a kind of metal powder degassing according to claim 1, encapsulation, pincers seal integration apparatus, it is characterised in that described Vacuum pipe one(10)On by it is upper under be sequentially provided with powder mass flow flow speed control valve two(19), powder mass flow flow speed control valve three(20)、 Vacuum corrugated pipe two(21).
5. a kind of metal powder degassing according to claim 1, encapsulation, pincers seal integration apparatus, it is characterised in that described Vacuum pipe one(10)Tube wall on tube wall vibration device is installed(9).
6. a kind of metal powder degassing according to claim 1, encapsulation, pincers seal integration apparatus, it is characterised in that described Tube wall vibration device(9)With powder mass flow flow speed control valve three(20)Between vacuum pipe one(10)It is provided with powder level detecting apparatus two (24).
7. a kind of metal powder degassing according to claim 1, encapsulation, pincers seal integration apparatus, it is characterised in that described Dress powder jacket(12)Powder inlet be equipped with hydraulic tongs seal apparatus(11);Described dress powder jacket(12)It is flat that bottom is provided with vibration Platform(13).
8. a kind of metal powder degassing according to claim 1, encapsulation, pincers seal integration apparatus, it is characterised in that described Shaking platform(13)Designed using three-dimensional vibrating direction.
9. a kind of metal powder degassing according to claim 1, encapsulation, pincers seal integration apparatus, it is characterised in that described Vacuum valve(17)With vacuum pump set(18)Between be provided with vacuum pipe two(23);Vacuum pipe two(23)Centre is provided with one section very Empty bellows three(22).
10. a kind of metal powder degassing according to claim 9, encapsulation, pincers seal integration apparatus, it is characterised in that institute The vacuum pump set stated(18)Including one group of sliding vane rotary vacuum pump and one group of diffusion vacuum pump, working vacuum is 5 × 10-3Pa。
CN201710114614.6A 2017-02-28 2017-02-28 A kind of metal powder degassing, encapsulation, pincers envelope integration apparatus Active CN106903302B (en)

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CN201710114614.6A CN106903302B (en) 2017-02-28 2017-02-28 A kind of metal powder degassing, encapsulation, pincers envelope integration apparatus

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CN201710114614.6A CN106903302B (en) 2017-02-28 2017-02-28 A kind of metal powder degassing, encapsulation, pincers envelope integration apparatus

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107457400A (en) * 2017-08-24 2017-12-12 中国航发北京航空材料研究院 Vacuum thermal dynamic metal powder degassing device
CN108465810A (en) * 2018-06-05 2018-08-31 西安聚能装备技术有限公司 A kind of metal powder degassing encapsulation soldering and sealing device
CN108746597A (en) * 2018-08-03 2018-11-06 苏州振湖电炉有限公司 A kind of vacuum vibration densified device of aluminium titanium mother alloy powder
CN108817379A (en) * 2018-05-23 2018-11-16 航天材料及工艺研究所 A kind of powder metallurgy superalloy properties of product stability of improving fills out powder device
CN109865831A (en) * 2017-12-04 2019-06-11 北京有色金属研究总院 A kind of degasification method of particle enhanced aluminum-based composite material powder
CN114192773A (en) * 2021-10-21 2022-03-18 深圳市深汕特别合作区万泽精密科技有限公司 Automatic vacuum degassing method and device for metal powder
CN120480195A (en) * 2025-07-21 2025-08-15 西安欧中材料科技股份有限公司 Powder filling device of sheath for hot isostatic pressing and powder filling method and application thereof

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CN102398028A (en) * 2011-11-15 2012-04-04 中国航空工业集团公司北京航空材料研究院 Vacuum thermal dynamic metal powder degassing and canning method
CN103785846A (en) * 2014-01-23 2014-05-14 西安欧中材料科技有限公司 Method for preparing titanium alloy spherical powder at all levels

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US4515629A (en) * 1981-02-12 1985-05-07 United Technologies Corporation Degassing metal powder
EP2412461A2 (en) * 2010-07-30 2012-02-01 United Technologies Corporation Powder processing method
CN102127672A (en) * 2011-02-22 2011-07-20 中南大学 Method for preparing iron-base superalloy by extrusion forming of gas atomized powder
CN102189261A (en) * 2011-05-30 2011-09-21 华中科技大学 Densification method of porous workpiece
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Cited By (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107457400A (en) * 2017-08-24 2017-12-12 中国航发北京航空材料研究院 Vacuum thermal dynamic metal powder degassing device
CN109865831A (en) * 2017-12-04 2019-06-11 北京有色金属研究总院 A kind of degasification method of particle enhanced aluminum-based composite material powder
CN108817379A (en) * 2018-05-23 2018-11-16 航天材料及工艺研究所 A kind of powder metallurgy superalloy properties of product stability of improving fills out powder device
CN108465810A (en) * 2018-06-05 2018-08-31 西安聚能装备技术有限公司 A kind of metal powder degassing encapsulation soldering and sealing device
CN108465810B (en) * 2018-06-05 2024-03-05 西安聚能装备技术有限公司 Metal powder degasification dress cover seal welding device
CN108746597A (en) * 2018-08-03 2018-11-06 苏州振湖电炉有限公司 A kind of vacuum vibration densified device of aluminium titanium mother alloy powder
CN108746597B (en) * 2018-08-03 2024-02-20 苏州振湖电炉有限公司 A vacuum vibration densification processing device for aluminum-titanium master alloy powder
CN114192773A (en) * 2021-10-21 2022-03-18 深圳市深汕特别合作区万泽精密科技有限公司 Automatic vacuum degassing method and device for metal powder
CN114192773B (en) * 2021-10-21 2024-04-23 深圳市深汕特别合作区万泽精密科技有限公司 Automatic vacuum degassing method and device for metal powder
CN120480195A (en) * 2025-07-21 2025-08-15 西安欧中材料科技股份有限公司 Powder filling device of sheath for hot isostatic pressing and powder filling method and application thereof
CN120480195B (en) * 2025-07-21 2025-11-25 西安欧中材料科技股份有限公司 A powder loading device, powder loading method and application for hot isostatic pressing.

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