CN106809866A - A kind of sugar mill mud high-efficiency comprehensive utilization method and device - Google Patents
A kind of sugar mill mud high-efficiency comprehensive utilization method and device Download PDFInfo
- Publication number
- CN106809866A CN106809866A CN201710072575.8A CN201710072575A CN106809866A CN 106809866 A CN106809866 A CN 106809866A CN 201710072575 A CN201710072575 A CN 201710072575A CN 106809866 A CN106809866 A CN 106809866A
- Authority
- CN
- China
- Prior art keywords
- sugar mill
- mill mud
- sugar
- mud
- comprehensive utilization
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- Pending
Links
- 235000000346 sugar Nutrition 0.000 title claims abstract description 33
- 238000000034 method Methods 0.000 title claims abstract description 26
- 238000001354 calcination Methods 0.000 claims abstract description 19
- 238000009923 sugaring Methods 0.000 claims abstract description 6
- 239000007787 solid Substances 0.000 claims abstract description 5
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 3
- 239000011575 calcium Substances 0.000 claims abstract description 3
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 3
- 230000003647 oxidation Effects 0.000 claims abstract description 3
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 3
- 238000001035 drying Methods 0.000 claims description 16
- 239000002918 waste heat Substances 0.000 claims description 9
- 241000196324 Embryophyta Species 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 5
- 238000011084 recovery Methods 0.000 claims description 4
- 238000001914 filtration Methods 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- 238000003825 pressing Methods 0.000 claims description 3
- 235000007201 Saccharum officinarum Nutrition 0.000 claims description 2
- 240000000111 Saccharum officinarum Species 0.000 claims description 2
- 239000002893 slag Substances 0.000 claims description 2
- 238000007670 refining Methods 0.000 claims 1
- 239000002699 waste material Substances 0.000 abstract description 5
- 239000002910 solid waste Substances 0.000 abstract description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 13
- 239000000292 calcium oxide Substances 0.000 description 9
- 235000012255 calcium oxide Nutrition 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 8
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 6
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 5
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 5
- 235000008733 Citrus aurantifolia Nutrition 0.000 description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 4
- 235000011941 Tilia x europaea Nutrition 0.000 description 4
- 229910002092 carbon dioxide Inorganic materials 0.000 description 4
- 239000004571 lime Substances 0.000 description 4
- 229930006000 Sucrose Natural products 0.000 description 3
- 229910000019 calcium carbonate Inorganic materials 0.000 description 3
- 239000001569 carbon dioxide Substances 0.000 description 3
- 238000003837 high-temperature calcination Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000005720 sucrose Substances 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 238000002309 gasification Methods 0.000 description 1
- 235000021552 granulated sugar Nutrition 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- ZLNQQNXFFQJAID-UHFFFAOYSA-L magnesium carbonate Chemical compound [Mg+2].[O-]C([O-])=O ZLNQQNXFFQJAID-UHFFFAOYSA-L 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910001868 water Inorganic materials 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/02—Oxides or hydroxides
- C01F11/04—Oxides or hydroxides by thermal decomposition
- C01F11/06—Oxides or hydroxides by thermal decomposition of carbonates
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F11/00—Treatment of sludge; Devices therefor
- C02F11/10—Treatment of sludge; Devices therefor by pyrolysis
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/32—Nature of the water, waste water, sewage or sludge to be treated from the food or foodstuff industry, e.g. brewery waste waters
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Treatment Of Sludge (AREA)
Abstract
The present invention relates to industrial solid castoff technical field of comprehensive utilization, a kind of sugar mill mud high-efficiency comprehensive utilization method and device is particularly disclosed.The sugar mill mud high-efficiency comprehensive utilization method, is process object with sugar mill mud, it is characterised in that：The sugar mill mud is dried after crushing, is then fed into high temperature furnace calcining, and calcining heat is 900 1050 DEG C, and calcination time is 20 30min, finally obtains oxidation calcium product.Step of the present invention is simple, easily realizes, solves the treatment problem that carbonatation process sugaring produces a large amount of solid waste filter muds, turns waste into wealth, and has reached the purpose of changing waste into resources.
Description
（One）Technical field
The present invention relates to industrial solid castoff technical field of comprehensive utilization, more particularly to a kind of sugar mill mud high-efficiency comprehensive utilization
Method and device.
