CN106629909A - Industrial sewage treatment agent and preparation method thereof - Google Patents
Industrial sewage treatment agent and preparation method thereof Download PDFInfo
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- CN106629909A CN106629909A CN201611157728.0A CN201611157728A CN106629909A CN 106629909 A CN106629909 A CN 106629909A CN 201611157728 A CN201611157728 A CN 201611157728A CN 106629909 A CN106629909 A CN 106629909A
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- parts
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- industrial sewage
- sewage treatment
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- 239000010865 sewage Substances 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 26
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 21
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 239000001632 sodium acetate Substances 0.000 claims abstract description 19
- 235000017281 sodium acetate Nutrition 0.000 claims abstract description 19
- 239000000440 bentonite Substances 0.000 claims abstract description 16
- 229910000278 bentonite Inorganic materials 0.000 claims abstract description 16
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000011780 sodium chloride Substances 0.000 claims abstract description 13
- 239000001488 sodium phosphate Substances 0.000 claims abstract description 13
- 229910000162 sodium phosphate Inorganic materials 0.000 claims abstract description 13
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 claims abstract description 13
- AEQDJSLRWYMAQI-UHFFFAOYSA-N 2,3,9,10-tetramethoxy-6,8,13,13a-tetrahydro-5H-isoquinolino[2,1-b]isoquinoline Chemical compound C1CN2CC(C(=C(OC)C=C3)OC)=C3CC2C2=C1C=C(OC)C(OC)=C2 AEQDJSLRWYMAQI-UHFFFAOYSA-N 0.000 claims abstract description 12
- SURQXAFEQWPFPV-UHFFFAOYSA-L iron(2+) sulfate heptahydrate Chemical compound O.O.O.O.O.O.O.[Fe+2].[O-]S([O-])(=O)=O SURQXAFEQWPFPV-UHFFFAOYSA-L 0.000 claims abstract description 12
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 12
- 239000000176 sodium gluconate Substances 0.000 claims abstract description 12
- 235000012207 sodium gluconate Nutrition 0.000 claims abstract description 12
- 229940005574 sodium gluconate Drugs 0.000 claims abstract description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims abstract description 10
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 15
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims description 15
- WBYWAXJHAXSJNI-VOTSOKGWSA-M .beta-Phenylacrylic acid Natural products [O-]C(=O)\C=C\C1=CC=CC=C1 WBYWAXJHAXSJNI-VOTSOKGWSA-M 0.000 claims description 12
- WBYWAXJHAXSJNI-SREVYHEPSA-N Cinnamic acid Chemical compound OC(=O)\C=C/C1=CC=CC=C1 WBYWAXJHAXSJNI-SREVYHEPSA-N 0.000 claims description 12
- 229930016911 cinnamic acid Natural products 0.000 claims description 12
- 235000013985 cinnamic acid Nutrition 0.000 claims description 12
- WBYWAXJHAXSJNI-UHFFFAOYSA-N methyl p-hydroxycinnamate Natural products OC(=O)C=CC1=CC=CC=C1 WBYWAXJHAXSJNI-UHFFFAOYSA-N 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 5
- 231100000252 nontoxic Toxicity 0.000 abstract description 3
- 230000003000 nontoxic effect Effects 0.000 abstract description 3
- 230000036632 reaction speed Effects 0.000 abstract description 3
- 231100000331 toxic Toxicity 0.000 abstract description 3
- 230000002588 toxic effect Effects 0.000 abstract description 3
- KJPRLNWUNMBNBZ-QPJJXVBHSA-N (E)-cinnamaldehyde Chemical compound O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- 230000001580 bacterial effect Effects 0.000 abstract 1
- 229910021538 borax Inorganic materials 0.000 abstract 1
- 230000007797 corrosion Effects 0.000 abstract 1
- 238000005260 corrosion Methods 0.000 abstract 1
- 231100000614 poison Toxicity 0.000 abstract 1
- 235000010339 sodium tetraborate Nutrition 0.000 abstract 1
- 239000003440 toxic substance Substances 0.000 abstract 1
- BSVBQGMMJUBVOD-UHFFFAOYSA-N trisodium borate Chemical compound [Na+].[Na+].[Na+].[O-]B([O-])[O-] BSVBQGMMJUBVOD-UHFFFAOYSA-N 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 3
- 241000894006 Bacteria Species 0.000 description 2
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 2
- 230000001473 noxious effect Effects 0.000 description 2
- 239000011574 phosphorus Substances 0.000 description 2
