CN106852906A - Micron level Chinese medicine liquid extract preparation and preparation method thereof - Google Patents
Micron level Chinese medicine liquid extract preparation and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of micron level Chinese medicine liquid extract preparation and preparation method thereof, the method is identified Chinese medicine or herbal mixture, processed, being dried first, then precomminution is carried out, or again with superfine grinding methods such as Ultrasonic Pulverizations after extraction effective substance, granularity is ground into more than 1 micron and the particle less than 75 microns, plus auxiliary materials such as honey, with steps such as conventional method mixing, allotments, micron level Chinese medicine liquid extract preparation is made.Micron level Chinese medicine liquid extract preparation can improve bioavilability, keep pharmacodynamic substances basis, improve curative effect;Save Chinese material medicine resource；Be conducive to improving competitiveness of the Chinese medicine on world pharmaceutical market.
Description
Technical field
The present invention relates to Chinese medicine preparation and preparation method thereof, micron level Chinese medicine liquid extract preparation and preparation method thereof is more particularly to.
Background technology
Chinese medicine and its Chinese medicine preparation are traditional rarities of the Chinese nation, are that the prosperity of the Chinese nation has made indelible contribution.Chinese medicine liquid extract preparation is one kind of Chinese medicine preparation, is a kind of conventional Chinese medicine preparation easy to use.The processing of existing Chinese medicine liquid extract preparation is typically adopted with the following method, Chinese medicine or herbal mixture identification are carried out first, processed, are dried, then the crushing and extraction of conventional Chinese medicine or herbal mixture are carried out, then liquid extract preparation is made with conventional method mixing, allotment.The liquid extract preparation that this processing mode is made, the active ingredient availability that it is disadvantageous in that Chinese medicine or herbal mixture is low, and curative effect is not high, it is relatively slow to work, and usage amount is big, and insufficient is utilized to limited drug resource, the waste to some rare drug resources is particularly unfortunate.
Micron level Chinese medicine liquid extract preparation refers to pray for the liquid extract preparation that rice extracts are made with Chinese medicine micron extract or herbal mixture.
Chinese medicine micron extract refers to that the granularity of the extract obtained by the extracted effective substance of Chinese medicine is more than 1 micron and the Chinese medical extract less than 75 microns.
Herbal mixture micron extract refers to that the granularity of the extract obtained by the extracted effective substance of herbal mixture is more than 1 micron and the compound Chinese medicine extract less than 75 microns.
The content of the invention
The purpose of the present invention is made micron Chinese medicine stream and is soaked descendants' preparation with Chinese medicine micron extract or herbal mixture micron extract, and provides its preparation method.Micron Chinese medicine stream leaching descendants' preparation medicine composition is rapid-action, improves the absorptivity and curative effect of Chinese drugs, can reduce dose, and improve drug resource bioavilability.
In order to achieve the above object, the present invention is made micron level Chinese medicine liquid extract preparation, the following technical schemes of its preparation method Bian with Chinese medicine micron extract or herbal mixture micron extract：
Choose Chinese medicine or herbal mixture, it is first identified, process, dry, Chinese medicine micron extract or herbal mixture micron extract are ground into after extracted effective substance, along with water, sucrose or honey, by mixing, allotment, it is made micron level Chinese medicine liquid extract preparation.The present invention has following advantages compared with prior art：
1st, because the granularity of Chinese medicine micron extract or herbal mixture micron extract is more than 1 micron and less than 75 microns, particle diameter is not related to the aspect of atomic and molecular structure in this scope, so having substantially no effect on the original Chinese medicine attribute of effective substance, pharmacodynamic properties and curing mainly function, but this particle size range can make most of crude drug cell broken walls, therefore, micron level Chinese medicine liquid extract preparation can improve the availability of biology.
2nd, because the diffusion release rates of solid drugs are directly proportional to its area, and the granularity of Chinese medicine micron extract or herbal mixture micron extract is significantly smaller than existing Chinese medical extract, so as to greatly increased its surface area and drug solubility, therefore, the micron level Chinese medicine liquid extract preparation being made of Chinese medicine micron extract or herbal mixture micron extract, make the absorption of human body more convenient and rapid so that curative effect is higher, clinical therapeutic efficacy can be effectively improved.
