CN106837317A - Tight reservoir oil charging simulation method and system - Google Patents
Tight reservoir oil charging simulation method and system Download PDFInfo
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Abstract
Description
技术领域technical field
本发明涉及石油勘探开发领域,特别涉及一种致密储层石油充注模拟方法及系统。The invention relates to the field of petroleum exploration and development, in particular to a tight reservoir petroleum charging simulation method and system.
背景技术Background technique
致密储层具有岩性致密、低孔低渗透率、气藏压力系数低、自然产能低等特点,其作为一种非常规储层,具有较大的开发难度和要求。目前,尽管通过水平井和体积压裂实现了致密油的一定的开发。但由于致密储层内发育不同于常规储层的微米—纳米级孔喉,其微纳米孔喉内原油的充注、运移和聚集机理仍不清楚,一定程度上限制了致密储层的勘探开发。Tight reservoirs have the characteristics of tight lithology, low porosity and low permeability, low gas reservoir pressure coefficient, and low natural productivity. As an unconventional reservoir, it has great development difficulties and requirements. At present, although tight oil has been developed to a certain extent through horizontal wells and volume fracturing. However, due to the development of micro-nano pore throats in tight reservoirs that are different from conventional reservoirs, the mechanism of crude oil charging, migration and accumulation in micro-nano pore throats is still unclear, which limits the exploration of tight reservoirs to a certain extent. develop.
目前,国内现有的研究及其对应的模拟实验和模拟装置主要针对常规储层设计,通常含有一个供液系统,通过高压泵入原油研究油气在储集岩心中的成藏过程。事实上,烃源岩生烃模拟研究表明烃源岩生烃模拟产物中不仅仅生成原油,还含H2O、H2、CO2以及轻烃等气体。而生成的水和气体对原油的充注和成藏影响巨大。特别是致密储层,使用传统的高压泵入流体方法,基本上不能实现致密储层原油的有效聚集;而且,目前的模拟常用的供液体系很难完全模拟烃源岩生成的原油及其组成,因此,针对致密储层需要提供新的方法和设备,实现模拟烃源岩生成的石油及其组成,以指导致密储层的勘探开发。At present, the existing domestic research and its corresponding simulation experiments and simulation devices are mainly designed for conventional reservoirs, usually including a liquid supply system, through which crude oil is pumped under high pressure to study the accumulation process of oil and gas in the reservoir core. In fact, the hydrocarbon generation simulation studies of source rocks show that not only crude oil is produced in the hydrocarbon generation simulation products of source rocks, but also gases such as H 2 O, H 2 , CO 2 and light hydrocarbons. The generated water and gas have a great impact on the charging and accumulation of crude oil. Especially in tight reservoirs, using the traditional high-pressure pumping fluid method basically cannot realize the effective accumulation of crude oil in tight reservoirs; moreover, it is difficult to completely simulate the crude oil generated by source rocks and its composition in the current liquid supply system commonly used for simulation Therefore, it is necessary to provide new methods and equipment for tight reservoirs to simulate the oil and its composition generated by source rocks, so as to guide the exploration and development of tight reservoirs.
发明内容Contents of the invention
本发明的目的是提供一种致密储层石油充注模拟方法及系统,能够真实模拟烃源岩生成的原油及其组成,以指导致密储层的勘探开发。The purpose of the present invention is to provide a tight reservoir oil filling simulation method and system, which can truly simulate the crude oil and its composition generated by source rocks, so as to guide the exploration and development of tight reservoirs.
本发明的上述目的可采用下列技术方案来实现:Above-mentioned purpose of the present invention can adopt following technical scheme to realize:
一种致密储层石油充注模拟方法,包括:A method for simulating oil charging in tight reservoirs, comprising:
分别获取与致密储层对应的第一样品和与目标烃源岩对应的第二样品;Obtaining a first sample corresponding to the tight reservoir and a second sample corresponding to the target source rock respectively;
对所述第一样品进行预处理并进行覆压物性测定和注地层水,获取第一资料;Pretreating the first sample and measuring the physical properties of the overburden and injecting formation water to obtain the first data;
对所述第二样品进行总有机碳、热解和成熟度测定,对成熟度低于预定值的第二样品进行开放体系的生烃动力学测试,获取第二资料;performing total organic carbon, pyrolysis, and maturity measurements on the second sample, and performing an open-system hydrocarbon generation kinetics test on the second sample whose maturity is lower than a predetermined value, to obtain second information;
根据测井资料、所述第一资料和第二资料确定所述致密储层的源储配制关系,并根据所述源储配制关系装填第一样品和第二样品,获得装填后的模拟样品;Determine the source-reservoir preparation relationship of the tight reservoir according to the logging data, the first data and the second data, and fill the first sample and the second sample according to the source-reservoir preparation relationship to obtain a simulated sample after filling ;
根据地层埋藏史和热史,现今地层温度和压力,对所述模拟样品进行地质过程约束模拟实验;According to the burial history and thermal history of the formation, the current formation temperature and pressure, carry out a geological process constraint simulation experiment on the simulated sample;
对所述模拟样品进行石油分布测定,确定石油分布情况。Oil distribution measurement is carried out on the simulated sample to determine the oil distribution.
