CN106829000B - The equipment and its sterilization filling method of sterilization filling facial mask - Google Patents
The equipment and its sterilization filling method of sterilization filling facial mask Download PDFInfo
- Publication number
- CN106829000B CN106829000B CN201710069759.9A CN201710069759A CN106829000B CN 106829000 B CN106829000 B CN 106829000B CN 201710069759 A CN201710069759 A CN 201710069759A CN 106829000 B CN106829000 B CN 106829000B
- Authority
- CN
- China
- Prior art keywords
- facial mask
- sterilization
- bottle placer
- sterilizing
- filling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 230000001954 sterilising effect Effects 0.000 title claims abstract description 93
- 230000001815 facial effect Effects 0.000 title claims abstract description 72
- 238000004659 sterilization and disinfection Methods 0.000 title claims abstract description 57
- 238000011049 filling Methods 0.000 title claims description 34
- 238000000034 method Methods 0.000 title claims description 26
- 238000012546 transfer Methods 0.000 claims abstract description 25
- 238000001035 drying Methods 0.000 claims abstract description 11
- 238000002360 preparation method Methods 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims description 39
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 33
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 24
- 239000004006 olive oil Substances 0.000 claims description 24
- 235000008390 olive oil Nutrition 0.000 claims description 24
- ACTIUHUUMQJHFO-UPTCCGCDSA-N coenzyme Q10 Chemical compound COC1=C(OC)C(=O)C(C\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CC\C=C(/C)CCC=C(C)C)=C(C)C1=O ACTIUHUUMQJHFO-UPTCCGCDSA-N 0.000 claims description 23
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 15
- 239000000203 mixture Substances 0.000 claims description 13
- 239000005022 packaging material Substances 0.000 claims description 13
- BIVBRWYINDPWKA-VLQRKCJKSA-L Glycyrrhizinate dipotassium Chemical compound [K+].[K+].O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@H]1CC[C@]2(C)[C@H]3C(=O)C=C4[C@@H]5C[C@](C)(CC[C@@]5(CC[C@@]4(C)[C@]3(C)CC[C@H]2C1(C)C)C)C(O)=O)C([O-])=O)[C@@H]1O[C@H](C([O-])=O)[C@@H](O)[C@H](O)[C@H]1O BIVBRWYINDPWKA-VLQRKCJKSA-L 0.000 claims description 12
- 108010020346 Polyglutamic Acid Proteins 0.000 claims description 12
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 12
- 229940101029 dipotassium glycyrrhizinate Drugs 0.000 claims description 12
- UPBDXRPQPOWRKR-UHFFFAOYSA-N furan-2,5-dione;methoxyethene Chemical compound COC=C.O=C1OC(=O)C=C1 UPBDXRPQPOWRKR-UHFFFAOYSA-N 0.000 claims description 12
- 235000011187 glycerol Nutrition 0.000 claims description 12
- AGBQKNBQESQNJD-UHFFFAOYSA-M lipoate Chemical compound [O-]C(=O)CCCCC1CCSS1 AGBQKNBQESQNJD-UHFFFAOYSA-M 0.000 claims description 12
- 235000019136 lipoic acid Nutrition 0.000 claims description 12
- 229920002643 polyglutamic acid Polymers 0.000 claims description 12
- 229960002663 thioctic acid Drugs 0.000 claims description 12
- 239000011726 vitamin B6 Substances 0.000 claims description 12
- FYGDTMLNYKFZSV-URKRLVJHSA-N (2s,3r,4s,5s,6r)-2-[(2r,4r,5r,6s)-4,5-dihydroxy-2-(hydroxymethyl)-6-[(2r,4r,5r,6s)-4,5,6-trihydroxy-2-(hydroxymethyl)oxan-3-yl]oxyoxan-3-yl]oxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1OC1[C@@H](CO)O[C@@H](OC2[C@H](O[C@H](O)[C@H](O)[C@H]2O)CO)[C@H](O)[C@H]1O FYGDTMLNYKFZSV-URKRLVJHSA-N 0.000 claims description 11
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 11
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- DFPAKSUCGFBDDF-UHFFFAOYSA-N Nicotinamide Chemical compound NC(=O)C1=CC=CN=C1 DFPAKSUCGFBDDF-UHFFFAOYSA-N 0.000 claims description 11
- 239000008367 deionised water Substances 0.000 claims description 11
- 229910021641 deionized water Inorganic materials 0.000 claims description 11
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- 239000011570 nicotinamide Substances 0.000 claims description 11
- 229960003966 nicotinamide Drugs 0.000 claims description 11
- 235000005152 nicotinamide Nutrition 0.000 claims description 11
- 239000001540 sodium lactate Substances 0.000 claims description 11
- 229940005581 sodium lactate Drugs 0.000 claims description 11
- 235000011088 sodium lactate Nutrition 0.000 claims description 11
- AXPZIVKEZRHGAS-UHFFFAOYSA-N 3-benzyl-5-[(2-nitrophenoxy)methyl]oxolan-2-one Chemical compound [O-][N+](=O)C1=CC=CC=C1OCC1OC(=O)C(CC=2C=CC=CC=2)C1 AXPZIVKEZRHGAS-UHFFFAOYSA-N 0.000 claims description 10
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 8
- 229930003268 Vitamin C Natural products 0.000 claims description 8
- 229920000193 polymethacrylate Polymers 0.000 claims description 8
- 229910001220 stainless steel Inorganic materials 0.000 claims description 8
- 239000010935 stainless steel Substances 0.000 claims description 8
- 235000019154 vitamin C Nutrition 0.000 claims description 8
- 239000011718 vitamin C Substances 0.000 claims description 8
- 230000003139 buffering effect Effects 0.000 claims description 7
- ZUFQODAHGAHPFQ-UHFFFAOYSA-N pyridoxine hydrochloride Chemical compound Cl.CC1=NC=C(CO)C(CO)=C1O ZUFQODAHGAHPFQ-UHFFFAOYSA-N 0.000 claims description 7
- 230000000740 bleeding effect Effects 0.000 claims description 6
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- 239000011716 vitamin B2 Substances 0.000 claims description 6
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 5
- ACTIUHUUMQJHFO-UHFFFAOYSA-N Coenzym Q10 Natural products COC1=C(OC)C(=O)C(CC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)CCC=C(C)C)=C(C)C1=O ACTIUHUUMQJHFO-UHFFFAOYSA-N 0.000 claims description 5
- 235000017471 coenzyme Q10 Nutrition 0.000 claims description 5
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- 230000002572 peristaltic effect Effects 0.000 claims description 5