- 229910052698 phosphorus Inorganic materials 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 229940037003 alum Drugs 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 239000000498 cooling water Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- UPMFZISCCZSDND-JJKGCWMISA-M sodium gluconate Chemical compound [Na+].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O UPMFZISCCZSDND-JJKGCWMISA-M 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses an industrial sewage treatment agent and a preparation method thereof. The industrial sewage treatment agent consists of the following components in parts by mass: 18 to 20 parts of polymeric aluminum silicate-sulfate, 10 to 15 parts of anisaldehyde, 13 to 17 parts of sodium borate, 12 to 14 parts of sodium acetate, 4 to 6 parts of porous suspended spheres, 16 to 18 parts of sodium phosphate, 4 to 6 parts of sodium chloride, 5 to 15 parts of cinnamyl aldehyde, 5 to 7 parts of polyferric chloride, 6 to 10 parts of copperas, 6 to 8 parts of bentonite and 6 to 8 parts of sodium gluconate. According to the industrial sewage treatment agent and the preparation method thereof, the reaction speed is high, and toxic and harmful gas is avoided in the reaction process; and a product after the reaction is stable and is not decomposed into toxic substances. The industrial sewage treatment agent can be discharged into a sewage treatment plant, does not damage active bacterial in the sewage treatment plant, is shock-free to the sewage treatment plant, is efficient and non-toxic, is safe for a human body before and after reaction and avoids corrosion to equipment; and the use method is simple and convenient, the process flow is not modified, and equipment and addition materials do not need to be added.
Description
Technical field
The present invention relates to technical field of sewage, in particular to a kind of industrial sewage treating agent and its preparation side
Method.
Background technology
The problems such as sewage disposal technology is to water saving, energy-conservation has a very important role, but while sewage treatment drug
Also affect to environment during use.In cooling water system, under water temperature is higher than the various occasions of environment temperature,
The fouling of the inorganic salts such as calcium carbonate can bring serious consequence.In recent years, in water treatment field, using alkalescence, pH is not adjusted
The water technology of value is growing, wherein adding corrosion-mitigation scale-inhibition medicament, the application of low-phosphorous, without phosphorus formula is more and more extensive, nothing
The green water treatment agent of phosphorus has become the hot subject in terms of domestic and international water treatment agent research.Scientific utilization water treatment agent can
Effectively anticorrosion and fouling is prevented, the purpose of saving water source and the energy is reached so as to improve the utilization rate of equipment and water.
The content of the invention
The invention provides a kind of industrial sewage treating agent and preparation method thereof, reaction speed of the present invention is fast, course of reaction
It is middle to produce without toxic and harmful；Reacted product is stablized, and will not be further decomposed into noxious material.Can directly at sewage effluent
Reason field, does not damage the active bacteria in sewage farm, to sewage farm without impact；Efficiently, it is nontoxic, human body is pacified before and after reaction
Entirely, it is corrosion-free to equipment；Using method simplicity does not change technological process, without the need for increasing equipment and additional materials.
For achieving the above object, the present invention provides following technical scheme：
A kind of industrial sewage treating agent and preparation method thereof, is made up of following mass fraction formula components：Polymeric aluminum sulfate silicate
18-20 parts, anisaldehyde 10-15 parts, Boratex 13-17 parts, sodium acetate 12-14 parts, porous suspended ball 4-6 parts, sodium phosphate 16-18
Part, sodium chloride 4-6 parts, cinnamic acid 5-15 parts, polyferric chloride 5-7 parts, green vitriol 6-10 parts, bentonite 6-8 parts, gluconic acid
Sodium 6-8 parts.
