CN106818747A - A kind of coated slow-release plant growth regulator and preparation method and application - Google Patents
A kind of coated slow-release plant growth regulator and preparation method and application Download PDFInfo
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- CN106818747A CN106818747A CN201611159032.1A CN201611159032A CN106818747A CN 106818747 A CN106818747 A CN 106818747A CN 201611159032 A CN201611159032 A CN 201611159032A CN 106818747 A CN106818747 A CN 106818747A
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- Prior art keywords
- plant growth
- growth regulator
- coating
- coated slow
- release
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- 239000005648 plant growth regulator Substances 0.000 title claims abstract description 107
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 239000011248 coating agent Substances 0.000 claims abstract description 100
- 238000000576 coating method Methods 0.000 claims abstract description 99
- 239000000843 powder Substances 0.000 claims abstract description 39
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 37
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 37
- 241001330002 Bambuseae Species 0.000 claims abstract description 37
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 37
- 239000011425 bamboo Substances 0.000 claims abstract description 37
- 239000003610 charcoal Substances 0.000 claims abstract description 37
- 239000004200 microcrystalline wax Substances 0.000 claims abstract description 32
- 239000002383 tung oil Substances 0.000 claims abstract description 28
- 239000007921 spray Substances 0.000 claims abstract description 27
- 241000209140 Triticum Species 0.000 claims abstract description 25
- 235000021307 Triticum Nutrition 0.000 claims abstract description 25
- PRPINYUDVPFIRX-UHFFFAOYSA-N 1-naphthaleneacetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CC=CC2=C1 PRPINYUDVPFIRX-UHFFFAOYSA-N 0.000 claims abstract description 17
- HBYKUCARMGQRCF-UHFFFAOYSA-N [K].C(CCC)(=O)O Chemical compound [K].C(CCC)(=O)O HBYKUCARMGQRCF-UHFFFAOYSA-N 0.000 claims abstract description 17
- 238000001035 drying Methods 0.000 claims abstract description 9
- 238000002844 melting Methods 0.000 claims abstract description 9
- 230000008018 melting Effects 0.000 claims abstract description 9
- 238000013329 compounding Methods 0.000 claims abstract description 5
- 238000010790 dilution Methods 0.000 claims abstract description 3
- 239000012895 dilution Substances 0.000 claims abstract description 3
- 239000002245 particle Substances 0.000 claims description 46
- 235000013339 cereals Nutrition 0.000 claims description 26
- 239000000203 mixture Substances 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 9
- 238000007599 discharging Methods 0.000 claims description 8
- 238000005096 rolling process Methods 0.000 claims description 8
- 230000008635 plant growth Effects 0.000 claims description 5
- OVSKIKFHRZPJSS-DOMIDYPGSA-N 2-(2,4-dichlorophenoxy)acetic acid Chemical group OC(=O)[14CH2]OC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-DOMIDYPGSA-N 0.000 claims description 3
- 241000196324 Embryophyta Species 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 230000001105 regulatory effect Effects 0.000 claims description 3
- AXKBOWBNOCUNJL-UHFFFAOYSA-M sodium;2-nitrophenolate Chemical compound [Na+].[O-]C1=CC=CC=C1[N+]([O-])=O AXKBOWBNOCUNJL-UHFFFAOYSA-M 0.000 claims description 3
- 238000013268 sustained release Methods 0.000 claims description 3
- 239000012730 sustained-release form Substances 0.000 claims description 3
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 claims description 2
- 239000004327 boric acid Substances 0.000 claims description 2
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 2
- BVTBRVFYZUCAKH-UHFFFAOYSA-L disodium selenite Chemical compound [Na+].[Na+].[O-][Se]([O-])=O BVTBRVFYZUCAKH-UHFFFAOYSA-L 0.000 claims description 2
- 235000013924 ferrous gluconate Nutrition 0.000 claims description 2
- 239000004222 ferrous gluconate Substances 0.000 claims description 2
- 229960001645 ferrous gluconate Drugs 0.000 claims description 2
- VRIVJOXICYMTAG-IYEMJOQQSA-L iron(ii) gluconate Chemical compound [Fe+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O VRIVJOXICYMTAG-IYEMJOQQSA-L 0.000 claims description 2
- 229960001471 sodium selenite Drugs 0.000 claims description 2
- 235000015921 sodium selenite Nutrition 0.000 claims description 2
- 239000011781 sodium selenite Substances 0.000 claims description 2
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims description 2
- 229960001763 zinc sulfate Drugs 0.000 claims description 2
- 229910000368 zinc sulfate Inorganic materials 0.000 claims description 2
- 239000003630 growth substance Substances 0.000 claims 1
- 229940099596 manganese sulfate Drugs 0.000 claims 1
- 235000007079 manganese sulphate Nutrition 0.000 claims 1
- 239000011702 manganese sulphate Substances 0.000 claims 1
- SQQMAOCOWKFBNP-UHFFFAOYSA-L manganese(II) sulfate Chemical compound [Mn+2].[O-]S([O-])(=O)=O SQQMAOCOWKFBNP-UHFFFAOYSA-L 0.000 claims 1
- 238000005507 spraying Methods 0.000 claims 1
- -1 compound sodium nitrophenolate Chemical class 0.000 abstract description 22
- OVSKIKFHRZPJSS-UHFFFAOYSA-N 2,4-D Chemical group OC(=O)COC1=CC=C(Cl)C=C1Cl OVSKIKFHRZPJSS-UHFFFAOYSA-N 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 206010067482 No adverse event Diseases 0.000 abstract description 2