- 229960005323 phenoxyethanol Drugs 0.000 claims description 5
- 230000001681 protective effect Effects 0.000 claims description 5
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 4
- 230000006750 UV protection Effects 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 4
- 238000001514 detection method Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- -1 nicotinoyl Chemical group 0.000 claims description 4
- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 claims description 4
- 238000007789 sealing Methods 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 3
- 235000013772 propylene glycol Nutrition 0.000 claims description 3
- RADKZDMFGJYCBB-UHFFFAOYSA-N pyridoxal hydrochloride Natural products CC1=NC=C(CO)C(C=O)=C1O RADKZDMFGJYCBB-UHFFFAOYSA-N 0.000 claims description 3
- 235000019158 vitamin B6 Nutrition 0.000 claims description 3
- 229940011671 vitamin b6 Drugs 0.000 claims description 3
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 2
- 235000002710 Ilex cornuta Nutrition 0.000 claims 1
- 241001310146 Ilex cornuta Species 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 235000010326 Osmanthus heterophyllus Nutrition 0.000 claims 1
- 210000000481 breast Anatomy 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 238000010792 warming Methods 0.000 claims 1
- 239000003755 preservative agent Substances 0.000 abstract description 13
- 230000002335 preservative effect Effects 0.000 abstract description 12
- 239000002537 cosmetic Substances 0.000 abstract description 6
- 238000012859 sterile filling Methods 0.000 abstract description 3
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 description 10
- 239000000047 product Substances 0.000 description 10
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- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 description 5
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- 238000010586 diagram Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
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- 229930003231 vitamin Natural products 0.000 description 4
- 235000013343 vitamin Nutrition 0.000 description 4
- 239000011782 vitamin Substances 0.000 description 4
- 150000003722 vitamin derivatives Chemical class 0.000 description 4
- 238000012371 Aseptic Filling Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 229940100555 2-methyl-4-isothiazolin-3-one Drugs 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 2
- 206010020751 Hypersensitivity Diseases 0.000 description 2
- 208000034809 Product contamination Diseases 0.000 description 2
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 2
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- BEGLCMHJXHIJLR-UHFFFAOYSA-N methylisothiazolinone Chemical compound CN1SC=CC1=O BEGLCMHJXHIJLR-UHFFFAOYSA-N 0.000 description 2
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- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
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- 241001269238 Data Species 0.000 description 1
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical class CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 1
- 229930003471 Vitamin B2 Natural products 0.000 description 1
- 238000004378 air conditioning Methods 0.000 description 1
- 230000001857 anti-mycotic effect Effects 0.000 description 1
- 239000004599 antimicrobial Substances 0.000 description 1
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- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B3/00—Packaging plastic material, semiliquids, liquids or mixed solids and liquids, in individual containers or receptacles, e.g. bags, sacks, boxes, cartons, cans, or jars
- B65B3/04—Methods of, or means for, filling the material into the containers or receptacles
- B65B3/10—Methods of, or means for, filling the material into the containers or receptacles by application of pressure to material
- B65B3/12—Methods of, or means for, filling the material into the containers or receptacles by application of pressure to material mechanically, e.g. by pistons or pumps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
- A61K8/355—Quinones
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4986—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with sulfur as the only hetero atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
- B65B55/02—Sterilising, e.g. of complete packages
- B65B55/12—Sterilising contents prior to, or during, packaging
- B65B55/14—Sterilising contents prior to, or during, packaging by heat
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65B—MACHINES, APPARATUS OR DEVICES FOR, OR METHODS OF, PACKAGING ARTICLES OR MATERIALS; UNPACKING
- B65B55/00—Preserving, protecting or purifying packages or package contents in association with packaging
- B65B55/02—Sterilising, e.g. of complete packages
- B65B55/12—Sterilising contents prior to, or during, packaging
- B65B55/16—Sterilising contents prior to, or during, packaging by irradiation
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Mechanical Engineering (AREA)
- Engineering & Computer Science (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Toxicology (AREA)
- Cosmetics (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
Abstract
The invention belongs to cosmetic technical field, more particularly to the apparatus and its facial mask preparation method of a kind of sterile filling facial mask, the apparatus includes high temperature drying case, autoclave sterilization tank, the transfer pipeline of high-temp steam sterilizing can be used, can high-temp steam sterilizing bottle placer and hundred grades of racking rooms.The equipment can be sterilized well to facial mask, and preservative need not be added in facial mask, can both ensure the sterile of facial mask.