在优选的实施方式中,所述成熟度低于预定值的第二样品为成熟度低于0.6%的样品。In a preferred embodiment, the second sample with a maturity lower than a predetermined value is a sample with a maturity lower than 0.6%.
在优选的实施方式中,所述第二资料包括:活化能和指前因子。In a preferred embodiment, the second data includes: activation energy and pre-exponential factor.
在优选的实施方式中,所述第二资料由:通过不少于两组不同加热速率的测试获取不少于两组产烃曲线,并依据阿伦尼乌斯方程计算得到。In a preferred embodiment, the second data is obtained by obtaining no less than two sets of hydrocarbon production curves through no less than two sets of tests with different heating rates, and calculating according to the Arrhenius equation.
在优选的实施方式中,所述石油分布测定的方法包括下述中的任意一种:In a preferred embodiment, the method for determining the distribution of oil comprises any one of the following:
拉曼光谱、热解分析和核磁共振法。Raman spectroscopy, pyrolysis analysis and NMR.
在优选的实施方式中,所述致密储层的地层渗透率小于0.1毫达西;In a preferred embodiment, the formation permeability of the tight reservoir is less than 0.1 mD;
相应的,对所述第一样品进行预处理包括:对所述第一样品进行洗油处理,至洗油液体不再有荧光。Correspondingly, performing pretreatment on the first sample includes: performing oil washing treatment on the first sample until the oil washing liquid no longer has fluorescence.
在优选的实施方式中,所述源储配置关系包括:In a preferred embodiment, the source-storage configuration relationship includes:
下生上储型、上生下储型和夹层型。Bottom-born and upper-storage type, upper-growth and lower-storage type, and interlayer type.
在优选的实施方式中,对所述模拟样品进行地质过程约束模拟实验中,所述约束包括升温速率。In a preferred embodiment, when performing a geological process constraint simulation experiment on the simulated sample, the constraint includes a heating rate.
在优选的实施方式中,对所述第二样品进行总有机碳、热解和成熟度测定前,还包括:将所述第二样品粉碎处理,粉碎至预定目数。In a preferred embodiment, before performing total organic carbon, pyrolysis and maturity determination on the second sample, it further includes: pulverizing the second sample to a predetermined mesh size.
一种致密储层石油充注模拟系统,包括:A tight reservoir oil charging simulation system, including:
温度压力装置,用于提供模拟实验过程中的温度和压力;The temperature and pressure device is used to provide the temperature and pressure during the simulation experiment;
流体供排装置,其包括供液管线设备、收液管线设备及自密封和开启阀门;Fluid supply and discharge devices, including liquid supply pipeline equipment, liquid collection pipeline equipment and self-sealing and opening valves;
设备监测装置,用于设定实验过程中的升温速率、升压速率以及监测装置内温度压力;The equipment monitoring device is used to set the heating rate and pressure increasing rate and monitor the temperature and pressure in the device during the experiment;
含油测定装置,用于测定石油的分布情况。The oil content measuring device is used to measure the distribution of oil.
在优选的实施方式中,所述温度压力装置包括加热设备和油压设备,其中,所述加热设备能达到的最高温度为550摄氏度,所述油压设备能达到的最大压力为70兆帕。In a preferred embodiment, the temperature and pressure device includes a heating device and an oil pressure device, wherein the maximum temperature that the heating device can reach is 550 degrees Celsius, and the maximum pressure that the oil pressure device can reach is 70 MPa.
本发明的特点和优点是:通过温度压力装置、流体供排装置、设备监测装置、含油监测装置,针对致密储层开展石油充注成藏研究,操作简单、符合实际,重复性好、且能定量评价。相比传统的测方法,本发明可以实现生烃与致密储层石油充注一体化、更符合地质情况,能够真实模拟烃源岩生成的石油及其组成。The characteristics and advantages of the present invention are: through temperature and pressure devices, fluid supply and discharge devices, equipment monitoring devices, and oil monitoring devices, research on oil filling and accumulation in tight reservoirs is simple, practical, repeatable, and capable of Quantitative evaluation. Compared with the traditional measurement method, the present invention can realize the integration of hydrocarbon generation and tight reservoir oil charging, is more in line with geological conditions, and can truly simulate the oil generated by source rocks and its composition.
