CN106732168A - A kind of surface activator composition and preparation method thereof - Google Patents
A kind of surface activator composition and preparation method thereof Download PDFInfo
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- CN106732168A CN106732168A CN201611157671.4A CN201611157671A CN106732168A CN 106732168 A CN106732168 A CN 106732168A CN 201611157671 A CN201611157671 A CN 201611157671A CN 106732168 A CN106732168 A CN 106732168A
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- parts
- acid
- activator composition
- surface activator
- glycinebetaine
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K23/00—Use of substances as emulsifying, wetting, dispersing, or foam-producing agents
- C09K23/017—Mixtures of compounds
- C09K23/018—Mixtures of two or more different organic oxygen-containing compounds
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Abstract
The invention discloses a kind of surface activator composition and preparation method thereof, it is made up of following mass fraction formula components：57 parts of glycinebetaine, 48 parts of petroleum ether, 6 10 parts of ethane, 68 parts of sulfuric acid, 57 parts of sulfonic acid, 5 15 parts of n-butanol, 57 parts of hydroxyethyliminodiacetic acid disodium, 79 parts of aspartic acid, 12 parts of auxiliary agent, 35 parts of carboxylate, 15 25 parts of stable emulsion, 57 parts of four sodium of oxalic acid, 68 parts of Isosorbide Dinitrate hydrophobic group, 24 parts of sulfur trioxide, the present invention relates to purposes of the surface activator composition in food, beverage, medicine, cosmetics, personal care product, detergent or cleaning agent.
Description
Technical field
The present invention relates to surfactant field, in particular to a kind of surface activator composition and its preparation side
Method.
Background technology
Surfactant (surface active agents, also referred to as surfactant (tens ide)) is common, and is used for
Wherein it is necessary the surface tension that reduces between two immiscible phases or is wherein necessarily increased one in another phase
In the product and application of solubility.Generally, one of these phases are by water or the mixture rich in water is constituted (water phase), and another
(oil phase) is constituted by liquid phase or solid phase, the oil phase is immiscible in or is insoluble in water by oneself.Surfactant is by being adsorbed onto
Interface between water phase and oil phase, and/or perform their effect by spontaneously forming aggregation (such as liquid crystal or micella).
In order to accomplish this point, it is necessary that but surfactant molecule is made up of two parts for individually connecting；One can
It is dissolved in the hydrophilic parts (" head base ") of water, and an oil-soluble hydrophobic parts (" afterbody ").Molecule it is this dual
Property is referred to as amphipathic.The amphiphilic nature of surfactant molecule will refer to during the hydrophilic parts will preferably rest on water phase, and be somebody's turn to do
Hydrophobic parts will be preferably rested in oil phase.Therefore, surfactant will generally preferably rest on the boundary between water phase and oil phase
At face, therefore reduce the surface tension between the two phases and promote to mix (dispersion) in another phase by one.Should
Another amphipathic effect of surfactant is the ability that it spontaneously forms aggregation.
The content of the invention
The invention provides a kind of surface activator composition and preparation method thereof, the present invention relates to the surfactant
Purposes of the composition in food, beverage, medicine, cosmetics, personal care product, detergent or cleaning agent.
To achieve the above object, the present invention provides following technical scheme：
A kind of surface activator composition and preparation method thereof, is made up of following mass fraction formula components：Glycine is sweet
5-7 parts of dish alkali, petroleum ether 4-8 parts, ethane 6-10 parts, sulfuric acid 6-8 parts, sulfonic acid 5-7 parts, n-butanol 5-15 parts, ethoxy imido
5-7 parts of base diethyl acid disodium, aspartic acid 7-9 parts, auxiliary agent 1-2 parts, carboxylate 3-5 parts, stable emulsion 15-25 parts, oxalic acid
Four sodium 5-7 parts, 6-8 parts, sulfur trioxide 2-4 parts of Isosorbide Dinitrate hydrophobic groups.