Description
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of equipment of sterilization filling facial mask and its sterilization filling side
Method.
Background technology
In mask product, because water content is very more in facial mask, easily by microorganism pollution, so to sterilizing and anti-corrosion
Ability has higher requirement.Existing facial mask generally use has preservative, and preservative is for face pack prescription inhibitor effectiveness application conduct
Protect a product from microorganism pollution, go bad, extend the shelf life of product.But it is itself unwanted contributions for skin care,
The excitant of skin can possibly even be increased and cause allergy etc.；To ensure the security of product, in order to prevent consumer because using
Caused possible infection by the product of microorganism pollution, if the amount of preservative addition is inadequate, is likely to occur microorganism and fits
Growing environment around answering, develops immunity to drugs, so as to cause anti-corrosion to fail.Preferable preservative should have spectrum activity, can be compared with
It is fast make microorganism deactivated, formulation stable, it is long-term use of safely, have no stimulation and sensitization.In general, it is most of anti-
Rotten agent or to antibacterium effectively or to it is antimycotic effectively, it is impossible to it is while effective to both；At present on the market for Compositional antiseptic agent compared with
It is more.Preservative is useless to skin care itself, or even can increase excitant and sensitization of skin etc. on the contrary, such as produced by Phenoxyethanol
Burning heat sensation, methylisothiazolinone (MIT) issuable allergy etc..Therefore existing cosmetics relevant laws and regulations require also clear and definite
Define the addition requirement of regulated substance (preservative).At present in mask product production, gone out using traditional hot pressing
Bacterium process, this method, which has the drawback that, can make the mounted facial mask in face cause facial mask bag deformed dilation, fracture phenomena.With
Cosmetics in China consumption consciousness successive Regression with natural safe theory, " zero addition " " zero burden ", " does not add anti-corrosion originally
Agent " etc. is increasingly taken seriously and praised highly, and especially with the fast sale of facial mask in recent years, the development and application of sterilization technology is to changing
Cosmetic safety and natural research and development field play more and more important effect
The content of the invention
For these reasons, by obtaining a kind of new apparatus for many years, the apparatus includes applicant：Including height
Warm drying box, autoclave sterilization tank, the transfer pipeline of high-temp steam sterilizing can be used, can high-temp steam sterilizing bottle placer and hundred grades
Racking room；The equipment can be sterilized well to facial mask, and preservative need not be added in facial mask, can both ensure facial mask
It is sterile.
What the present invention was achieved through the following technical solutions.
A kind of equipment of sterilization filling facial mask, including high temperature drying case, autoclave sterilization tank, can use high-temp steam sterilizing
Transfer pipeline, can high-temp steam sterilizing bottle placer and hundred grades of racking rooms, described sterilization tank uses high-temp steam sterilizing, institute
State closed tank body, air cleaner, material-feeding port, peristaltic pump, temperature inductor and control of the sterilization tank by jacketed and agitating paddle
System composition processed；The transfer pipeline is by with the tank connected inlet valve of the sterilizing, stainless steel delivery pipe, steam inlet valve, dead
Angle air bleeding valve, blowoff valve, blow-off pipe and the outlet valve composition being connected with bottle placer；The bottle placer is by top transparent guarantor with holes
Shield, high temperature resistant conveying flexible pipe, high temperature resistant gear pump, stainless steel filling head, ultraviolet lamp system, UV resistance lamp outer cover and blowdown
Pipeline forms；Hundred grades of bottling departments by changing rooms, buffering between, Airshower chamber, buffering corridor, Full fresh air purifying air-conditioning, high efficiency particulate air filter,
Uviol lamp and differential pressure indicator composition；Facial mask packaging material high temperature drying box sterilization, facial mask raw material is sterilized with the sterilization tank, through delivery pipe
Road is transported to bottle placer, and sterilized facial mask packaging material filling and sealing is used under hundred grades of racking rooms.
Wherein facial mask packaging material is handled 2 hours in high temperature drying case with 90 DEG C, can just be used after detection is sterile, facial mask bag
Material transport process is sealed with sterile sealed bag.
Wherein facial mask raw material sterilizing is completed, and is conveyed filtrated air by air cleaner, is kept sterilization tank malleation.
Wherein transfer pipeline sterilizing and bottle placer sterilizing is carried out simultaneously, and high-temperature steam, steam warp are passed through by steam inlet valve
Discharged by transfer pipeline, outlet valve, high temperature resistant conveying flexible pipe, high temperature resistant gear pump, stainless steel filling head and blow-off pipe；Delivery pipe
Road will open dead angle air bleeding valve and ensure that sterilizing is thorough when sterilizing.
Wherein the sterile wind of bottle placer is exported directly over bottle placer, and sterile wind is direct via top transparent protective shield with holes
Into inside bottle placer, bottle placer internal positive pressure is kept.
Wherein ultraviolet lamp system is opened inside pouring process bottle placer, and pouring process is carried out under uviol lamp protection.