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 239000003814 drug Substances 0.000 description 13
- 231100000572 poisoning Toxicity 0.000 description 8
- 230000000607 poisoning effect Effects 0.000 description 8
- 239000000463 material Substances 0.000 description 7
- 239000000243 solution Substances 0.000 description 7
- 230000002459 sustained effect Effects 0.000 description 7
- 239000000470 constituent Substances 0.000 description 6
- 239000003337 fertilizer Substances 0.000 description 6
- 230000012010 growth Effects 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 4
- 239000003905 agrochemical Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- YGGXZTQSGNFKPJ-UHFFFAOYSA-N methyl 2-naphthalen-1-ylacetate Chemical compound C1=CC=C2C(CC(=O)OC)=CC=CC2=C1 YGGXZTQSGNFKPJ-UHFFFAOYSA-N 0.000 description 2
- RWMKSKOZLCXHOK-UHFFFAOYSA-M potassium;butanoate Chemical compound [K+].CCCC([O-])=O RWMKSKOZLCXHOK-UHFFFAOYSA-M 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 239000002689 soil Substances 0.000 description 2
- 230000001988 toxicity Effects 0.000 description 2
- 231100000419 toxicity Toxicity 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 235000010678 Paulownia tomentosa Nutrition 0.000 description 1
- 240000002834 Paulownia tomentosa Species 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 238000012271 agricultural production Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 150000002475 indoles Chemical class 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 229920000620 organic polymer Polymers 0.000 description 1
- 230000008121 plant development Effects 0.000 description 1
- 238000003900 soil pollution Methods 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229940032330 sulfuric acid Drugs 0.000 description 1
- 230000003075 superhydrophobic effect Effects 0.000 description 1
- 210000002262 tip cell Anatomy 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000003911 water pollution Methods 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/18—Vapour or smoke emitting compositions with delayed or sustained release
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01G—HORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
- A01G7/00—Botany in general
- A01G7/06—Treatment of growing trees or plants, e.g. for preventing decay of wood, for tingeing flowers or wood, for prolonging the life of plants
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
- A01N33/16—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds containing nitrogen-to-oxygen bonds
- A01N33/18—Nitro compounds
- A01N33/20—Nitro compounds containing oxygen or sulfur attached to the carbon skeleton containing the nitro group
- A01N33/22—Nitro compounds containing oxygen or sulfur attached to the carbon skeleton containing the nitro group having at least one oxygen or sulfur atom and at least one nitro group directly attached to the same aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/10—Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N39/00—Biocides, pest repellants or attractants, or plant growth regulators containing aryloxy- or arylthio-aliphatic or cycloaliphatic compounds, containing the group or, e.g. phenoxyethylamine, phenylthio-acetonitrile, phenoxyacetone
- A01N39/02—Aryloxy-carboxylic acids; Derivatives thereof
- A01N39/04—Aryloxy-acetic acids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/36—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings
- A01N43/38—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom five-membered rings condensed with carbocyclic rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/02—Sulfur; Selenium; Tellurium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/14—Boron; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
- A01N59/20—Copper
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Environmental Sciences (AREA)
- Wood Science & Technology (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Inorganic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Biodiversity & Conservation Biology (AREA)
- Ecology (AREA)
- Forests & Forestry (AREA)
- Toxicology (AREA)
- Botany (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of coated slow-release plant growth regulator and preparation method and application, the coated slow-release plant growth regulator includes coating and sandwich layer, the coating is cheap and easy to get, it is environment-friendly, the tung oil easily degraded, bamboo charcoal and microwax, the sandwich layer is 2, 4 dichlorphenoxyacetic acids, compound sodium nitrophenolate, the plant growth regulator of Nafusaku and butyric acid potassium compounding, preparation method is to form internal layer coating with tung oil and bamboo charcoal powder on plant growth regulator surface, the plant growth regulator that tung oil will have been sprayed is wrapped up with bamboo charcoal powder, drying, then the surface of internal layer coating is sprayed on the microwax after heating melting, form outer layer coating.Coated slow-release plant growth regulator of the invention is taken root the phase in wheat, after being watered dilution, in foliage-spray 23 times, 25% or so can be increased production, wheat quality is had no adverse effects.