Further：It is made up of following mass fraction formula components：5 parts of glycinebetaine, 4 parts of petroleum ether, 6 parts of ethane,
6 parts of sulfuric acid, 5 parts of sulfonic acid, 5 parts of n-butanol, 5 parts of hydroxyethyliminodiacetic acid disodium, 7 parts of aspartic acid, 1 part of auxiliary agent, carboxylic acid
3 parts of salt, 15 parts of stable emulsion, 5 parts of four sodium of oxalic acid, 6 parts of Isosorbide Dinitrate hydrophobic group, 2 parts of sulfur trioxide.
Further：It is made up of following mass fraction formula components：6 parts of glycinebetaine, 6 parts of petroleum ether, 8 parts of ethane,
7 parts of sulfuric acid, 6 parts of sulfonic acid, 10 parts of n-butanol, 6 parts of hydroxyethyliminodiacetic acid disodium, 8 parts of aspartic acid, 1.5 parts of auxiliary agent, carboxylic
4 parts of hydrochlorate, 20 parts of stable emulsion, 6 parts of four sodium of oxalic acid, 7 parts of Isosorbide Dinitrate hydrophobic group, 3 parts of sulfur trioxide.
Further：It is made up of following mass fraction formula components：7 parts of glycinebetaine, 8 parts of petroleum ether, 10 parts of ethane,
8 parts of sulfuric acid, 7 parts of sulfonic acid, 15 parts of n-butanol, 7 parts of hydroxyethyliminodiacetic acid disodium, 9 parts of aspartic acid, 2 parts of auxiliary agent, carboxylic acid
5 parts of salt, 25 parts of stable emulsion, 7 parts of four sodium of oxalic acid, 8 parts of Isosorbide Dinitrate hydrophobic group, 4 parts of sulfur trioxide.
Further：Preparation method of the present invention has following steps：
Step one, by the presence of institute's glycinebetaine and hydroxyethyliminodiacetic acid disodium and reaction temperature be 85~
160 DEG C, less than being reacted under the conditions of 0.80MPa gauge pressures, reaction terminates pressure, makes reactant mixture with the desired amount of epoxy second
Alkane is 85~160 DEG C in reaction temperature, and pressure obtains the alkylol or alkyl less than react under the conditions of 0.80MPa gauge pressures
Phenol polyoxyethylene polyoxypropylene ether, wherein catalyst amount are the 0.5~5% of alkylol or alkyl phenol quality；
Step 2, by step one gained surplus stock be well mixed, obtain required composition.
The beneficial effects of the invention are as follows：The present invention relates to the surface activator composition in food, beverage, medicine, change
Purposes in cosmetic, personal care product, detergent or cleaning agent.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
Embodiment one：
A kind of surface activator composition is made up of following mass fraction formula components：Glycinebetaine 5-7 parts, oil
Ether 4-8 parts, ethane 6-10 parts, sulfuric acid 6-8 parts, sulfonic acid 5-7 parts, n-butanol 5-15 parts, hydroxyethyliminodiacetic acid disodium 5-7
Part, aspartic acid 7-9 part, auxiliary agent 1-2 parts, carboxylate 3-5 parts, stable emulsion 15-25 parts, sodium 5-7 parts of oxalic acid four, be dehydrated mountain
6-8 parts, sulfur trioxide 2-4 parts of pears alcohol ester hydrophobic group.
Embodiment two：
A kind of surface activator composition is made up of following mass fraction formula components：5 parts of glycinebetaine, petroleum ether
4 parts, 6 parts of ethane, 6 parts of sulfuric acid, 5 parts of sulfonic acid, 5 parts of n-butanol, 5 parts of hydroxyethyliminodiacetic acid disodium, 7 parts of aspartic acid,
1 part of auxiliary agent, 3 parts of carboxylate, 15 parts of stable emulsion, 5 parts of four sodium of oxalic acid, 6 parts of Isosorbide Dinitrate hydrophobic group, sulfur trioxide 2
Part.