Further：It is made up of following mass fraction formula components：18 parts of polymeric aluminum sulfate silicate, 10 parts of anisaldehyde, Boratex 13
It is part, 12 parts of sodium acetate, 4 parts of porous suspended ball, 16 parts of sodium phosphate, 4 parts of sodium chloride, 5 parts of cinnamic acid, 5 parts of polyferric chloride, green
6 parts of alum, 6 parts of bentonite, 6 parts of sodium gluconate.
Further：It is made up of following mass fraction formula components：19 parts of polymeric aluminum sulfate silicate, 12.5 parts of anisaldehyde, Boratex
15 parts, 13 parts of sodium acetate, 5 parts of porous suspended ball, 17 parts of sodium phosphate, 5 parts of sodium chloride, 10 parts of cinnamic acid, polyferric chloride 6
Part, 8 parts of green vitriol, 7 parts of bentonite, 7 parts of sodium gluconate.
Further：It is made up of following mass fraction formula components：20 parts of polymeric aluminum sulfate silicate, 15 parts of anisaldehyde, Boratex 17
Part, 14 parts of sodium acetate, 6 parts of porous suspended ball, 18 parts of sodium phosphate, 6 parts of sodium chloride, 15 parts of cinnamic acid, 7 parts of polyferric chloride,
10 parts of green vitriol, 8 parts of bentonite, 8 parts of sodium gluconate.
Further：Preparation method of the present invention has following steps：
Step one, raw material are measured according to above-mentioned mass fraction, check mixer, add secondary water；
Step 2, sodium acetate is slowly added in mixer, records mixing time, fed intake to sodium acetate from mixer is opened
It is 5～10 minutes the time required to terminating；
Step 3, by polymeric aluminum sulfate silicate be slowly added in mixer stir；
Slow input bentonite under step 4, normal pressure, control maximum temperature is less than 60 DEG C, when reaction temperature rise compared with
When fast, slow down charging rate, until charging terminates, whole course of reaction was completed in 40 minutes；
Slow input surplus stock under step 5, normal pressure, control maximum temperature is less than 60 DEG C, when reaction temperature rises
When very fast, slow down charging rate, until charging terminates, whole course of reaction was completed in 40 minutes, pH is controlled between 3～6,
Stop mixer, examination and test of products packaging.
The invention has the beneficial effects as follows：
1st, reaction speed of the present invention is fast, produces without toxic and harmful in course of reaction；
2nd, reacted product is stablized, and will not be further decomposed into noxious material.Can direct sewage effluent Treatment stations, do not damage
The active bacteria in sewage farm, to sewage farm without impact；
3rd, it is efficient, nontoxic, it is safe to the human body before and after reaction, it is corrosion-free to equipment；
4th, using method simplicity does not change technological process, without the need for increasing equipment and additional materials.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the invention, rather than the embodiment of whole.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
Embodiment one：
A kind of industrial sewage treating agent is made up of following mass fraction formula components：Polymeric aluminum sulfate silicate 18-20 parts, anisaldehyde
10-15 parts, Boratex 13-17 parts, sodium acetate 12-14 parts, porous suspended ball 4-6 parts, sodium phosphate 16-18 parts, sodium chloride 4-6
Part, cinnamic acid 5-15 parts, polyferric chloride 5-7 parts, green vitriol 6-10 parts, bentonite 6-8 parts, sodium gluconate 6-8 parts.
Embodiment two：
A kind of industrial sewage treating agent is made up of following mass fraction formula components：18 parts of polymeric aluminum sulfate silicate, anisaldehyde 10
Part, 13 parts of Boratex, 12 parts of sodium acetate, 4 parts of porous suspended ball, 16 parts of sodium phosphate, 4 parts of sodium chloride, 5 parts of cinnamic acid, polymerization three
5 parts of iron chloride, 6 parts of green vitriol, 6 parts of bentonite, 6 parts of sodium gluconate.