附图说明Description of drawings
图1是本申请实施方式中一种致密储层石油充注模拟方法的步骤流程图;Fig. 1 is a flow chart of the steps of a tight reservoir oil filling simulation method in the embodiment of the present application;
图2是本申请实施方式中一种致密储层石油充注模拟系统的结构示意图;Fig. 2 is a structural schematic diagram of a tight reservoir oil filling simulation system in the embodiment of the present application;
图3是本申请一种依据致密储层石油充注模拟方法进行模拟实验后获得的生烃量转换率-温度的曲线图;Fig. 3 is a graph of conversion rate-temperature of hydrocarbon generation amount obtained after a simulation experiment based on the tight reservoir oil charging simulation method of the present application;
图4是本申请一种依据致密储层石油充注模拟方法进行模拟实验后获得的生烃量-温度的曲线图;Fig. 4 is a curve diagram of hydrocarbon generation amount-temperature obtained after a simulation experiment is carried out according to the tight reservoir oil charging simulation method of the present application;
图5是本申请一种依据致密储层石油充注模拟方法进行模拟实验后获得的生烃量分布-活化能分布的柱状图;Fig. 5 is a histogram of hydrocarbon generation distribution-activation energy distribution obtained after a simulation experiment based on the tight reservoir oil charging simulation method of the present application;
图6是致密储层的源储配制关系为底生型岩心高度-含油饱和度的曲线图;Fig. 6 is a graph showing that the source-reservoir configuration relationship of tight reservoirs is bottom-grown core height-oil saturation;
图7是致密储层的源储配制关系为夹层型岩心高度-含油饱和度的曲线图;Fig. 7 is a graph showing that the source-reservoir configuration relationship of tight reservoirs is interlayer core height-oil saturation;
图8是致密储层的源储配制关系为顶生型岩心高度-含油饱和度的曲线图。Fig. 8 is a graph showing the source-reservoir configuration relationship of tight reservoirs as the top-grown core height-oil saturation.
具体实施方式detailed description
下面将结合附图和具体实施方式,对本发明的技术方案作详细说明,应理解这些实施方式仅用于说明本发明而不用于限制本发明的范围,在阅读了本发明之后,本领域技术人员对本发明的各种等价形式的修改均落入本申请所附权利要求所限定的范围内。The technical solution of the present invention will be described in detail below in conjunction with the accompanying drawings and specific embodiments. It should be understood that these embodiments are only used to illustrate the present invention and are not intended to limit the scope of the present invention. After reading the present invention, those skilled in the art Modifications to various equivalent forms of the present invention fall within the scope defined by the appended claims of the present application.
下面结合附图对本申请所述的致密储层石油充注模拟方法及系统进行详细的说明。图1是本申请一个实施方式提供的致密储层石油充注模拟方法的流程图。虽然本申请提供了如下述实施方式或附图所示的方法操作步骤或装置结构,但基于常规或者无需创造性的劳动在所述方法或装置中可以包括更多或者更少的操作步骤或模块结构。在逻辑性上不存在必要因果关系的步骤或结构中,这些步骤的执行顺序或装置的模块结构不限于本申请实施方式提供的执行顺序或模块结构。所述的方法或模块结构的在实际中的装置或终端产品执行时,可以按照实施方式或者附图所示的方法或模块结构连接进行顺序执行或者并行执行(例如并行处理器或者多线程处理的环境)。The method and system for simulating oil filling in tight reservoirs described in this application will be described in detail below with reference to the accompanying drawings. Fig. 1 is a flow chart of a method for simulating oil charging in tight reservoirs provided by an embodiment of the present application. Although the present application provides the method operation steps or device structure as shown in the following embodiments or drawings, more or less operation steps or module structures may be included in the method or device based on conventional or creative work . In steps or structures that do not logically have a necessary causal relationship, the execution order of these steps or the modular structure of the device is not limited to the execution order or modular structure provided in the embodiments of the present application. When the described method or module structure is executed in an actual device or terminal product, it can be executed sequentially or in parallel according to the method or module structure connection shown in the implementation mode or drawings (such as parallel processor or multi-threaded processing) environment).
除非另有定义,本文所使用的所有的技术和科学术语与属于本申请的技术领域的技术人员通常理解的含义相同。本文中在本申请的说明书中所使用的术语只是为了描述具体的实施方式的目的,不是旨在于限制本申请。Unless otherwise defined, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the technical field to which this application belongs. The terminology used herein in the description of the application is only for the purpose of describing specific embodiments, and is not intended to limit the application.
需要说明的是,当元件被称为“设置于”另一个元件,它可以直接在另一个元件上或者也可以存在居中的元件。当一个元件被认为是“连接”另一个元件,它可以是直接连接到另一个元件或者可能同时存在居中元件。本文所使用的术语“垂直的”、“水平的”、“上”、“下”、“左”、“右”以及类似的表述只是为了说明的目的,并不表示是唯一的实施方式。It should be noted that when an element is referred to as being “disposed on” another element, it may be directly on the other element or there may also be an intervening element. When an element is referred to as being "connected to" another element, it can be directly connected to the other element or intervening elements may also be present. As used herein, the terms "vertical", "horizontal", "upper", "lower", "left", "right" and similar expressions are for the purpose of illustration only and are not intended to represent the only embodiment.
本发明提供一种致密储层石油充注模拟方法及装置,能够真实模拟烃源岩生成的原油及其组成。The invention provides a method and device for simulating oil filling in tight reservoirs, which can truly simulate crude oil generated by source rocks and its composition.
请参阅图1,本申请实施方式中提供的一种致密储层石油充注模拟方法可以包括如下步骤。Please refer to FIG. 1 , a method for simulating oil filling in tight reservoirs provided in an embodiment of the present application may include the following steps.