Wherein sterilization filling method comprises the following steps：
Step (1) adds the facial mask raw material prepared in sterilization tank, closed sterilization tank, agitating paddle is opened, by each component
Stir；
Step (2) provides high temperature and high pressure steam with steam generator and heated up to sterilization tank, stops when tank temperature rise is to 105 DEG C
Heating, 105 DEG C of retaining surface film raw material temperature 15~30 minutes, then starts to cool, is cooled to 20-40 DEG C；
Sterilized while step (3) facial mask raw material sterilizes with high-temperature steam to air cleaner, air mistake is kept after sterilizing
Filter is closed；
Step (4) provides compressed air with air compressor, is passed through via air cleaner in sterilization tank, keeps sterilization tank
Interior malleation；
Step (5) is passed through steam into transfer pipeline via steam inlet valve, is sterilized to transfer pipeline and bottle placer, keeps
Lead to steam -40 minutes 20 minutes, then closed all pipe-line systems；
Step (6) is sterilized more than 20 minutes with uviol lamp to hundred grades of bottling department spaces, is closed uviol lamp, is passed through sterile wind,
Keep hundred grades of bottling department malleations；
Step (7) opens the ultraviolet lamp system of bottle placer, opens transfer pipeline inlet valve, outlet valve, feed liquid is via conveying
Pipeline enters bottle placer, starts filling.
Wherein facial mask raw material is made up of following parts by weight：Co-Q10 0.01-0.1, olive oil 5-10, lipoic acid 0.1-
0.5, niacinamide 0.1-0.5, beta glucan 0.1-0.5, vitamin B60.1-0.5, vitamin C 1.0-3.0, vitamin B2
0.1-0.5, dipotassium glycyrrhizinate 0.1-0.5, citric acid 0.1-0.5, vitamin E 0.5-2.0,1,2-PD 5.0-10.0,1,
3- butanediol 1.0-5.0, polyglutamic acid 3.0-5.0, hydroxyethyl cellulose 0.1-0.3, glycerine polymethacrylates/1,2- third
Glycol/Gantrez AN-119 4.0-8.0, triethanolamine 0.1-0.5, sodium lactate 1.0-3.5, Sensiva SC50 0.1-0.3, adds
Deionized water is to 100.
Wherein facial mask preparation method for raw material is：Co-Q10 is taken, is added in olive oil, shakes 30 minutes, makes auxiliary at 35 DEG C
Enzyme Q10 is substantially dissolved in standby in olive oil；Deionized water, 1,3-BDO, polyglutamic acid, hydroxyethyl cellulose and water are mixed
Close, be heated to 85 DEG C, add Co-Q10, middle olive oil after dissolving completely, the poly- methyl of triethanolamine, glycerine is added at 50 DEG C
Acrylate/1,2- propane diols/Gantrez AN-119, sodium lactate, niacinamide, beta glucan, lipoic acid, dipotassium glycyrrhizinate, are stirred
Mix to being completely dissolved；Less than 45 DEG C add vitamin C, vitamin B6, citric acid, Phenoxyethanol, Sensiva SC50 etc. other
Raw material, the facial mask raw material prepared.
The present invention compared with prior art, has advantages below and high-lighting effect：Changing facial mask raw material completely needs to add
The present situation of adding preservative agent or preservative substance, complete preservative free preservative substance can be produced using the system and technique of the present invention
Facial mask raw material, the security of product is greatly improved, reduce the use limitation to anti-corrosion class material sensitive crowd, thoroughly eliminate potential
Use hidden danger.The present invention is to reach anti-corrosion purpose with the sterilizing of pure physical means, does not have any chemistry, radiation residual in product,
And closed product integral asepsis in theory, substantially prolongs the shelf-life of product after filling, not damaged in sealing packaging material
In the case of the shelf-life be the several years.Condition needed for the system and technique of the present invention easily reaches in normal cosmetics industrial enterprise
Into suitable large-scale production and application.
Brief description of the drawings
Fig. 1 is aseptic filling systems principle schematic diagram provided by the invention
In figure：1- autoclave sterilization tanks；2- transfer pipelines；3- can high-temp steam sterilizing bottle placer；4- chucks；5- is stirred
Oar；6- air cleaners；7- material-feeding ports；8- peristaltic pumps；9- temperature inductors；10- inlet valves；11- steam inlet valves；12- is dead
Angle air bleeding valve；13- blowoff valves；14- blow-off pipes；15- outlet valves；Transparent protective shield with holes at the top of 16-；17- high temperature resistant conveyings are soft
Pipe；18- high temperature resistant gear pumps；19- stainless steel filling heads；20- ultraviolet lamp systems；21- UV resistance lamp outer covers；22- blowoff lines；
23- high efficiency particulate air filters；24- feed supplement bottles.
Fig. 2 is sterile filling process flow diagram provided by the invention.
Specific embodiment
Technical scheme, but protection scope of the present invention not limited to this are illustrated with specific embodiment below.
Content described in this specification embodiment is only enumerating to the way of realization of inventive concept, protection of the invention
Scope is not construed as being only limitted to the concrete form that embodiment is stated, protection scope of the present invention is also and in art technology
Personnel according to present inventive concept it is conceivable that equivalent technologies mean.Although embodiment of the invention below is retouched
State, but the invention is not limited in above-mentioned specific embodiments and applications field, following specific embodiments are only to show
It is meaning property, guiding rather than restricted.One of ordinary skill in the art is under the enlightenment of this specification and is not taking off
In the case of the scope protected from the claims in the present invention, the form of many kinds can also be made, these belong to the present invention
The row of protection.