Description
Technical field
The invention belongs to plant growth regulator field, it is related to a kind of coated slow-release plant growth regulator and its preparation side
Method and application.
Background technology
Release-controlled coated material is divided into inorganic coating material and the major class of organic polymer coated fertilizer two, with sustained release performance,
The nutrition rate of release in coating can be made to slow down, acquisition time extension.In view of a large amount of use of common chemical fertilizer causes soil texture
A series of bad influences such as destruction, underground water pollution, quality of agricultural product decline, film-coated and slow release fertilizer can reduce the use of chemical fertilizer
Amount, improves fertilizer nutrient utilization, and mitigates the environmental pollution that fertilizer loss is caused, and therefore suffers from the widely studied of world scholar
And concern.However, very few about the research report of coated slow-release plant growth regulator.
Plant growth regulator is the class agricultural chemicals for coordinate plant growth development, in enhancing crop anti-adversity, is improved
The aspects such as crop yield, improvement product quality, raising planting benefit have played great function, with low cost, fast, benefit of producing effects
The advantages of height, saving labour, field crop, industrial crops, fruit tree, forest, vegetables, flowers etc. have been widely used in it each
Individual aspect.
The increase of production of China's plant growth regulator is surprising in recent years, with its largely using in agricultural production, deposits
Below of both defect and deficiency, one is as the plant growth regulator agricultural chemicals artificial synthesized with other, with one
Fixed toxicity, although major part belongs to lower toxicity agricultural chemicals, but the enzyme of plant growth regulator is decomposed due to not existing in plant
Class, thus its longevity of residure is longer, improper use will also result in serious poisoning and environmental pollution；Two is plant growth regulator tool
There is notable, efficient mediating effect+6, plant growth, development and metabolism can just be played using the plant growth regulator of low concentration
Important adjustment effect, a large amount of of plant growth regulator use, except the various poisoning performance on plant is caused, it is also possible to
Remain in soil, form soil pollution.Particularly in recent years, it is caused in food due to the abuse of plant growth regulator
Increasingly paid close attention to by people with the residual in environment, safety problem.
In consideration of it, the research of coated slow-release plant growth regulator will turn into a focus of scientific and technical innovation and seize market
Technology commanding elevation.
The content of the invention
To solve the drug injury problem of plant growth regulator, the invention provides a kind of coated slow-release plant growth regulating
Agent, the coated slow-release plant growth regulator is to form internal layer coating with tung oil and bamboo charcoal powder on plant growth regulator surface,
Outer layer coating is formed with microwax on the surface of internal layer coating.
It is a further object of the present invention to provide the preparation method of above-mentioned coated slow-release plant growth regulator, first time coating
Using tung oil and bamboo charcoal powder as coating agent, the plant growth regulator that will spray tung oil is wrapped up with bamboo charcoal powder, dried；
After second coating melts microwax heating, the product surface being sprayed on obtained by first time coating.
Present invention also offers the application of above-mentioned coated slow-release plant growth regulator.
In order to solve the above technical problems, the technical solution adopted by the present invention is as follows：
Coated slow-release plant growth regulator of the invention includes outer layer coating, internal layer coating and sandwich layer, the outer layer bag
Film is microwax, and the internal layer coating is tung oil and bamboo charcoal powder, and the sandwich layer is plant growth regulator, each component in its composition
It is expressed as by weight：Grain diameter is 90 parts of the plant growth regulator of 3-4mm, tung oil 40-60 parts, grain diameter<0.08mm
Bamboo charcoal powder 4-6 parts, microwax 20-30 parts.