（Two）Background technology
Using carbonatation process and sulfurous method both cleaning procedures in current sugar manufacturing industry production, filter mud is that raw sugar liquid is helped with processing
Agent CaO, H2O and CO2The solid waste produced in clarifying process, the process is referred to as full charge in sugar manufacturing industry.Carbonatation process is refined sugar
Technique is to generate CaCO by full charge3Precipitation adsorption effect, with reach removal sugarcane juice in non-sugar material purpose.Produced
Filter mud discharge capacity is big in journey, at present still without thorough, effective processing method, white granulated sugar（Soft white sugar）This large agricultural and sideline product
The treatment of accessory substance in product production process, has a strong impact on and constrains the healthy, quick of sugar industry, sustainable development, make its into
For the hang-up that sugar manufacturing industry faces.The filter mud main component that carbonatation process sugaring is produced is calcium carbonate（CaCO3）, its content
（Butt）It is 80%-85%, containing organic matters such as a small amount of carbohydrates, also including a small amount of magnesium carbonate（MgCO3）, silica（SiO2）, three
Al 2 O（Al2O3）, iron oxide（Fe2O3）Deng mineral matter.
（Three）The content of the invention
The present invention is in order to make up the deficiencies in the prior art, there is provided a kind of step is simple, improve energy utilization rate, and reduction is produced into
This sugar mill mud high-efficiency comprehensive utilization method and device.
The present invention is achieved through the following technical solutions：
A kind of sugar mill mud high-efficiency comprehensive utilization method, is process object with sugar mill mud, it is characterised in that：The sugar mill mud
It is dried after crushing, is then fed into high temperature furnace calcining, calcining heat is 900-1050 DEG C, and calcination time is 20-30min,
Finally obtain oxidation calcium product.
The filter mud that the present invention produces carbonatation process sugaring produces the calcium oxide of high-quality by high-temperature calcination（CaO）, so that
The treatment problem of sugar mill mud is solved, there is huge realistic meaning to current severe environmental pollution situation, technology warp
Ji, society and environmental benefit are notable.
More excellent technical scheme of the invention is：
The sugar mill mud is the solid slag that the refined job shop of sucrose is produced after raw sugar liquid passes through plate-frame filtering, is contained
The moisture of 20-40%, in bulk, bulk footpath is up to 20cm, and sugar mill mud is homogeneous, particle diameter integrated distribution 30-70 μm it
Between, account for gross mass 84.9% of particle diameter less than 80 μm, account for gross mass 4.1% of particle diameter more than 100 μm, under hot conditions easily
Decompose.
The waste heat that the sugar mill mud high-temperature calcination is produced is delivered to drying section, improves energy utilization rate, reduces production
Operating cost.
The device of the method for the invention is realized, including the filter mud of connection sheet frame filter-pressing device is exported, it is characterised in that：Institute
Filter mud outlet connection breaker is stated, the outlet at bottom of breaker connects fluidized bed drying device entrance by conveying device,
The outlet at bottom of fluidized bed drying device connects calciner plant entrance by conveying device.
The calciner plant connects fluidized bed drying device by waste-heat recovery device, realizes the transmission of waste heat.
After the present invention crushes sugar mill mud, it is dried, into high temperature furnace calcining after drying, by adjusting calcining heat
And the time, filter mud is decomposed into calcium oxide and carbon dioxide, the calcium oxide of generation is a kind of Chemical Manufacture raw material of high-quality,
Can be processed with reuse to sucrose, complete the high-efficiency comprehensive utilization of filter mud.
Step of the present invention is simple, easily realizes, solves carbonatation process sugaring and produces the treatment of a large amount of solid waste-filter muds difficult
Topic, turns waste into wealth, and has reached the purpose of changing waste into resources.
（Four）Brief description of the drawings
The present invention is further illustrated below in conjunction with the accompanying drawings.
Fig. 1 is the structural representation of apparatus of the present invention.
In figure, 1 filter mud outlet, 2 breakers, 3 conveying devices, 4 fluidized bed drying devices, 5 calciner plants, 6 waste heats are returned
Receiving apparatus, 7 products.
（Five）Specific embodiment
Accompanying drawing is a kind of specific embodiment of the invention.The embodiment includes the filter mud outlet 1 of connection sheet frame filter-pressing device, described
Filter mud outlet 1 connects breaker 2, and the outlet at bottom of breaker 2 connects fluidized bed drying device 4 and enters by conveying device 3
Mouthful, the outlet at bottom of fluidized bed drying device 4 connects the entrance of calciner plant 5 by conveying device 3；The calciner plant 5 passes through
Waste-heat recovery device 6 connects fluidized bed drying device 4.
Breaker 2 is added at sugaring workshop filter mud outlet 1, by the filter mud bulk crushing after plate and frame filter press press filtration, just
The evaporation of moisture in filter mud is accelerated, reduces the energy consumption in later stage calcination process；Filter mud after broken is transported to through conveying device 3
Fluidized bed drying device 4, the moisture in removal filter mud, reduces calcinating consumption；After being dried through fluidized bed drying device 4, filter mud enters
Enter calciner plant 5, calcined under conditions of 900-1050 DEG C, calcination time is 20-30 minutes, and filter mud is finally decomposed to calcium oxide
And carbon dioxide, the organic substance such as a small amount of sugar contained in filter mud is carbon dioxide, calcining dress by gasification after high-temperature calcination
The waste heat and product cooling waste heat of 5 generations are put by waste-heat recovery device 6 with to fluidized bed drying device 4.