Concrete structure, principle and the technical process of the present invention are described further below in conjunction with the accompanying drawings.
Embodiment 1
Facial mask prescription is：Co-Q10 0.01kg, olive oil 5kg, lipoic acid 0.1kg, niacinamide 0.1kg, beta glucan
0.1kg, vitamin B6 0.1kg, vitamin C 1.0kg, vitamin B2 0.1kg, dipotassium glycyrrhizinate 0.1kg, citric acid
0.1kg, vitamin E 0.5kg, 1,2-PD 5.0kg, 1,3-BDO 1.0kg, polyglutamic acid 3.0kg, hydroxy ethyl fiber
Plain 0.1kg, glycerine polymethacrylates/1,2-PD/Gantrez AN-119 4.0kg, triethanolamine 0.1kg, sodium lactate
1.0kg, Sensiva SC50 0.1kg, add deionized water to 100kg.
Facial mask preparation method for raw material is：Co-Q10 is taken, is added in olive oil, is shaken 30 minutes at 35 DEG C, makes coenzyme
Q10 is substantially dissolved in standby in olive oil；By deionized water, 1,3-BDO, polyglutamic acid, hydroxyethyl cellulose mixing, add
Heat adds in Co-Q10, olive oil after dissolving completely to 85 DEG C, triethanolamine, glycerine polymethylacrylic acid is added at 50 DEG C
Ester/1,2-PD/Gantrez AN-119, sodium lactate, niacinamide, beta glucan, lipoic acid, dipotassium glycyrrhizinate, is stirred to complete
Fully dissolved；Less than 45 DEG C addition vitamin Cs, vitamin B6, citric acid, other raw materials such as Sensiva SC50, prepared
Facial mask raw material.
Embodiment 2
Facial mask prescription is：Co-Q10 0.05kg, olive oil 7.5kg, lipoic acid 0.25kg, niacinamide 0.25kg, β-Portugal
Glycan 0.25kg, vitamin B60.25kg, vitamin C 2kg, vitamin B20.25kg, dipotassium glycyrrhizinate 0.25kg, citric acid
0.25kg, vitamin E 1.5kg, 1,2-PD 7.5kg, 1,3-BDO 2.5kg, polyglutamic acid 4kg, hydroxyethyl cellulose
0.2kg, glycerine polymethacrylates/1,2-PD/Gantrez AN-119 6kg, triethanolamine 0.25kg, sodium lactate
2.5kg, Sensiva SC50 0.2kg, add deionized water to 100kg.
Facial mask preparation method for raw material is：Co-Q10 is taken, is added in olive oil, is shaken 30 minutes at 35 DEG C, makes coenzyme
Q10 is substantially dissolved in standby in olive oil；By deionized water, 1,3-BDO, polyglutamic acid, hydroxyethyl cellulose mixing, add
Heat adds in Co-Q10, olive oil after dissolving completely to 85 DEG C, triethanolamine, glycerine polymethylacrylic acid is added at 50 DEG C
Ester/1,2-PD/Gantrez AN-119, sodium lactate, niacinamide, beta glucan, lipoic acid, dipotassium glycyrrhizinate, is stirred to complete
Fully dissolved；Less than 45 DEG C addition vitamin Cs, vitamin B6, citric acid, other raw materials such as Sensiva SC50, prepared
Facial mask raw material.
Embodiment 3
Co-Q10 0.1kg, olive oil 10kg, lipoic acid 0.5kg, niacinamide 0.5kg, beta glucan 0.5kg, vitamin
B60.5kg, vitamin C 3kg, vitamin B20.5kg, dipotassium glycyrrhizinate 0.5kg, citric acid 0.5kg, vitamin E 2kg, 1,
2- propane diols 10kg, 1,3-BDO 5kg, polyglutamic acid 5kg, hydroxyethyl cellulose 0.3kg, glycerine polymethacrylates/
1,2-PD/Gantrez AN-119 8kg, triethanolamine 0.5kg, sodium lactate 3.5kg, Sensiva SC50 0.3kg, add from
Sub- water is to 100kg.
Facial mask preparation method for raw material is：Co-Q10 is taken, is added in olive oil, is shaken 30 minutes at 35 DEG C, makes coenzyme
Q10 is substantially dissolved in standby in olive oil；By deionized water, 1,3-BDO, polyglutamic acid, hydroxyethyl cellulose mixing, add
For heat to 85 DEG C, addition Co-Q10, olive oil are total after dissolving completely, and triethanolamine, glycerine polymethylacrylic acid are added at 50 DEG C
Ester/1,2-PD/Gantrez AN-119, sodium lactate, niacinamide, beta glucan, lipoic acid, dipotassium glycyrrhizinate, is stirred to complete
Fully dissolved；Less than 45 DEG C addition vitamin Cs, vitamin B6, citric acid, other raw materials such as Sensiva SC50, prepared
Facial mask raw material.