步骤S10:分别获取与致密储层对应的第一样品和与目标烃源岩对应的第二样品;Step S10: acquiring a first sample corresponding to the tight reservoir and a second sample corresponding to the target source rock;
步骤S11:对所述第一样品进行预处理并进行覆压物性测定和注地层水,获取第一资料;Step S11: performing pretreatment on the first sample and measuring the physical properties of the overburden and injecting formation water to obtain the first data;
步骤S12:对所述第二样品进行总有机碳、热解和成熟度测定,对成熟度低于预定值的第二样品进行开放体系的生烃动力学测试,获取第二资料;Step S12: performing total organic carbon, pyrolysis, and maturity measurements on the second sample, and performing an open-system hydrocarbon generation kinetics test on the second sample whose maturity is lower than a predetermined value, to obtain second data;
步骤S13:根据测井资料、所述第一资料和第二资料确定所述致密储层的源储配制关系,并根据所述源储配制关系装填第一样品和第二样品,获得装填后的模拟样品;Step S13: Determine the source-storage composition relationship of the tight reservoir according to the logging data, the first data and the second data, and fill the first sample and the second sample according to the source-storage composition relationship, and obtain the filled simulated sample;
步骤S14:根据地层埋藏史和热史,现今地层温度和压力,对所述模拟样品进行地质过程约束模拟实验;Step S14: According to the burial history and thermal history of the formation, the current formation temperature and pressure, conduct a geological process constraint simulation experiment on the simulated sample;
步骤S15:对所述模拟样品进行石油分布测定,确定石油分布情况。Step S15: Carry out oil distribution measurement on the simulated sample to determine the oil distribution.
在本实施方式中,研究的对象为致密储层,具体的,该致密储层的地层渗透率可以小于0.1毫达西。In this embodiment, the research object is a tight reservoir, specifically, the formation permeability of the tight reservoir may be less than 0.1 mD.
在本实施方式中,在进行模拟实验前需要分别获取致密储层对应的第一样品和目标烃源岩对应的第二样品。In this embodiment, before performing the simulation experiment, the first sample corresponding to the tight reservoir and the second sample corresponding to the target source rock need to be obtained respectively.
其中,获取第一样品时,可以依据目标区域如盆地的盆地露头、测井资料和地震资料等资料,采集该致密储层预定位置的岩心,钻取柱塞状的样品,从而获得所述第一样品。Wherein, when obtaining the first sample, it is possible to collect the core at the predetermined position of the tight reservoir according to the data of the target area such as basin outcrop, logging data and seismic data, etc., and drill a plunger-shaped sample, thereby obtaining the described first sample.
然后,对该第一样品进行预处理。具体的,该预处理可以包括对所述第一样品进行洗油处理,至洗油液体不再有荧光。接着,可以将预处理后的第一样品进行晾干。接下来,可以对预处理后的第一样品开展覆压物性测试,并将其充满地层水,模拟第一样品处于真实的地层环境中。其中,所述第一资料可以包括:覆压孔隙度、渗透率等参数。Then, the first sample is pretreated. Specifically, the pretreatment may include washing the first sample with oil until the oil washing liquid no longer has fluorescence. Next, the pretreated first sample can be dried. Next, the overburden physical property test can be carried out on the pretreated first sample, which is filled with formation water, simulating that the first sample is in a real formation environment. Wherein, the first data may include parameters such as overburden porosity and permeability.
在本实施方式中,获取第二样品时,可以采集目标区域,如盆地典型的低成熟度源岩,将其粉碎至预定目数,然后进行总有机碳、热解和成熟度测定,对成熟度低于预定值的第二样品进行开放体系的生烃动力学测试,获取第二样品对应的第二资料。In this embodiment, when obtaining the second sample, the target area can be collected, such as the typical low-maturity source rock in the basin, crushed to a predetermined mesh, and then carried out for total organic carbon, pyrolysis and maturity measurement. The second sample whose degree is lower than the predetermined value is subjected to the hydrocarbon generation kinetics test of the open system to obtain the second data corresponding to the second sample.
其中,所述低成熟度源岩具体可以为成熟度低于0.6%的烃源岩。所述烃源岩(source rock)也叫生油岩,富含有机质、大量生成油气与排出油气的岩石。也就是说烃源岩是一种能够产生或已经产生可移动烃类的岩石。所述第二样品获取时,可以为柱状或者块状等形状,具体的本申请在此并不作具体的限定。当需要进行参数测定时,可以将获取的样品粉碎至预定目数。该预定目数具体可以根据地球化学分析测试所需样品要求而定,例如可以为200目等,具体的,本申请在此并不作具体的限定。Wherein, the low-maturity source rock may specifically be a source rock with a maturity lower than 0.6%. The source rock (source rock) is also called oil source rock, which is a rock that is rich in organic matter and produces and discharges oil and gas in large quantities. That is to say, a source rock is a rock that can produce or has produced mobile hydrocarbons. When the second sample is obtained, it may be in the shape of a column or a block, which is not specifically limited in this application. When parameter determination is required, the obtained sample can be pulverized to a predetermined mesh. The predetermined mesh number can be specifically determined according to the sample requirements for geochemical analysis and testing, for example, it can be 200 mesh, etc. Specifically, this application does not specifically limit it here.