3rd, the raising because of micron level Chinese medicine liquid extract preparation than traditional Chinese medicine liquid extract preparation effective substance availability, the usage amount of Chinese medicine can be reduced, the contradiction between growing Chinese medicine demand and tight market and resource is extenuated, limited Chinese material medicine resource is fully utilized.
4th, because micron Chinese medicine stream leaching descendants' preparation has above advantage, the surcharge of Chinese medicine is greatly improved, the Chinese material medicine resource of same amount is obtained more preferable economic benefit.
5th, same drug effect, micron level Chinese medicine liquid extract preparation amount capable of reducing using compared with traditional Chinese medicine stream leaching descendants' preparation, thus it is more easily accepted by people, it is more easy to enter international market, improve competitiveness of the traditional Chinese medicine in international market.
The preparation method of micron level Chinese medicine liquid extract preparation of the present invention is further described below.
Micron level Chinese medicine liquid extract preparation of the present invention has following 4 kinds of preparation methods, is now described respectively.
The first preparation method：
1st, Chinese medicine or herbal mixture identification are to confirm the true and false and quality of Chinese medicine or herbal mixture；
2nd, process is processed by the concocting method of traditional Chinese medicine；
3rd, drying is that the Chinese medicine or herbal mixture after processing are dried；
4th, precomminution is to being crushed with pulverizer by Chinese medicine or herbal mixture after the treatment of upper methods described, its granularity is reached 76 microns to 800 microns；
5th, extract is, by adding the water of solvent one or ethanol of 4 10 times of its weight, to filter method or circumfluence method using infusion process Huo Seepage or extraction extracts the effective substance of Chinese medicine or herbal mixture to the Chinese medicine or herbal mixture after precomminution；
6th, ultramicro grinding be with ball mill grinding, vibration crushings, Ultrasonic Pulverization, stirring crushing,
The breaking method of one of them is crushed in centrifugation, and Chinese medicinal material extract or compound Chinese medicine extract are made into Chinese medicine micron extract or herbal mixture of the granularity more than 1 micron and less than 75 microns prays for rice extracts；
7th, mixed by traditional handicraft, allocated, be made liquid extract preparation.
Second preparation method：
1st, Chinese medicine or herbal mixture identification are to confirm the true and false and quality of Chinese medicine or herbal mixture；
2nd, processing is processed by the concocting method of traditional Chinese medicine,
3rd, thousand it is dry be that the Chinese medicine or herbal mixture after processing are dried；
4th, extracting is to Chinese medicine or herbal mixture by adding the water of solvent one or ethanol of 4 10 times of its weight, and Bian infusion processes or Seepage filter method or circumfluence method or extraction extracts the effective substance of Chinese medicine or herbal mixture.
5th, ultramicro grinding is to be crushed with air-flow crushing, ball mill grinding, vibration crushing, Ultrasonic Pulverization, stirring, be centrifuged and crush the breaking method of one of them, and Chinese medicinal material extract or compound Chinese medicine extract are made into the granularity more than 1 micron and less than 75 microns；
6th, mixed by traditional handicraft, allocated, be made liquid extract preparation.
Specific embodiment
Embodiment 1
The preparation method of micron Xuanmai Ganju liquid extract preparation
1st, radix scrophulariae, the tuber of dwarf lilyturf, balloonflower root, the true and false of Radix Glycyrrhizae and quality are identified and is processed；Take radix scrophulariae 400g, the g of the tuber of dwarf lilyturf 400, Chinese parasol tree and obstruct 400 g, the g of Radix Glycyrrhizae 400;
2nd, dry；
3rd, 8000g water Bian is added to be extracted with infusion process；
4th, into clear descendants, relative density is 1.2-1.6 to Nong Shrink;
5th, Bian Ultrasonic Pulverizations, granularity is ground into more than 1 micron and less than 75 by extract
The extract of micron；
6th, Xuanmai Ganju micron extract is added into water, sucrose or honey, after mixing, is made the sweet Chinese parasol tree liquid extract preparation of the profound wheat of micron.