Preferably, plant growth regulator of the present invention is 2,4- dichlorphenoxyacetic acids, compound sodium nitrophenolate, methyl α-naphthyl acetate
The mixture of sodium, butyric acid potassium compounding.
Specifically, 2,4- dichlorphenoxyacetic acids, compound sodium nitrophenolate, methyl α-naphthyl acetate in described coated slow-release plant growth regulator
Sodium, the mass ratio of butyric acid potassium are 2-5:5-8:5-10:3-7.
Preferably, plant growth regulator of the present invention can also add ferrous gluconate, zinc sulfate, sulfuric acid
The trace element of one or more in manganese, sodium selenite, copper sulphate, boric acid.
The preparation method of coated slow-release plant growth regulator of the present invention, it is characterised in that：Coating is completed through coating twice
The preparation of plant growth regulator is sustained, following steps are specifically included：
(1) first time coating：By particle diameter for 3-4mm plant growth regulator particle input coating machine in, use hair dryer
Preheating 5-10min, then tung oil be sprayed on the plant growth regulator particle surface of rolling with high-pressure spray gun, after 3-5min, to
Grain diameter is put into coating machine rotary drum<The bamboo charcoal powder of 0.08mm, keeps rotating speed and heating-up temperature, is discharged after 5-10 minutes, dries
Siccative is obtained after dry；
(2) second coating：During first time coating gained siccative put into coating machine again, sprayed in rotary drum using spray gun
Enter the microwax of heated melting, after microwax has been sprayed, close electric furnace, coating machine keeps rotating speed, is discharged after 5-10 minutes, obtains
Coated slow-release plant growth regulator.
Preferably, the particle diameter described in step (1) is the plant growth regulator particle and grain diameter of 3-4mm<
The bamboo charcoal powder of 0.08mm is crushed by airslide disintegrating mill, crosses rotary screen or Vibration Screen is got.
Preferably, the rotating speed of coating machine described in step (1) be 60r/min, preheating temperature be 50-70 DEG C.
Preferably, the discharging described in step (1) is dried in an oven with 50 DEG C.
Preferably, coating machine rotating speed described in step (2) be 60r/min, heating-up temperature be 60-80 DEG C.
A kind of application of coated slow-release plant growth regulator, specifically takes root the phase in wheat, after being watered dilution, in blade face
Spray 2-3 times.
Beneficial effects of the present invention are as follows：
(1) coated slow-release plant growth regulator of the invention is with tung oil and bamboo charcoal powder on plant growth regulator surface
Internal layer coating is formed, outer layer coating is formed with microwax on the surface of internal layer coating, be made coated slow-release plant growth regulator,
Wherein main chemical compositions-the α of tung oil-tung oil triglyceride contains conjugated double bond, with film forming rate of drying is fast, adhesive force
By force, a little, and bamboo charcoal, used as a kind of novel absorption material, its molecule is fine and closely woven porous, with superpower for water-fast and good corrosion resistance
Adsorption capacity, the suction-operated by bamboo charcoal to plant growth regulator delays the release to plant growth regulator, but
Form that internal layer coating film-strength is relatively low by tung oil and bamboo charcoal powder, initial stage release rate is high, and super hydrophobic material-crystallite is wrapped on its surface
Wax, can delay the dissolution velocity of plant growth regulator, extend the acquisition time of plant growth regulator, while moistureproof, anti-sticking
Knot.
(2) present invention is selected release-controlled coated material-tung oil, bamboo charcoal and microwax, it is cheap and easy to get, environment-friendly, easy
Degraded, had good sustained release effect.
(3) plant growth regulator that the present invention is selected is 2,4 dichlorophenoxyacetic acid, compound sodium nitrophenolate, Nafusaku, Yin
The mixture of diindyl potassium butyrate compounding, 2, the 4- dichlorphenoxyacetic acids of wherein low concentration can promote the division of Wheat root tip cells, and
Then there are obvious inhibitory action, 2,4- dichlorphenoxyacetic acids and compound sodium nitrophenolate, Nafusaku, indoles beyond suitable concentration range
The compounding of potassium butyrate can reduce the consumption of 2,4- dichlorphenoxyacetic acids, and with significant facilitation, rooting efficiency is good, in wheat
Take root phase foliage-spray 2-3 times, 25% or so can be increased production, wheat quality is had no adverse effects.
Specific embodiment
The above of the invention is described in further detail below by way of specific embodiment, but this should not be understood
For the scope of above-mentioned theme of the invention is only limitted to following embodiment.Without departing from the idea case in the present invention described above, root
The various replacements or change made according to ordinary skill knowledge and customary means, all should be included within the scope of the invention.