在具体测定时,可以利用碳硫仪,热解仪和显微镜分别测试总有机碳(TOC totalorganic carbon),生烃潜量和成熟度(Ro)。当然,还可以利用现有的其他仪器进行测定,本申请在此并不作具体的限定。In the specific measurement, the total organic carbon (TOC total organic carbon), hydrocarbon generation potential and maturity (Ro) can be tested respectively by using a carbon-sulfur analyzer, a pyrolysis analyzer and a microscope. Of course, other existing instruments can also be used for measurement, and this application does not make specific limitations here.
其中,生烃潜量指某一体积或某一重量烃源岩中有机质,在自然地质条件下可以生成烃类物质的最大数量。它包括至今已生成的烃量和尚未转化的剩余生烃潜量两部分。其基本单位为公斤(kg)或吨(t)或立方米(m3)。有机碳是指岩石中存在于有机物中的碳。它不包括碳酸盐岩、石墨中的碳。通常用岩石质量的百分比来表示。从原理上讲,岩石中有机质的量还应该包括H、O、N、S等所有存在于有机质中的元素的总量。Among them, hydrocarbon generation potential refers to the maximum amount of organic matter in a certain volume or weight of source rock that can generate hydrocarbons under natural geological conditions. It includes two parts: the amount of hydrocarbons that have been generated so far and the remaining hydrocarbon generation potential that has not been converted. Its basic unit is kilogram (kg) or ton (t) or cubic meter (m 3 ). Organic carbon refers to the carbon present in organic matter in rocks. It does not include carbon in carbonate rocks, graphite. Usually expressed as a percentage of rock mass. In principle, the amount of organic matter in rocks should also include the total amount of all elements present in organic matter, such as H, O, N, and S.
在本实施方式中,可以选择低成熟度烃源岩样品进行开放体系的生烃动力学分析测试,获取第二资料。具体的,该第二资料可以包括:活化能(Ea)和指前因子(A)。其中,所述活化能是指分子从常态转变为容易发生化学反应的活跃状态所需要的能量称为活化能。(阿伦尼乌斯公式中的活化能区别于由动力学推导出来的活化能,又称阿伦尼乌斯活化能或经验活化能)活化分子的平均能量与反应物分子平均能量的差值即为活化能。所述指前因子A来源于阿伦尼乌斯公式k=A·exp(-Ea/RT)中,k、R、T、Ea分别是化学反应速率常数、摩尔气体常数、反应温度及活化能,式中的A称为指前因子。它是一个只由反应本性决定而与反应温度及系统中物质浓度无关的常数,与k具有相同的量纲。A是反应的重要动力学参量之一。具体的,所述第二资料可以由:通过不少于两组不同加热速率的测试获取不少于两组产烃曲线,并依据阿伦尼乌斯方程计算得到。In this embodiment, low-maturity source rock samples may be selected for open-system hydrocarbon generation kinetics analysis and testing to obtain second data. Specifically, the second data may include: activation energy (Ea) and pre-exponential factor (A). Wherein, the activation energy refers to the energy required for a molecule to change from a normal state to an active state where chemical reactions are likely to occur, which is called activation energy. (The activation energy in the Arrhenius formula is different from the activation energy derived from kinetics, also known as Arrhenius activation energy or empirical activation energy) The difference between the average energy of activated molecules and the average energy of reactant molecules is the activation energy. The pre-exponential factor A is derived from the Arrhenius formula k=A·exp(-Ea/RT), k, R, T, Ea are respectively the chemical reaction rate constant, the molar gas constant, the reaction temperature and the activation energy , where A is called the pre-exponential factor. It is a constant determined only by the nature of the reaction and has nothing to do with the reaction temperature and the concentration of substances in the system, and has the same dimension as k. A is one of the important kinetic parameters of the reaction. Specifically, the second data can be obtained by: obtaining no less than two sets of hydrocarbon production curves through no less than two sets of tests with different heating rates, and calculating according to the Arrhenius equation.
在本实施方式中可以根据测井资料以及岩心样品资料包括所述第一资料、第二资料,确定所述致密储层的源储配制关系,并根据所述源储配制关系获取模拟样品。具体的,所述源储配置关系指源岩与储层的位置关系,可以包括:下生上储型、上生下储型和夹层型,即源岩在下储层在上、源岩在上储层在下、源岩和储层混层。然后,根据所述源储配制关系获取模拟样品具体可以为按照所述源储配制关系装填第一样品和第二样品,获取所述模拟样品。In this embodiment, the source-reservoir configuration relationship of the tight reservoir can be determined according to the logging data and core sample data including the first data and the second data, and simulated samples can be obtained according to the source-reservoir configuration relationship. Specifically, the source-reservoir configuration relationship refers to the positional relationship between the source rock and the reservoir, which may include: lower-generation upper-reservoir type, upper-generation lower-reservoir type, and interlayer type, that is, the source rock is on the lower reservoir layer, and the source rock is on the upper layer. Reservoir is below, mixed source rock and reservoir. Then, obtaining the simulated sample according to the source-storage preparation relationship may specifically be filling the first sample and the second sample according to the source-storage preparation relationship, and obtaining the simulation sample.