Embodiment 3
The preparation method of micron Sapporo U.S. arm liquid extract preparation
1st, the fleece-flower root, Radix Angelicae Sinensis, Psoralea corylifolia, the fruit of Chinese wolfberry, Semen Cuscutae, Poria cocos, the true and false of the root of bidentate achyranthes and quality are identified and is processed；Take fleece-flower root 640g, Radix Angelicae Sinensis 160g, Psoralea corylifolia（Fry）160g, fruit of Chinese wolfberry 160g, Semen Cuscutae (stir-fry) 160g, Poria cocos 160g, root of bidentate achyranthes 160g;
2nd, dry；
3rd, 8000g ethanol Bian is added to be extracted with circumfluence method；
4th, clear descendants are condensed into, relative density is 1.2-1.6;
5th, the method crushed using stirring, extract of the granularity more than 1 micron and less than 75 microns is ground into by extract；
6th, seven ingredient beard beautifying micron extract is added into water and sucrose or honey, after mixing, is made a micron seven ingredient beard beautifying liquid extract preparation.
Embodiment 4
The preparation method of the micron liquid extract preparation of XIANGSHALIUJUNZI
1st, the banksia rose, fructus amomi, Radix Codonopsis, the bighead atractylodes rhizome, Poria cocos, Radix Glycyrrhizae, dried orange peel, the true and false of the tuber of pinellia and quality are identified and is processed；Take banksia rose 70g, fructus amomi 76g, Radix Codonopsis 100g, the bighead atractylodes rhizome（Fry) 200g, Poria cocos 200g, Radix Glycyrrhizae（Process）70g, dried orange peel 76g, the tuber of pinellia（System）100g;
2nd, dry；
The 3rd, above-mentioned herbal mixture pulverizer is ground into 76 microns 800 microns of particle；
4th, plus 6000g ethanol Bian Yong Seepage filter method extraction；
5th, it is condensed into and educates clearly, relative density is 1.2-1.6;
6th, the method that Bian is crushed with vibration, extract of the granularity more than 1 micron and less than 75 microns is ground into by extract；
7th, the sub- micron extract of XIANGSHALIUJUNZI is added into water or sucrose or honey, stirring mixing is made the sub- liquid extract preparation of micron XIANGSHALIUJUNZI.
Embodiment 5
Pray for a meter preparation method for six drugs containing rehmanniae liquid extract preparation
1st, prepared rhizome of rehmannia, Fructus Corni, moutan bark, Chinese yam, Poria cocos, the true and false of rhizoma alismatis and quality are identified and is processed；Take prepared rhizome of rehmannia 160g, Fructus Corni（System）76g, moutan bark 60g, Chinese yam 76g, Fu Hui 60g, the thirsty 60g in pool；
2nd, dry；
The 3rd, above-mentioned herbal mixture pulverizer is ground into 76 microns 800 microns of particle；
4th, medium is made with COa, is extracted with supercritical fluid extraction, obtain granularity more than 1 micron and the extract less than 75 microns；
5th, six drugs containing rehmanniae micron extract is added into water and sucrose or honey, is made and prays for meter six drugs containing rehmanniae stream leaching descendants' preparation.
Embodiment 6
The preparation method of micron tonifying middle-Jiao and Qi liquid extract preparation
1st, the Radix Astragali, Radix Codonopsis, Radix Glycyrrhizae, the bighead atractylodes rhizome, Radix Angelicae Sinensis, rattletop, radix bupleuri, the true and false of dried orange peel and quality are identified and is processed；Take the Radix Astragali（Process）200g, Radix Codonopsis 60g, Radix Glycyrrhizae（Process）100g, the bighead atractylodes rhizome（Fry）60g, Radix Angelicae Sinensis 60g, rattletop 60g, radix bupleuri 60g, dried orange peel 60g;
2nd, dry；
3rd, medium is made with C02, is extracted with supercritical fluid extraction, obtain granularity more than 1 micron and the extract less than 75 microns；
4th, tonifying middle-Jiao and Qi micron extract is added into water and sucrose or honey, is made a micron tonifying middle-Jiao and Qi liquid extract preparation.