Embodiment 1
Each component is expressed as by weight in the coated slow-release plant growth regulator composition of the present embodiment：Grain diameter is 3-
2, the 4- dichlorphenoxyacetic acids 12g of 4mm, compound sodium nitrophenolate 30g, Nafusaku 30g, butyric acid potassium 18g, tung oil 40g, particle
Footpath<The bamboo charcoal powder 4g of 0.08mm, microwax 20g.
The preparation method of coated slow-release plant growth regulator of the present invention is：
(1) first time coating：By particle diameter for 3-4mm plant growth regulator particle input coating machine in, use hair dryer
Preheating 5min, then tung oil is sprayed on the plant growth regulator particle surface of rolling with high-pressure spray gun, after 3min, to coating machine
Grain diameter is put into rotary drum<The bamboo charcoal powder of 0.08mm, keeps rotating speed and heating-up temperature, is discharged after 5 minutes, must be done after drying
Material；
(2) second coating：During first time coating gained siccative put into coating machine again, sprayed in rotary drum using spray gun
Enter the microwax of heated melting, after microwax has been sprayed, close electric furnace, coating machine keeps rotating speed, is discharged after 5 minutes, must wrap
Film is sustained plant growth regulator.
Specifically, the particle diameter described in step (1) is the plant growth regulator particle and grain diameter of 3-4mm<0.08mm
Bamboo charcoal powder crushed by airslide disintegrating mill, cross rotary screen or Vibration Screen and get.
Specifically, the rotating speed of the coating machine described in step (1) be 60r/min, preheating temperature be 50 DEG C.
Specifically, the discharging described in step (1) is dried in an oven with 50 DEG C.
Specifically, the coating machine rotating speed described in step (2) be 60r/min, heating-up temperature be 60 DEG C.
Test and taken root the phase in wheat, the coated slow-release plant growth regulator 30g that will be made is watered 100kg, stirs,
In foliage-spray 3 times, (wherein, normal control medicament is 5% with active constituent content identical normal control medicament is not sprayed
2,4 dichlorophenoxyacetic acid ethanol solution, 2.85% compound sodium nitrophenolate and Nafusaku is compound aqueous and 2% butyric acid potassium can
Soluble powder) wheat paddock compare, the present embodiment to wheat growth unrestraint and the generation of poisoning phenomenon, volume increase 21%.
Embodiment 2
Each component is expressed as by weight in the coated slow-release plant growth regulator composition of the present embodiment：Grain diameter is 3-
2, the 4- dichlorphenoxyacetic acids 15g of 4mm, compound sodium nitrophenolate 24g, Nafusaku 30g, butyric acid potassium 21g, tung oil 60g, particle
Footpath<The bamboo charcoal powder 6g of 0.08mm, microwax 30g.
The preparation method of coated slow-release plant growth regulator of the present invention is：
(1) first time coating：By particle diameter for 3-4mm plant growth regulator particle input coating machine in, use hair dryer
Preheating 10min, then tung oil is sprayed on the plant growth regulator particle surface of rolling with high-pressure spray gun, after 5min, to coating
Grain diameter is put into machine rotary drum<The bamboo charcoal powder of 0.08mm, keeps rotating speed and heating-up temperature, is discharged after 10 minutes, after drying
Siccative；
(2) second coating：During first time coating gained siccative put into coating machine again, sprayed in rotary drum using spray gun
Enter the microwax of heated melting, after microwax has been sprayed, close electric furnace, coating machine keeps rotating speed, is discharged after 10 minutes, must wrap
Film is sustained plant growth regulator.
Specifically, the particle diameter described in step (1) is the plant growth regulator particle and grain diameter of 3-4mm<0.08mm
Bamboo charcoal powder crushed by airslide disintegrating mill, cross rotary screen or Vibration Screen and get.
Specifically, the rotating speed of the coating machine described in step (1) be 60r/min, preheating temperature be 70 DEG C.
Specifically, the discharging described in step (1) is dried in an oven with 50 DEG C.
Specifically, the coating machine rotating speed described in step (2) be 60r/min, heating-up temperature be 80 DEG C.
Test and taken root the phase in wheat, the coated slow-release plant growth regulator 30g that will be made is watered 100kg, stirs,
In foliage-spray 2 times, (wherein, normal control medicament is 5% with active constituent content identical normal control medicament is not sprayed
2,4 dichlorophenoxyacetic acid ethanol solution, 2.85% compound sodium nitrophenolate and Nafusaku is compound aqueous and 2% butyric acid potassium can
Soluble powder) wheat paddock compare, the present embodiment occurs to the growth unrestraint of wheat and poisoning phenomenon, volume increase 23%.