在本实施方式中,当获取所述模拟样品后,可以根据地层埋藏史和热史,现今地层温度和压力,对所述模拟样品进行地质过程约束模拟实验。In this embodiment, after the simulated sample is obtained, a geological process constraint simulation experiment can be performed on the simulated sample according to the burial history and thermal history of the formation, and the current formation temperature and pressure.
沉积盆地的热历史主要取决于两个方面,一是盆地基底热流密度的变化,二是盆地内部沉积物的性质及埋藏历史。由于不同类型的地球动力学背景和形成机制不同,描述不同类型沉积盆地构造演化的地球动力学模型也不相同。在进行模拟实验前,可以根据目标研究盆地的地层埋藏史和热史确定相应的模型。The thermal history of a sedimentary basin mainly depends on two aspects, one is the change of heat flux in the basement of the basin, and the other is the nature and burial history of the sediments inside the basin. Due to the different geodynamic backgrounds and formation mechanisms of different types, the geodynamic models describing the tectonic evolution of different types of sedimentary basins are also different. Before carrying out the simulation experiment, the corresponding model can be determined according to the stratum burial history and thermal history of the target research basin.
在本实施方式中,对所述模拟样品进行地质过程约束模拟实验中,所述约束包括升温速率。此外,也可以包括升压速率等。In this embodiment, when performing a geological process constraint simulation experiment on the simulated sample, the constraint includes a heating rate. In addition, the boost rate and the like may also be included.
在本实施方式中,具体的根据地层埋藏史和热史,现今地层温度和压力,对所述模拟样品进行地质过程约束模拟实验的过程可以为:根据埋藏史和热史对模拟实验过程中的升温速度和升压速率进行约束,确保等效成熟度时的压力与地质实际一致;根据地层水的矿化度配置模拟过程中的加入流体类型。实验结束后可以获得油气充注后致密储层样品,为开展下一步的石油分布测定提供样品。In this embodiment, according to the burial history and thermal history of the formation, the current formation temperature and pressure, the process of performing the geological process constraint simulation experiment on the simulated sample can be: The temperature rise rate and pressure rise rate are constrained to ensure that the pressure at equivalent maturity is consistent with the geological reality; the type of fluid added during the simulation process is configured according to the salinity of the formation water. After the experiment is over, tight reservoir samples after oil and gas filling can be obtained to provide samples for the next step of oil distribution determination.
最后,对所述模拟样品进行石油分布测定,确定石油分布情况。其中,所述石油分布测定的方法包括下述中的任意一种:拉曼光谱、热解分析和核磁共振法。当然,所述石油分布的测定还可以为其他方式,例如,可以根据实验需求,通过薄片、荧光等方法进行定性分析,具体的,本申请在此并不作具体的限定。Finally, oil distribution measurement is carried out on the simulated sample to determine the oil distribution. Wherein, the method for determining the oil distribution includes any one of the following: Raman spectroscopy, pyrolysis analysis and nuclear magnetic resonance. Certainly, the determination of the oil distribution can also be done in other ways, for example, qualitative analysis can be carried out by thin section, fluorescence and other methods according to the experimental requirements. Specifically, this application does not make specific limitations here.
请参阅图2,本申请实施方式中还提供了一种致密储层石油充注模拟系统,其可以包括:Please refer to Fig. 2, the embodiment of the present application also provides a tight reservoir oil charging simulation system, which may include:
温度压力装置1,用于提供模拟实验过程中的温度和压力;The temperature and pressure device 1 is used to provide the temperature and pressure during the simulation experiment;
流体供排装置2,其包括供液管线设备、收液管线设备及自密封和开启阀门;Fluid supply and discharge device 2, which includes liquid supply pipeline equipment, liquid collection pipeline equipment and self-sealing and opening valves;
设备监测装置3,用于设定实验过程中的升温速率、升压速率以及监测装置内温度压力;The equipment monitoring device 3 is used to set the heating rate, the pressure increasing rate and the temperature and pressure in the monitoring device during the experiment;
含油测定装置4,用于测定石油的分布情况。The oil content measuring device 4 is used for measuring the distribution of oil.
在本实施方式中,所述温度压力装置1包括加热设备和油压设备。其中,所述加热设备能达到的最高温度为550摄氏度。也就是说,所述加热设备的温度范围为常温至550摄氏度。当然,所述加热设备的温度范围也可以根据实验需要进行相应的选择温度范围,本申请在此并不作具体的限定。所述油压设备能达到的最大压力为70兆帕。也就是说,所述压力设备的压力范围为常压至70兆帕。当然,所述油压设备的具体压力范围可以根据实际实验需求进行相应地选择,本申请在此并不作具体的限定。In this embodiment, the temperature and pressure device 1 includes heating equipment and hydraulic equipment. Wherein, the maximum temperature that the heating equipment can reach is 550 degrees Celsius. That is to say, the temperature range of the heating device is from room temperature to 550 degrees Celsius. Of course, the temperature range of the heating device can also be selected according to the needs of experiments, which is not specifically limited in this application. The maximum pressure that the hydraulic equipment can reach is 70 MPa. That is to say, the pressure range of the pressure equipment is from normal pressure to 70 MPa. Of course, the specific pressure range of the hydraulic equipment can be selected according to actual experimental requirements, and this application does not make specific limitations here.