Fig. 1 is aseptic filling systems principle schematic diagram provided by the invention, and the system includes packaging material disinfection system, face
Film raw material is prepared and disinfection system, facial mask feedstock transportation and aseptic filling systems, i.e., is mainly gone out by high temperature drying case, HTHP
Bacterium tank (1), can use high-temp steam sterilizing transfer pipeline (2), can high-temp steam sterilizing bottle placer (3) and hundred grades of racking rooms,
Described high-temperature sterilization tank uses high-temp steam sterilizing, and the device is by jacketed (4) and closed tank body, the air of agitating paddle (5)
Filter (6), material-feeding port (7), peristaltic pump (8) and temperature inductor (9) composition；The facial mask feedstock transportation pipeline (2) by
With tank connected inlet valve (10), steam inlet valve (11), dead angle air bleeding valve (12), blowoff valve (13), the blow-off pipe (14) of sterilizing
And outlet valve (15) composition being connected with bottle placer；It is described can sterilization filling machine by top transparent protective shield with holes (16), resistance to
High temperature conveying flexible pipe (17), high temperature resistant gear pump (18), stainless steel filling head (19), ultraviolet lamp system (20), outside UV resistance lamp
Cover (21) and blowoff line (22) composition；Described hundred grades of bottling departments by changing rooms, buffering between, Airshower chamber, buffering corridor, completely newly
Wind clean air conditioner, high efficiency particulate air filter (23), uviol lamp and differential pressure indicator composition.Facial mask raw material packaging material high temperature drying box sterilization, face
Film raw material is sterilized with sterilization tank, and bottle placer is transported to through transfer pipeline, and sterilized facial mask raw material bag is used under hundred grades of environment
Material filling and sealing.
Fig. 2 is sterile filling process flow diagram provided by the invention, and the filling process mainly includes packaging material sterilizing, facial mask
The process procedure such as raw material preparation, the sterilizing of facial mask raw material, feed supplement, transfer pipeline sterilizing, bottle placer sterilizing, bottling department sterilizing, filling,
It specifically comprises the following steps：
Facial mask raw material packaging material is handled 2 hours in high temperature drying case with 90 DEG C, can just be used after detection is sterile, and facial mask is former
Material packaging material transport process is sealed with sterile sealed bag；
Embodiment 1 or the facial mask raw material of embodiment 2 or embodiment 3 are added in sterilization tank (1), closed sterilization tank, opening is stirred
Oar (5) is mixed, each component is stirred；
High temperature and high pressure steam is provided with steam generator to heat up to sterilization tank, stops heating when tank temperature rise is to 105 DEG C, is protected
Hold facial mask material temperature 105 DEG C 15~30 minutes, then start to cool, be cooled to less than 40 DEG C, sampling detection, examine qualified side
Next process can be carried out；
Sterilized -30 minutes 15 minutes to air cleaner with high-temperature steam while facial mask raw material sterilizes, kept after sterilizing
Air cleaner is closed；
Such as need feed supplement that sterilized feed supplement bottle (24) is connected into sterilization tank (1) by material-feeding port (7), will with peristaltic pump (8)
Feed supplement is pumped into sterilization tank, and stirring is well mixed for -40 minutes 20 minutes with tank facial mask material liquid；
Compressed air is provided with air compressor, is passed through via air cleaner (6) in sterilization tank, keeps pressure inside the tank to exist
0.05MPa~0.1MPa (gauge pressure)；
Steam is passed through into conveying pipeline (2) via steam inlet valve (11), (3) are sterilized to feeding pipe (2) and bottle placer,
Keep logical steam more than 20 minutes, then closed all pipe-line systems；
Sterilized more than 20 minutes to bottling department space with uviol lamp, close uviol lamp, be passed through sterile wind, keeping bottling department just
Pressure, with buffering corridor pressure difference in more than 8Pa；
Open bottle placer ultraviolet lamp system (20), open transfer pipeline inlet valve (10), outlet valve (11), feed liquid via
Transfer pipeline (2) enters bottle placer (3), and beginning is filling, obtains facial mask.
Comparative example：Facial mask prescription is：Co-Q10 0.05kg, olive oil 7.5kg, lipoic acid 0.25kg, niacinamide
0.25kg, beta glucan 0.25kg, vitamin B60.25kg, vitamin C 2kg, vitamin B20.25kg, dipotassium glycyrrhizinate
0.25kg, citric acid 0.25kg, vitamin E 1.5kg, 1,2-PD 7.5kg, 1,3-BDO 2.5kg, polyglutamic acid
4kg, hydroxyethyl cellulose 0.2kg, glycerine polymethacrylates/1,2-PD/Gantrez AN-119 6kg, triethanolamine
0.25kg, sodium lactate 2.5kg, Phenoxyethanol 0.2g, Sensiva SC50 0.2kg, add deionized water to 100kg.
Facial mask preparation method for raw material is：Co-Q10 is taken, is added in olive oil, is shaken 30 minutes at 35 DEG C, makes coenzyme
Q10 is substantially dissolved in standby in olive oil；By deionized water, 1,3-BDO, polyglutamic acid, hydroxyethyl cellulose mixing, add
Heat to 85 DEG C, dissolve completely after add Co-Q10 olive oil, added at 50 DEG C triethanolamine, glycerine polymethacrylates/
1,2-PD/Gantrez AN-119, sodium lactate, niacinamide, beta glucan, lipoic acid, dipotassium glycyrrhizinate, stir to completely molten
Solution；Less than 45 DEG C addition vitamin Cs, vitamin B6, other are former for citric acid, Phenoxyethanol (preservative), Sensiva SC50 etc.