Embodiment three：
A kind of surface activator composition is made up of following mass fraction formula components：6 parts of glycinebetaine, petroleum ether
6 parts, 8 parts of ethane, 7 parts of sulfuric acid, 6 parts of sulfonic acid, 10 parts of n-butanol, 6 parts of hydroxyethyliminodiacetic acid disodium, 8 parts of aspartic acid,
1.5 parts of auxiliary agent, 4 parts of carboxylate, 20 parts of stable emulsion, 6 parts of four sodium of oxalic acid, 7 parts of Isosorbide Dinitrate hydrophobic group, sulfur trioxide
3 parts.
Example IV：
A kind of surface activator composition is made up of following mass fraction formula components：7 parts of glycinebetaine, petroleum ether
8 parts, 10 parts of ethane, 8 parts of sulfuric acid, 7 parts of sulfonic acid, 15 parts of n-butanol, 7 parts of hydroxyethyliminodiacetic acid disodium, aspartic acid 9
Part, 2 parts of auxiliary agent, 5 parts of carboxylate, 25 parts of stable emulsion, 7 parts of four sodium of oxalic acid, 8 parts of Isosorbide Dinitrate hydrophobic group, three oxidations
4 parts of sulphur.
Embodiment five：
A kind of preparation method preparation method of surface activator composition comprises the following steps：
Step one, by the presence of institute's glycinebetaine and hydroxyethyliminodiacetic acid disodium and reaction temperature be 85~
160 DEG C, less than being reacted under the conditions of 0.80MPa gauge pressures, reaction terminates pressure, makes reactant mixture with the desired amount of epoxy second
Alkane is 85~160 DEG C in reaction temperature, and pressure obtains the alkylol or alkyl less than react under the conditions of 0.80MPa gauge pressures
Phenol polyoxyethylene polyoxypropylene ether, wherein catalyst amount are the 0.5~5% of alkylol or alkyl phenol quality；
Step 2, by step one gained surplus stock be well mixed, obtain required composition.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each implementation method is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should
Specification an as entirety, the technical scheme in each embodiment can also be formed into those skilled in the art through appropriately combined
May be appreciated other embodiment.
Claims (5)
1. a kind of surface activator composition, it is characterised in that：It is made up of following mass fraction formula components：
Glycinebetaine 5-7 parts, petroleum ether 4-8 parts, ethane 6-10 parts, sulfuric acid 6-8 parts, sulfonic acid 5-7 parts, n-butanol 5-15
Part, 5-7 parts of hydroxyethyliminodiacetic acid disodium, aspartic acid 7-9 parts, auxiliary agent 1-2 parts, carboxylate 3-5 parts, stable emulsion
15-25 parts, sodium 5-7 parts of oxalic acid four, 6-8 parts, sulfur trioxide 2-4 parts of Isosorbide Dinitrate hydrophobic group.
2. a kind of surface activator composition according to claim 1, it is characterised in that：It is formulated into by following mass fraction
It is grouped into：
5 parts of glycinebetaine, 4 parts of petroleum ether, 6 parts of ethane, 6 parts of sulfuric acid, 5 parts of sulfonic acid, 5 parts of n-butanol, ethoxy imino group
5 parts of diethyl acid disodium, 7 parts of aspartic acid, 1 part of auxiliary agent, 3 parts of carboxylate, 15 parts of stable emulsion, 5 parts of four sodium of oxalic acid, dehydration mountain
6 parts of pears alcohol ester hydrophobic group, 2 parts of sulfur trioxide.
3. a kind of surface activator composition according to claim 1, it is characterised in that：It is formulated into by following mass fraction
It is grouped into：
6 parts of glycinebetaine, 6 parts of petroleum ether, 8 parts of ethane, 7 parts of sulfuric acid, 6 parts of sulfonic acid, 10 parts of n-butanol, ethoxy imino group
6 parts of diethyl acid disodium, 8 parts of aspartic acid, 1.5 parts of auxiliary agent, 4 parts of carboxylate, 20 parts of stable emulsion, 6 parts of four sodium of oxalic acid, dehydration
7 parts of sorbitol ester hydrophobic group, 3 parts of sulfur trioxide.