在本实施方式中,所述流体供排装置2可以包括供液管线设备、收液管线设备以及自密封和开启阀门,以满足进行注地层水等实验需求。具体的,所述流体供排装置的具体连接和结构等本申请在此并不作具体的限定,整体上,样品的两端分布与供液管线设备和收液管线设备相连通,在连通的管线上,可以设置有开启阀门,另外在样品的端部可以设置有自密封结构。In this embodiment, the fluid supply and discharge device 2 may include liquid supply pipeline equipment, liquid collection pipeline equipment, and self-sealing and opening valves, so as to meet experimental requirements such as formation water injection. Specifically, the specific connection and structure of the fluid supply and discharge device are not specifically limited in this application. On the whole, the two ends of the sample are connected to the liquid supply pipeline equipment and the liquid collection pipeline equipment. On, an opening valve can be provided, and a self-sealing structure can be provided at the end of the sample.
在本实施方式中,设备监测装置3可以包括温压实时监测设备,用于实时监测系统的温度和压力变化。此外,所述设备监测装置3还可以包括在压力超过材料设计压力后的报警设备,具有较高的安全性能。In this embodiment, the equipment monitoring device 3 may include temperature and pressure real-time monitoring equipment for real-time monitoring of changes in temperature and pressure of the system. In addition, the device monitoring device 3 may also include an alarm device when the pressure exceeds the design pressure of the material, which has higher safety performance.
在本实施方式中,含油测定装置4可以根据测定的方法而进行相应的选择,本申请在此并不作具体的限定。具体的,所述测定方法具体可以包括拉曼光谱、热解分析和核磁共振法等,通过上述测定方法可以定量获得含油分布情况。此时,所述含油测定装置为其方法对应的装置,例如通过核磁共振法时,其对应的装置即为核磁共振仪。此外,也可以根据实验需要采用定性分析方法,此时所述含油测定装置4可以省略。In this embodiment, the oil content measurement device 4 can be selected according to the measurement method, which is not specifically limited in this application. Specifically, the measurement method may specifically include Raman spectroscopy, pyrolysis analysis, nuclear magnetic resonance, etc., and the oil content distribution can be quantitatively obtained through the above measurement methods. In this case, the oil content measuring device is a device corresponding to the method, for example, when the nuclear magnetic resonance method is used, the corresponding device is a nuclear magnetic resonance instrument. In addition, qualitative analysis methods can also be used according to experimental needs, and the oil content measuring device 4 can be omitted in this case.
在一个具体的应用场景下,利用本发明的致密储层石油充注模拟方法和系统,对鄂尔多斯盆地三叠系延长组长7致密砂岩石油充注聚集开展测定。低成熟烃源岩生烃动力学参数及实验加热数量可以参见图3至图5。In a specific application scenario, the tight reservoir oil charging simulation method and system of the present invention are used to measure the oil charging and accumulation of Chang 7 tight sandstone of the Triassic Yanchang Formation in the Ordos Basin. The hydrocarbon generation kinetic parameters and experimental heating quantities of low-mature source rocks can be seen in Fig. 3 to Fig. 5.
其中,图3为本申请一种依据致密储层石油充注模拟方法进行模拟实验后获得的生烃量转换率-温度的曲线图。横坐标表示模拟实验时的温度,单位为摄氏度(℃);纵坐标表示模拟实验中生烃量转换率。图中有三组曲线,分别为以10摄氏度/分的升温速率、20摄氏度/分的升温速率以及30摄氏度/分的升温速率获得生烃量转换率-温度的曲线图。Among them, Fig. 3 is a graph of hydrocarbon generation conversion rate-temperature obtained after a simulation experiment based on a tight reservoir oil charging simulation method of the present application. The abscissa indicates the temperature during the simulation experiment, in degrees Celsius (°C); the ordinate indicates the conversion rate of hydrocarbon generation in the simulation experiment. There are three sets of curves in the figure, which are the conversion rate-temperature curves of hydrocarbon generation amount obtained at the heating rate of 10°C/min, 20°C/min and 30°C/min.
其中,图4是本申请一种依据致密储层石油充注模拟方法进行模拟实验后获得的生烃量-温度的曲线图。横坐标表示模拟实验时的温度,单位为摄氏度(℃);左侧纵坐标表示生烃量,单位为:毫克/克(mg/gTOC);右侧纵坐标表示成熟度,单位为:百分数(%)。其中,图4中的第一曲线1A表示:成熟度;单位为:%;第二曲线1B表示:累计生烃量,单位为:毫克/克。Among them, Fig. 4 is a graph of hydrocarbon generation amount-temperature obtained after a simulation experiment based on a tight reservoir oil charging simulation method in the present application. The abscissa indicates the temperature during the simulation experiment, in degrees Celsius (°C); the left ordinate indicates the amount of hydrocarbon generation, in mg/g (mg/g TOC ); the right ordinate indicates the maturity, in percent (%). Wherein, the first curve 1A in Fig. 4 represents: maturity; the unit is: %; the second curve 1B represents: cumulative hydrocarbon generation amount, the unit is: mg/g.