Material, lets cool, and 0.22 μm of filtering, pours into infused film cloth in the container equipped with facial present situation bonded fabric, is packed after infiltration.
The different sterilizing methods mask product contamination rate experimental datas of table 1 are as follows
Conclusion (of pressure testing)：It can be seen from upper table, the mask product contamination rate produced with present invention process is below 0.5%, tool
The value of standby large-scale production.
Claims (9)
- A kind of 1. equipment of sterilization filling facial mask, it is characterised in that：Including high temperature drying case, the sterilization tank of HTHP, can use The transfer pipeline of high-temp steam sterilizing, can high-temp steam sterilizing bottle placer and hundred grades of racking rooms, described sterilization tank use High-temp steam sterilizing, the sterilization tank is by the closed tank body of jacketed and agitating paddle, air cleaner, material-feeding port, peristaltic pump, temperature Spend inductor and control system composition；The transfer pipeline by with the tank connected inlet valve of the sterilizing, stainless steel delivery pipe, Steam inlet valve, dead angle air bleeding valve, blowoff valve, blow-off pipe and the outlet valve composition being connected with bottle placer；The bottle placer by Top transparent protective shield with holes, high temperature resistant conveying flexible pipe, high temperature resistant gear pump, stainless steel filling head, ultraviolet lamp system, UV resistance Lamp outer cover and blowoff line composition；Described hundred grades of racking rooms by changing rooms, buffering between, Airshower chamber, buffering corridor, all-fresh air Clean air conditioner, high efficiency particulate air filter, uviol lamp and differential pressure indicator composition；Facial mask packaging material high temperature drying box sterilization, facial mask raw material institute Sterilization tank sterilizing is stated, bottle placer is transported to through transfer pipeline, it is filling using sterilized facial mask packaging material under hundred grades of racking rooms Sealing.
- A kind of 2. equipment of sterilization filling facial mask according to claim 1, it is characterised in that：Facial mask packaging material is in high temperature drying Handled 2 hours, can just be used after detection is sterile, facial mask packaging material transport process is sealed with sterile sealed bag with 90 DEG C in case.
- A kind of 3. equipment of sterilization filling facial mask according to claim 1, it is characterised in that：The sterilizing of facial mask raw material is completed, Filtrated air is conveyed by air cleaner, keeps sterilization tank malleation.
- A kind of 4. equipment of sterilization filling facial mask according to claim 1, it is characterised in that：Transfer pipeline sterilize and it is filling Machine sterilizing is carried out simultaneously, is passed through high-temperature steam by steam inlet valve, steam is via transfer pipeline, high temperature resistant conveying flexible pipe, resistance to height Warm gear pump and stainless steel filling head discharge；Transfer pipeline will open dead angle air bleeding valve and ensure that sterilizing is thorough when sterilizing.
- A kind of 5. equipment of sterilization filling facial mask according to claim 1, it is characterised in that：The sterile wind outlet of bottle placer Directly over bottle placer, sterile wind is directly entered inside bottle placer via top transparent protective shield with holes, is kept inside bottle placer Malleation.
- A kind of 6. equipment of sterilization filling facial mask according to claim 1, it is characterised in that：In pouring process, bottle placer Internal ultraviolet lamp system is opened, and pouring process is carried out under uviol lamp protection.
- 7. a kind of sterilization filling method of the equipment of sterilization filling facial mask according to claim 1, it comprises the following steps：Step (1) adds the facial mask raw material prepared in sterilization tank, closed sterilization tank, opens agitating paddle, each component is stirred Uniformly；Step (2) provides high temperature and high pressure steam with steam generator and heated up to sterilization tank, stops when sterilization tank is warming up to 105 DEG C Heating, 105 DEG C of retaining surface film raw material temperature 15~30 minutes, then starts to cool, is cooled to 20-40 DEG C；Sterilized while step (3) facial mask raw material sterilizes with high-temperature steam to air cleaner, air cleaner is kept after sterilizing It is closed；Step (4) provides compressed air with air compressor, is passed through via air cleaner in sterilization tank, keeps in sterilization tank just Pressure；Step (5) is passed through steam into transfer pipeline via steam inlet valve, is sterilized to transfer pipeline and bottle placer, keeps logical and steams Vapour -40 minutes 20 minutes, then closed all pipe-line systems；Step (6) is sterilized more than 20 minutes with uviol lamp to hundred grades of racking rooms, closes uviol lamp, is passed through sterile wind, keeps hundred Level racking room malleation；Step (7) opens the ultraviolet lamp system of bottle placer, opens transfer pipeline inlet valve, outlet valve, feed liquid is via transfer pipeline Into bottle placer, start filling.
- 8. a kind of sterilization filling method according to claim 7, wherein facial mask raw material are made up of following parts by weight：Coenzyme Q10 0.01-0.1, olive oil 5-10, lipoic acid 0.1-0.5, niacinamide 0.1-0.5, beta glucan 0.1-0.5, vitamin B6 0.1-0.5, vitamin C 1.0-3.0, vitamin B20.1-0.5, dipotassium glycyrrhizinate 0.1-0.5, citric acid 0.1-0.5, dimension life Plain E 0.5-2.0,1,2-PD 5.0-10.0,1,3-BDO 1.0-5.0, polyglutamic acid 3.0-5.0, hydroxyethyl cellulose 0.1-0.3, glycerine polymethacrylates/1,2-PD/Gantrez AN-119 4.0-8.0, triethanolamine 0.1-0.5, breast Sour sodium 1.0-3.5, Sensiva SC50 0.1-0.3, adds deionized water to 100.