Embodiment 7
The preparation method of micron five Siberian cockleburs stream leaching descendants' preparation
1st, Poria cocos, rhizoma alismatis, umbellate pore furgus, Chinese cassia tree, the true and false of the bighead atractylodes rhizome and quality are identified and is processed；Take Poria cocos 60g, rhizoma alismatis 300g, umbellate pore furgus 176g, Chinese cassia tree 120g, the bighead atractylodes rhizome（Fry）176g；
2nd, dry；
3rd, above-mentioned herbal mixture is crushed with pulverizer, is made its granularity between 76 microns 800 microns；
4th, add the water of 8400g, extracted using infusion process；
5th, clear cream is condensed into, relative density is 1.2-1.6;
6th, the method that Bian ball mill grindings and centrifugation are crushed, extract of the granularity more than 1 micron and less than 75 microns is ground into by extract；
7th, micron Wu Cutters extracts are added into water and sucrose or honey, after agitated mixing, is made the Siberian cocklebur liquid extract preparation of micron five.
Embodiment 8
The preparation method of micron returns spleen liquid extract preparation
1st, Radix Codonopsis, the bighead atractylodes rhizome, the Radix Astragali, Radix Glycyrrhizae, Poria cocos, polygala, spina date seed, arillus longan, Radix Angelicae Sinensis, the banksia rose, the true and false of date and quality are identified and is processed；Take Radix Codonopsis 76g, the bighead atractylodes rhizome（Fry) 160g, the Radix Astragali（Process）76g, Radix Glycyrrhizae（Process）40g, Poria cocos 160g, polygala（System）160g, spina date seed（Fry）76g, arillus longan 160g, Radix Angelicae Sinensis 160g, banksia rose 40g, date（Stoning）40g;
2nd, dry；
3rd, above-mentioned herbal mixture is crushed with pulverizer, is made its granularity between 76 microns 800 microns；
4th, add the water of 6000g, extracted using circumfluence method；
5th, clear descendants are condensed into, relative density is 1.2-1.6；
6th, the method crushed using stirring, the extract that granularity prays for rice more than 1 micron and less than 75 is ground into by extract；
7th, micron returns spleen extract is added into water or sucrose or honey, after stirring mixing, is made and prays for meter blue or green preparation of returns spleen stream leaching.
Embodiment 9
The preparation method of the instant raw arteries and veins liquid extract preparation of micron
1st, identification ginseng, winter wheat, the true and false and quality of the fruit of Chinese magnoliavine；Take ginseng 100g, winter wheat 200g, fruit of Chinese magnoliavine 100g；
2nd, process；
3rd, dry；
4th, crushed with pulverizer, made its granularity between 76 microns 800 microns；
5th, Bian makees medium to CQ, with supercritical liquid extraction technique, by ginseng, winter wheat,
Fructus Schisandrae Chinensis powder is broken into granularity more than 1 micron and the extract less than 75 microns；
6th, micron life arteries and veins extract is added into water and sucrose or honey, after stirring mixing, is made
The instant raw arteries and veins liquid extract preparation of micron.
Embodiment 10
The preparation method of micron five tastes sea-buckthorn liquid extract preparation
1st, dry sea-buckthorn high, the banksia rose, white grape, Radix Glycyrrhizae, the true and false and quality of cape jasmine are identified；
Take sea-buckthorn 176g high, banksia rose 150g, white grape dry 120g, Radix Glycyrrhizae 90g, Gardenia 60g;
2nd, process；
3rd, dry；
4th, the ethanol of 1800g is added, Bian is extracted with circumfluence method；
5th, clear cream, drying that relative density is 1.20 1.50 are condensed into；
6th, the method for Bian air-flow crushings, is ground into granularity more than 1 micron and small by extract
In 75 microns of extract；
7th, the micron extract of five tastes sea-buckthorn is pelletized plus lactose and dextrin with spray granulation；
8th, whole grain, total mixed, is made a micron five tastes sea-buckthorn liquid extract preparation.