Embodiment 3
Each component is expressed as by weight in the coated slow-release plant growth regulator composition of the present embodiment：Grain diameter is 3-
2, the 4- dichlorphenoxyacetic acids 15g of 4mm, compound sodium nitrophenolate 25g, Nafusaku 30g, butyric acid potassium 20g, tung oil 40g, particle
Footpath<The bamboo charcoal powder 6g of 0.08mm, microwax 20g.
The preparation method of coated slow-release plant growth regulator of the present invention is：
(1) first time coating：By particle diameter for 3-4mm plant growth regulator particle input coating machine in, use hair dryer
Preheating 10min, then tung oil is sprayed on the plant growth regulator particle surface of rolling with high-pressure spray gun, after 3min, to coating
Grain diameter is put into machine rotary drum<The bamboo charcoal powder of 0.08mm, keeps rotating speed and heating-up temperature, is discharged after 10 minutes, after drying
Siccative；
(2) second coating：During first time coating gained siccative put into coating machine again, sprayed in rotary drum using spray gun
Enter the microwax of heated melting, after microwax has been sprayed, close electric furnace, coating machine keeps rotating speed, is discharged after 5 minutes, must wrap
Film is sustained plant growth regulator.
Specifically, the particle diameter described in step (1) is the plant growth regulator particle and grain diameter of 3-4mm<0.08mm
Bamboo charcoal powder crushed by airslide disintegrating mill, cross rotary screen or Vibration Screen and get.
Specifically, the rotating speed of the coating machine described in step (1) be 60r/min, preheating temperature be 70 DEG C.
Specifically, the discharging described in step (1) is dried in an oven with 50 DEG C.
Specifically, the coating machine rotating speed described in step (2) be 60r/min, heating-up temperature be 60 DEG C.
Test and taken root the phase in wheat, the coated slow-release plant growth regulator 30g that will be made is watered 100kg, stirs,
In foliage-spray 3 times, (wherein, normal control medicament is 5% with active constituent content identical normal control medicament is not sprayed
2,4 dichlorophenoxyacetic acid ethanol solution, 2.85% compound sodium nitrophenolate and Nafusaku is compound aqueous and 2% butyric acid potassium can
Soluble powder) wheat paddock compare, the present embodiment occurs to the growth unrestraint of wheat and poisoning phenomenon, volume increase 26%.
Embodiment 4
Each component is expressed as by weight in the coated slow-release plant growth regulator composition of the present embodiment：Grain diameter is 3-
2, the 4- dichlorphenoxyacetic acids 12g of 4mm, compound sodium nitrophenolate 32g, Nafusaku 28g, butyric acid potassium 18g, tung oil 60g, particle
Footpath<The bamboo charcoal powder 4g of 0.08mm, microwax 30g.
The preparation method of coated slow-release plant growth regulator of the present invention is：
(1) first time coating：By particle diameter for 3-4mm plant growth regulator particle input coating machine in, use hair dryer
Preheating 5min, then tung oil is sprayed on the plant growth regulator particle surface of rolling with high-pressure spray gun, after 5min, to coating machine
Grain diameter is put into rotary drum<The bamboo charcoal powder of 0.08mm, keeps rotating speed and heating-up temperature, is discharged after 5 minutes, must be done after drying
Material；
(2) second coating：During first time coating gained siccative put into coating machine again, sprayed in rotary drum using spray gun
Enter the microwax of heated melting, after microwax has been sprayed, close electric furnace, coating machine keeps rotating speed, is discharged after 10 minutes, must wrap
Film is sustained plant growth regulator.
Specifically, the particle diameter described in step (1) is the plant growth regulator particle and grain diameter of 3-4mm<0.08mm
Bamboo charcoal powder crushed by airslide disintegrating mill, cross rotary screen or Vibration Screen and get.
Specifically, the rotating speed of the coating machine described in step (1) be 60r/min, preheating temperature be 50 DEG C.
Specifically, the discharging described in step (1) is dried in an oven with 50 DEG C.
Specifically, the coating machine rotating speed described in step (2) be 60r/min, heating-up temperature be 80 DEG C.