- 9. a kind of sterilization filling method according to claim 8, wherein facial mask preparation method for raw material are：Co-Q10 is taken, is added Enter in olive oil, shaken 30 minutes at 35 DEG C, be substantially dissolved in Co-Q10 standby in olive oil；By deionized water, 1,3- Butanediol, polyglutamic acid, hydroxyethyl cellulose and water mixing, are heated to 85 DEG C, and Co-Q10, olive oil are added after dissolving completely, Triethanolamine, glycerine polymethacrylates/1,2- propane diols/Gantrez AN-119, sodium lactate, nicotinoyl are added at 50 DEG C Amine, beta glucan, lipoic acid, dipotassium glycyrrhizinate, stirring is to being completely dissolved；Less than 45 DEG C add vitamin C, vitamin B6, Chinese holly Other raw materials such as rafter acid, Phenoxyethanol, Sensiva SC50, the facial mask raw material prepared.
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710069759.9A CN106829000B (en) | 2017-02-08 | 2017-02-08 | The equipment and its sterilization filling method of sterilization filling facial mask |
| PCT/CN2017/099148 WO2018145446A1 (en) | 2017-02-08 | 2017-08-25 | Aseptic facial mask filling device and mask preparation method therefor |
| SG11201801259PA SG11201801259PA (en) | 2017-02-08 | 2017-08-25 | Facial mask aseptic-filling apparatus and Facial Mask Preparation Method Thereof |
| ZA2018/00673A ZA201800673B (en) | 2017-02-08 | 2018-01-31 | Facial mask aseptic-filling apparatus and facial mask preparation method thereof |
| FR1851028A FR3062571B1 (en) | 2017-02-08 | 2018-02-07 | ASEPTIC FILLING APPARATUS FOR A FACE MASK AND METHOD FOR PREPARING THE FACE MASK |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710069759.9A CN106829000B (en) | 2017-02-08 | 2017-02-08 | The equipment and its sterilization filling method of sterilization filling facial mask |
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| Publication Number | Publication Date |
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| CN106829000A CN106829000A (en) | 2017-06-13 |
| CN106829000B true CN106829000B (en) | 2018-03-16 |
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|---|---|
| CN (1) | CN106829000B (en) |
| FR (1) | FR3062571B1 (en) |
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| CN107830391A (en) * | 2017-11-09 | 2018-03-23 | 河南道骐汽车科技有限公司 | A kind of lubricating oil filling apparatus with agitating function |
| CN108144373B (en) * | 2017-12-19 | 2020-12-11 | 新乡华青药业有限公司 | Sterile transfer system for sterile ophthalmic ointment materials |
| CN108569425A (en) * | 2017-12-29 | 2018-09-25 | 广州美中生物科技有限公司 | A kind of bottle placer of liquid of the no added preservative containing active material |
| CN108578255B (en) * | 2018-04-28 | 2023-07-04 | 苏州大学 | Production equipment of canthus subsides |
| CN110239752A (en) * | 2019-06-10 | 2019-09-17 | 安速日用化学(苏州)有限公司 | A kind of environmentally protective gel-like aromatic filling production lines |
| CN112675344B (en) * | 2019-10-18 | 2023-02-17 | 上海巨宜电气工程有限公司 | Online sterilization system for protecting filter in feed liquid conveying pipeline |
| CN111067804A (en) * | 2019-12-29 | 2020-04-28 | 广州无添加主义化妆品有限公司 | Preparation method of mask without preservative and preservative substitute |
| CN112870392B (en) * | 2021-01-18 | 2022-08-09 | 杭州和风细雨生物科技有限公司 | Preparation process of liquorice whitening and skin moistening cream |
| CN114013704B (en) * | 2021-02-07 | 2025-04-22 | 江苏新美星包装机械股份有限公司 | A sterile buffering and conveying device for liquid containing fruit particles |
| CN115193281A (en) * | 2022-06-14 | 2022-10-18 | 广州汉方医学生物科技有限公司 | Emulsification apparatus and emulsification method |
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- 2017-08-25 SG SG11201801259PA patent/SG11201801259PA/en unknown
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- 2018-01-31 ZA ZA2018/00673A patent/ZA201800673B/en unknown
- 2018-02-07 FR FR1851028A patent/FR3062571B1/en active Active
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| CN101543634A (en) * | 2009-05-11 | 2009-09-30 | 王相刚 | Method for sterilizing air bacterial filter for fermentation tank and fermentation tank provided with air bacterial filter |
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Also Published As
| Publication number | Publication date |
|---|---|
| FR3062571A1 (en) | 2018-08-10 |
| WO2018145446A1 (en) | 2018-08-16 |
| ZA201800673B (en) | 2018-12-19 |
| CN106829000A (en) | 2017-06-13 |
| SG11201801259PA (en) | 2018-09-27 |
| FR3062571B1 (en) | 2023-03-10 |
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