Claims (5)
1. a kind of micron level Chinese medicine liquid extract preparation, is that the middle medical abortion being made up of Chinese medical extract is soaked
Paste formulation, it is characterised in that micron level Chinese medicine liquid extract preparation is made of Chinese medicine micron extract or herbal mixture micron extract.
2. a kind of preparation side of the micron level Chinese medicine liquid extract preparation realized described in claim 1
Method, it is characterised in that the preparation method follow these steps to order to be carried out：
The identification of a, Chinese medicine or herbal mixture, processing, drying；
B, crushed with pulverizer, make its granularity be 76 microns to 800 microns；
C, the water of solvent one or ethanol that add 4 10 times of its weight；
D, Bian infusion process Huo Seepage filter method or circumfluence method or extraction extracts effective substance；
E, extract ball mill grinding, vibration crushings, Ultrasonic Pulverization, stirring are crushed, one of them breaking method is crushed in centrifugation, be ground into granularity and be more than 1 micron and less than 75 microns
Particle；
F, plus water, sucrose or honey；
G, with conventional method mix, allotment, be made liquid extract preparation.
3. a kind of preparation side of the micron level Chinese medicine liquid extract preparation realized described in claim 1
Method, it is characterised in that the preparation method follow these steps to order to be carried out：
The identification of a, Chinese medicine or herbal mixture, processing, drying；
B, the water of solvent one or ethanol that add 4 10 times of its weight；
C, Bian infusion process or percolation or circumfluence method or extraction extraction effective substance；
D, by extract ball mill grinding, vibration crushings, Ultrasonic Pulverization, stirring crushing, from
The heart crushes the breaking method of one of them, is ground into granularity more than 1 micron and less than 75 microns
Particle；
E, plus water, sucrose or honey；
F, with conventional method mix, allotment, be made liquid extract preparation.
4. a kind of preparation side of the micron level Chinese medicine liquid extract preparation realized described in claim 1
Method, it is characterised in that the preparation method follow these steps to order to be carried out：
The identification of a, Chinese medicine or herbal mixture, processing, drying；
B, crushed with pulverizer, make its granularity be 76 microns to 800 microns；
C, supercritical fluid extraction is carried out by the C02 of medium one or inert gas, obtain granularity
Chinese medicine or herbal mixture micron extract more than 1 micron and less than 75 microns；
D, plus water, sucrose or honey；
E, with conventional method mix, allotment, be made liquid extract preparation.
5. a kind of preparation side of the micron level Chinese medicine liquid extract preparation realized described in claim 1
Method, it is characterised in that the preparation method follow these steps to order to be carried out：
The identification of a, Chinese medicine or herbal mixture, processing, drying；
B, supercritical fluid extraction is carried out by the C02 of medium one or inert gas, obtain granularity
Chinese medicine or herbal mixture micron extract more than 1 micron and less than 75 microns；
C, plus water, sucrose or honey；
D, with conventional method mix, allotment, be made liquid extract preparation.
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| CN108926591A (en) * | 2018-08-08 | 2018-12-04 | 舒城县健康家庭农场 | A kind of processing method and its application of Radix Astragali micropowder |
| CN117100798A (en) * | 2023-07-10 | 2023-11-24 | 湖南中医药大学 | Soybean milk powder for replenishing qi and relieving asthma, preparation process and application thereof |
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2015
- 2015-12-08 CN CN201510893051.6A patent/CN106852906A/en active Pending
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108926591A (en) * | 2018-08-08 | 2018-12-04 | 舒城县健康家庭农场 | A kind of processing method and its application of Radix Astragali micropowder |
| CN117100798A (en) * | 2023-07-10 | 2023-11-24 | 湖南中医药大学 | Soybean milk powder for replenishing qi and relieving asthma, preparation process and application thereof |
| CN117100798B (en) * | 2023-07-10 | 2025-04-08 | 湖南中医药大学 | Qi-tonifying asthma-relieving soybean milk powder, preparation process and application thereof |
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Application publication date: 20170616 |