4. a kind of surface activator composition according to claim 1, it is characterised in that：It is formulated into by following mass fraction
It is grouped into：
7 parts of glycinebetaine, 8 parts of petroleum ether, 10 parts of ethane, 8 parts of sulfuric acid, 7 parts of sulfonic acid, 15 parts of n-butanol, ethoxy imido
7 parts of base diethyl acid disodium, 9 parts of aspartic acid, 2 parts of auxiliary agent, 5 parts of carboxylate, 25 parts of stable emulsion, 7 parts of four sodium of oxalic acid, dehydration
8 parts of sorbitol ester hydrophobic group, 4 parts of sulfur trioxide.
5. a kind of a kind of preparation method of surface activator composition according to claim 1, it is characterised in that：Including such as
Lower step：
Step one, by the presence of institute's glycinebetaine and hydroxyethyliminodiacetic acid disodium and reaction temperature be 85~160
DEG C, less than being reacted under the conditions of 0.80MPa gauge pressures, reaction terminates pressure, makes reactant mixture with the desired amount of oxirane
It it is 85~160 DEG C in reaction temperature, pressure obtains the alkylol or alkyl phenol less than react under the conditions of 0.80MPa gauge pressures
Polyoxyethylene polyoxypropylene ether, wherein catalyst amount are the 0.5~5% of alkylol or alkyl phenol quality；
Step 2, by step one gained surplus stock be well mixed, obtain required composition.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118299548A (en) * | 2024-06-04 | 2024-07-05 | 深圳市量能科技有限公司 | Positive electrode material of wide-temperature nickel-hydrogen battery and preparation method of wide-temperature nickel-hydrogen battery |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5177256A (en) * | 1990-02-27 | 1993-01-05 | Kao Corporation | Betaine compound and detergent composition |
| WO1997007089A1 (en) * | 1995-08-12 | 1997-02-27 | HÜLS Aktiengesellschaft | Amphiphilic compounds with several hydrophilic and hydrophobic groups based on aminosuccinic acid derivatives |
| CN1217187A (en) * | 1998-11-13 | 1999-05-26 | 王玉万 | Anti-parasite oral spray containing evericin and ivermectin for sheep |
| CN101607183A (en) * | 2008-06-20 | 2009-12-23 | 中国科学院成都有机化学有限公司 | Carboxylic acid betaine type gemini surfactant and preparation method |
| CN102670459A (en) * | 2012-06-06 | 2012-09-19 | 桑达化工（南通）有限公司 | Anti-winkle lotion |
| CN103254872B (en) * | 2012-09-12 | 2015-01-14 | 韩国绿色原料株式会社 | Oily dust preventive composition, preparation method and purpose for preventing dust from flying |
-
2016
- 2016-12-15 CN CN201611157671.4A patent/CN106732168A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5177256A (en) * | 1990-02-27 | 1993-01-05 | Kao Corporation | Betaine compound and detergent composition |
| WO1997007089A1 (en) * | 1995-08-12 | 1997-02-27 | HÜLS Aktiengesellschaft | Amphiphilic compounds with several hydrophilic and hydrophobic groups based on aminosuccinic acid derivatives |
| CN1217187A (en) * | 1998-11-13 | 1999-05-26 | 王玉万 | Anti-parasite oral spray containing evericin and ivermectin for sheep |
| CN101607183A (en) * | 2008-06-20 | 2009-12-23 | 中国科学院成都有机化学有限公司 | Carboxylic acid betaine type gemini surfactant and preparation method |
| CN102670459A (en) * | 2012-06-06 | 2012-09-19 | 桑达化工（南通）有限公司 | Anti-winkle lotion |
| CN103254872B (en) * | 2012-09-12 | 2015-01-14 | 韩国绿色原料株式会社 | Oily dust preventive composition, preparation method and purpose for preventing dust from flying |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118299548A (en) * | 2024-06-04 | 2024-07-05 | 深圳市量能科技有限公司 | Positive electrode material of wide-temperature nickel-hydrogen battery and preparation method of wide-temperature nickel-hydrogen battery |
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Application publication date: 20170531 |