Obtain the quick lime of product 7（Calcium oxide, CaO）Purity is high, in powdered, building, work is can be applied to without crushing
The fields such as industry production, medical treatment.
Filter mud sample composition is：CaCO3Content：80.3%, the content of organic matter：7.8%.
Calcination condition 1：950 DEG C are kept for 30 minutes, and the lime sample of generation is as follows after testing：
；
Calcination condition 2：950 DEG C are kept for 20 minutes, and the lime sample of generation is as follows after testing：
；
Calcination condition 3：1000 DEG C are kept for 20 minutes, and the lime sample of generation is as follows after testing：
；
Calcination condition 4：1000 DEG C are kept for 30 minutes, and the lime sample of generation is as follows after testing：
。
Claims (5)
1. a kind of sugar mill mud high-efficiency comprehensive utilization method, is process object with sugar mill mud, it is characterised in that：The sugaring filter
Mud is dried after crushing, is then fed into high temperature furnace calcining, and calcining heat is 900-1050 DEG C, and calcination time is 20-
30min, finally obtains oxidation calcium product.
2. sugar mill mud high-efficiency comprehensive utilization method according to claim 1, it is characterised in that：The sugar mill mud is sugarcane
The solid slag that sugar refining job shop is produced after raw sugar liquid passes through plate-frame filtering, the moisture containing 20-40%, in bulk,
Bulk footpath is up to 20cm, and sugar mill mud is homogeneous, and account for gross mass 84.9% of particle diameter less than 80 μm, particle diameter is more than 100 μm
Account for the 4.1% of gross mass.
3. sugar mill mud high-efficiency comprehensive utilization method according to claim 1, it is characterised in that：The sugar mill mud high temperature
Calcine the waste heat for producing and be delivered to drying section.
4. the device of claim 1 methods described is realized, including the filter mud of connection sheet frame filter-pressing device is exported（1）, its feature exists
In：The filter mud outlet（1）Connection breaker（2）, breaker（2）Outlet at bottom pass through conveying device（3）Connection flow
Change bed drying device（4）Entrance, fluidized bed drying device（4）Outlet at bottom pass through conveying device（3）Connection calciner plant（5）
Entrance.
5. device according to claim 4, it is characterised in that：The calciner plant（5）By waste-heat recovery device（6）Even
Connect fluidized bed drying device（4）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710072575.8A CN106809866A (en) | 2017-02-10 | 2017-02-10 | A kind of sugar mill mud high-efficiency comprehensive utilization method and device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710072575.8A CN106809866A (en) | 2017-02-10 | 2017-02-10 | A kind of sugar mill mud high-efficiency comprehensive utilization method and device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106809866A true CN106809866A (en) | 2017-06-09 |
Family
ID=59111929
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710072575.8A Pending CN106809866A (en) | 2017-02-10 | 2017-02-10 | A kind of sugar mill mud high-efficiency comprehensive utilization method and device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106809866A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108129002A (en) * | 2018-02-12 | 2018-06-08 | 辛生业 | The sugared mud of suspension sintering method processing realizes the method and device that fining agent recycles |
| CN112648621A (en) * | 2020-12-30 | 2021-04-13 | 大连科林能源工程技术开发有限公司 | System and method for calcining sugar-making filter mud and recycling sugar-making filter mud |
| CN115159938A (en) * | 2022-04-07 | 2022-10-11 | 广西大学 | Method for making air-entrained bricks by combining red mud and sugar-making filter mud |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108129002A (en) * | 2018-02-12 | 2018-06-08 | 辛生业 | The sugared mud of suspension sintering method processing realizes the method and device that fining agent recycles |
| CN108129002B (en) * | 2018-02-12 | 2024-02-20 | 泰安中意重型工业设备有限公司 | Method for treating sugar mud by suspension firing method to realize cyclic utilization of clarifying agent |
| CN112648621A (en) * | 2020-12-30 | 2021-04-13 | 大连科林能源工程技术开发有限公司 | System and method for calcining sugar-making filter mud and recycling sugar-making filter mud |
| CN115159938A (en) * | 2022-04-07 | 2022-10-11 | 广西大学 | Method for making air-entrained bricks by combining red mud and sugar-making filter mud |
| CN115159938B (en) * | 2022-04-07 | 2023-11-03 | 广西产研院智慧农业研究院有限公司 | Method for manufacturing aerated brick by combining red mud and sugar-making filter mud |
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Application publication date: 20170609 |