Test and taken root the phase in wheat, the coated slow-release plant growth regulator 30g that will be made is watered 100kg, stirs,
In foliage-spray 3 times, (wherein, normal control medicament is 5% with active constituent content identical normal control medicament is not sprayed
2,4 dichlorophenoxyacetic acid ethanol solution, 2.85% compound sodium nitrophenolate and Nafusaku is compound aqueous and 2% butyric acid potassium can
Soluble powder) wheat paddock compare, the present embodiment occurs to the growth unrestraint of wheat and poisoning phenomenon, volume increase 27%.
Embodiment 5
Each component is expressed as by weight in the coated slow-release plant growth regulator composition of the present embodiment：Grain diameter is 3-
2, the 4- dichlorphenoxyacetic acids 12g of 4mm, compound sodium nitrophenolate 30g, Nafusaku 30g, butyric acid potassium 18g, tung oil 50g, particle
Footpath<The bamboo charcoal powder 5g of 0.08mm, microwax 25g.
The preparation method of coated slow-release plant growth regulator of the present invention is：
(1) first time coating：By particle diameter for 3-4mm plant growth regulator particle input coating machine in, use hair dryer
Preheating 7min, then tung oil is sprayed on the plant growth regulator particle surface of rolling with high-pressure spray gun, after 4min, to coating machine
Grain diameter is put into rotary drum<The bamboo charcoal powder of 0.08mm, keeps rotating speed and heating-up temperature, is discharged after 8 minutes, must be done after drying
Material；
(2) second coating：During first time coating gained siccative put into coating machine again, sprayed in rotary drum using spray gun
Enter the microwax of heated melting, after microwax has been sprayed, close electric furnace, coating machine keeps rotating speed, is discharged after 7 minutes, must wrap
Film is sustained plant growth regulator.
Specifically, the particle diameter described in step (1) is the plant growth regulator particle and grain diameter of 3-4mm<0.08mm
Bamboo charcoal powder crushed by airslide disintegrating mill, cross rotary screen or Vibration Screen and get.
Specifically, the rotating speed of the coating machine described in step (1) be 60r/min, preheating temperature be 60 DEG C.
Specifically, the discharging described in step (1) is dried in an oven with 50 DEG C.
Specifically, the coating machine rotating speed described in step (2) be 60r/min, heating-up temperature be 70 DEG C.
Test and taken root the phase in wheat, the coated slow-release plant growth regulator 30g that will be made is watered 100kg, stirs,
In foliage-spray 3 times, (wherein, normal control medicament is 5% with active constituent content identical normal control medicament is not sprayed
2,4 dichlorophenoxyacetic acid ethanol solution, 2.85% compound sodium nitrophenolate and Nafusaku is compound aqueous and 2% butyric acid potassium can
Soluble powder) wheat paddock compare, the present embodiment occurs to the growth unrestraint of wheat and poisoning phenomenon, volume increase 25%.
Embodiment 6
Each component is expressed as by weight in the coated slow-release plant growth regulator composition of the present embodiment：Grain diameter is 3-
2, the 4- dichlorphenoxyacetic acids 15g of 4mm, compound sodium nitrophenolate 30g, Nafusaku 30g, butyric acid potassium 15g, tung oil 50g, particle
Footpath<The bamboo charcoal powder 5g of 0.08mm, microwax 25g.
The preparation method of coated slow-release plant growth regulator of the present invention is：
(1) first time coating：By particle diameter for 3-4mm plant growth regulator particle input coating machine in, use hair dryer
Preheating 5min, then tung oil is sprayed on the plant growth regulator particle surface of rolling with high-pressure spray gun, after 5min, to coating machine
Grain diameter is put into rotary drum<The bamboo charcoal powder of 0.08mm, keeps rotating speed and heating-up temperature, is discharged after 10 minutes, must be done after drying
Material；
(2) second coating：During first time coating gained siccative put into coating machine again, sprayed in rotary drum using spray gun
Enter the microwax of heated melting, after microwax has been sprayed, close electric furnace, coating machine keeps rotating speed, is discharged after 5 minutes, must wrap
Film is sustained plant growth regulator.
Specifically, the particle diameter described in step (1) is the plant growth regulator particle and grain diameter of 3-4mm<0.08mm
Bamboo charcoal powder crushed by airslide disintegrating mill, cross rotary screen or Vibration Screen and get.
Specifically, the rotating speed of the coating machine described in step (1) be 60r/min, preheating temperature be 60 DEG C.
Specifically, the discharging described in step (1) is dried in an oven with 50 DEG C.