其中,图5是本申请一种依据致密储层石油充注模拟方法进行模拟实验后获得的生烃量分布-活化能分布的柱状图。横坐标表示活化能分布,单位为千焦/摩尔(kj/mol);纵坐标表示生烃潜量分布。Among them, Fig. 5 is a histogram of hydrocarbon generation distribution-activation energy distribution obtained after a simulation experiment based on the tight reservoir oil charging simulation method of the present application. The abscissa indicates the distribution of activation energy in kilojoules/mole (kj/mol); the ordinate indicates the distribution of hydrocarbon generation potential.
通过本申请所述的模拟实验发现:致密储层背景下仍可以实现石油充注、石油充注程度受距离源岩远近控制,实验结果请参见图6至图8。Through the simulation experiments described in this application, it is found that oil charging can still be achieved under the background of tight reservoirs, and the degree of oil charging is controlled by the distance from the source rock. Please refer to Figure 6 to Figure 8 for the experimental results.
其中,图6为致密储层的源储配制关系为底生型岩心高度-含油饱和度的曲线图。所述储源配制关系为底生型时,即下生上储,下面为源岩,上面为储层。图中纵坐标表示岩心高度,单位为厘米(cm);横坐标表示含油饱和度。Among them, Fig. 6 is a graph showing the source-reservoir configuration relationship of tight reservoirs as the bottom-grown core height-oil saturation. When the reservoir-source configuration relationship is bottom-grown, that is, the bottom is the source rock, and the top is the reservoir. The ordinate in the figure represents the core height in centimeters (cm); the abscissa represents the oil saturation.
图7为致密储层的源储配制关系为夹层型岩心高度-含油饱和度的曲线图。所述储源配制关系为夹层型时,即源岩和储层混层。图中纵坐标表示岩心高度,单位为厘米(cm);横坐标表示含油饱和度。Fig. 7 is a graph showing the source-reservoir configuration relationship of tight reservoirs as interlayer core height-oil saturation. When the reservoir-source configuration relationship is an interlayer type, that is, the source rock and the reservoir are mixed. The ordinate in the figure represents the core height in centimeters (cm); the abscissa represents the oil saturation.
图8为致密储层的源储配制关系为顶生型岩心高度-含油饱和度的曲线图。所述储源配制关系为顶生型时,即上生下储,上面为源岩,下面为储层。图中纵坐标表示岩心高度,单位为厘米(cm);横坐标表示含油饱和度。Fig. 8 is a graph showing the source-reservoir configuration relationship of tight reservoirs as the top-grown core height-oil saturation. When the reservoir-source configuration relationship is the apical type, that is, the upper layer is the source rock and the lower layer is the reservoir layer. The ordinate in the figure represents the core height in centimeters (cm); the abscissa represents the oil saturation.
本发明实施方式中提供的致密储层石油成藏模拟方法与装置,借用温度压力装置、流体供排装置、设备监测装置,针对致密储层开展石油充注成藏研究,操作简单、复合实际,重复性好、定量评价。相比传统的测方法,本发明可以实现变地质过程约束下,定量和定性测定致密储层石油充注成藏,优点明显。The tight reservoir oil accumulation simulation method and device provided in the embodiments of the present invention use temperature and pressure devices, fluid supply and discharge devices, and equipment monitoring devices to carry out research on oil charging and accumulation in tight reservoirs. The operation is simple and practical, Good repeatability and quantitative evaluation. Compared with the traditional measuring method, the present invention can realize quantitative and qualitative determination of oil charging and accumulation in tight reservoirs under the constraint of variable geological process, and has obvious advantages.
本说明书中的上述各个实施方式均采用递进的方式描述,各个实施方式之间相同相似部分相互参照即可,每个实施方式重点说明的都是与其他实施方式不同之处。The above-mentioned implementations in this specification are described in a progressive manner, the same and similar parts of the implementations may be referred to each other, and each implementation focuses on the differences from other implementations.
以上所述仅为本发明的几个实施方式,虽然本发明所揭露的实施方式如上,但所述内容只是为了便于理解本发明而采用的实施方式,并非用于限定本发明。任何本发明所属技术领域的技术人员,在不脱离本发明所揭露的精神和范围的前提下,可以在实施方式的形式上及细节上作任何的修改与变化,但本发明的专利保护范围,仍须以所附权利要求书所界定的范围为准。The above descriptions are only a few implementations of the present invention. Although the disclosed implementations of the present invention are as above, the content described is only the implementations adopted for the convenience of understanding the present invention, and is not intended to limit the present invention. Any person skilled in the technical field to which the present invention belongs can make any modifications and changes in the form and details of the implementation without departing from the spirit and scope disclosed in the present invention, but the patent protection scope of the present invention is Still, the scope defined by the appended claims shall prevail.
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