Specifically, the coating machine rotating speed described in step (2) be 60r/min, heating-up temperature be 70 DEG C.
Test and taken root the phase in wheat, the coated slow-release plant growth regulator 30g that will be made is watered 100kg, stirs,
In foliage-spray 3 times, (wherein, normal control medicament is 5% with active constituent content identical normal control medicament is not sprayed
2,4 dichlorophenoxyacetic acid ethanol solution, 2.85% compound sodium nitrophenolate and Nafusaku is compound aqueous and 2% butyric acid potassium can
Soluble powder) wheat paddock compare, the present embodiment occurs to the growth unrestraint of wheat and poisoning phenomenon, volume increase 28%.
Claims (10)
1. a kind of coated slow-release plant growth regulator, it is characterised in that：The coated slow-release plant growth regulator includes outer layer
Coating, internal layer coating and sandwich layer, the outer layer coating are microwax, and the internal layer coating is tung oil and bamboo charcoal powder, the sandwich layer
It is plant growth regulator, each component is expressed as by weight in its composition：Grain diameter is the plant growth regulator 90 of 3-4mm
Part, tung oil 40-60 parts, grain diameter<Bamboo charcoal powder 4-6 parts of 0.08mm, microwax 20-30 parts.
2. coated slow-release plant growth regulator according to claim 1, it is characterised in that：Described plant growth regulating
Agent is 2,4 dichlorophenoxyacetic acid, compound sodium nitrophenolate, Nafusaku, the mixture of butyric acid potassium compounding.
3. coated slow-release plant growth regulator according to claim 2, it is characterised in that：Described coated slow-release plant
2,4 dichlorophenoxyacetic acid, compound sodium nitrophenolate, Nafusaku, the mass ratio of butyric acid potassium are 2-5 in growth regulator:5-8:5-
10:3-7。
4. coated slow-release plant growth regulator according to claim 1, it is characterised in that：Described plant growth regulating
Agent can also add the micro unit of one or more in ferrous gluconate, zinc sulfate, manganese sulfate, sodium selenite, copper sulphate, boric acid
Element.
5. a kind of preparation method of coated slow-release plant growth regulator, it is characterised in that complete coated slow-release through coating twice
The preparation of plant growth regulator, specifically includes following steps：
(1) first time coating：By particle diameter for 3-4mm plant growth regulator particle input coating machine in, preheated with hair dryer
5-10min, then tung oil is sprayed on the plant growth regulator particle surface of rolling with high-pressure spray gun, after 3-5min, to coating
Grain diameter is put into machine rotary drum<The bamboo charcoal powder of 0.08mm, keeps rotating speed and heating-up temperature, is discharged after 5-10 minutes, after drying
Obtain siccative；
(2) second coating：During siccative prepared by step (1) put into coating machine again, using spray gun to spraying into warp in rotary drum
The microwax of melting is heated, after microwax has been sprayed, electric furnace is closed, coating machine keeps rotating speed, is discharged after 5-10 minutes, obtains coating
Sustained release plant growth regulator.
6. the preparation method of coated slow-release plant growth regulator according to claim 5, it is characterised in that：Step (1)
Described particle diameter is the plant growth regulator particle and grain diameter of 3-4mm<The bamboo charcoal powder of 0.08mm is by airslide disintegrating mill
Crush, cross rotary screen or Vibration Screen is got.
7. the preparation method of coated slow-release plant growth regulator according to claim 5, it is characterised in that：Step (1)
The rotating speed of described coating machine is 60r/min, preheating temperature is 50-70 DEG C.
8. the preparation method of coated slow-release plant growth regulator according to claim 5, it is characterised in that：Step (1)
Described discharging is dried in an oven with 50 DEG C.
9. the preparation method of coated slow-release plant growth regulator according to claim 5, it is characterised in that：Step (2)
Described coating machine rotating speed is 60r/min, heating-up temperature is 60-80 DEG C.
10. a kind of application of coated slow-release plant growth regulator, it is characterised in that：Taken root the phase in wheat, after being watered dilution, in
Foliage-spray 2-3 times.
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| CN110432266A (en) * | 2019-08-28 | 2019-11-12 | 山东辉瀚生物科技有限公司 | A kind of high-efficiency sustained-release pesticide and its production technology |
| CN115735911A (en) * | 2022-11-16 | 2023-03-07 | 中国农业科学院农业环境与可持续发展研究所 | Active agent for promoting crop growth and preparation method and application thereof |
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Application publication date: 20170613 |