Embodiment three：
A kind of industrial sewage treating agent is made up of following mass fraction formula components：19 parts of polymeric aluminum sulfate silicate, anisaldehyde
12.5 parts, it is 15 parts of Boratex, 13 parts of sodium acetate, 5 parts of porous suspended ball, 17 parts of sodium phosphate, 5 parts of sodium chloride, 10 parts of cinnamic acid, poly-
Close 6 parts of ferric trichloride, 8 parts of green vitriol, 7 parts of bentonite, 7 parts of sodium gluconate.
Example IV：
A kind of industrial sewage treating agent is made up of following mass fraction formula components：20 parts of polymeric aluminum sulfate silicate, anisaldehyde 15
Part, 17 parts of Boratex, 14 parts of sodium acetate, 6 parts of porous suspended ball, 18 parts of sodium phosphate, 6 parts of sodium chloride, 15 parts of cinnamic acid, polymerization three
7 parts of iron chloride, 10 parts of green vitriol, 8 parts of bentonite, 8 parts of sodium gluconate.
Embodiment five：
A kind of preparation method preparation method of industrial sewage treating agent comprises the steps：
Step one, raw material are measured according to above-mentioned mass fraction, check mixer, add secondary water；
Step 2, sodium acetate is slowly added in mixer, records mixing time, fed intake to sodium acetate from mixer is opened
It is 5～10 minutes the time required to terminating；
Step 3, by polymeric aluminum sulfate silicate be slowly added in mixer stir；
Slow input bentonite under step 4, normal pressure, control maximum temperature is less than 60 DEG C, when reaction temperature rise compared with
When fast, slow down charging rate, until charging terminates, whole course of reaction was completed in 40 minutes；
Slow input surplus stock under step 5, normal pressure, control maximum temperature is less than 60 DEG C, when reaction temperature rises
When very fast, slow down charging rate, until charging terminates, whole course of reaction was completed in 40 minutes, pH is controlled between 3～6,
Stop mixer, examination and test of products packaging.
Moreover, it will be appreciated that although this specification is been described by according to embodiment, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity those skilled in the art should
Using specification as an entirety, the technical scheme in each embodiment can also Jing it is appropriately combined, form those skilled in the art
Understandable other embodiment.
Claims (5)
1. a kind of industrial sewage treating agent, it is characterised in that：It is made up of following mass fraction formula components：
Polymeric aluminum sulfate silicate 18-20 parts, anisaldehyde 10-15 parts, Boratex 13-17 parts, sodium acetate 12-14 parts, porous suspended ball 4-6
Part, sodium phosphate 16-18 parts, sodium chloride 4-6 parts, cinnamic acid 5-15 parts, polyferric chloride 5-7 parts, green vitriol 6-10 parts, bentonite
6-8 parts, sodium gluconate 6-8 parts.
2. a kind of industrial sewage treating agent according to claim 1, it is characterised in that：By following mass fraction formula components
Composition：
18 parts of polymeric aluminum sulfate silicate, 10 parts of anisaldehyde, 13 parts of Boratex, 12 parts of sodium acetate, 4 parts of porous suspended ball, 16 parts of sodium phosphate,
4 parts of sodium chloride, 5 parts of cinnamic acid, 5 parts of polyferric chloride, 6 parts of green vitriol, 6 parts of bentonite, 6 parts of sodium gluconate.
3. a kind of industrial sewage treating agent according to claim 1, it is characterised in that：By following mass fraction formula components
Composition：
19 parts of polymeric aluminum sulfate silicate, 12.5 parts of anisaldehyde, 15 parts of Boratex, 13 parts of sodium acetate, 5 parts of porous suspended ball, sodium phosphate 17
Part, 5 parts of sodium chloride, 10 parts of cinnamic acid, 6 parts of polyferric chloride, 8 parts of green vitriol, 7 parts of bentonite, 7 parts of sodium gluconate.
4. a kind of industrial sewage treating agent according to claim 1, it is characterised in that：By following mass fraction formula components
Composition：
20 parts of polymeric aluminum sulfate silicate, 15 parts of anisaldehyde, 17 parts of Boratex, 14 parts of sodium acetate, 6 parts of porous suspended ball, 18 parts of sodium phosphate,
6 parts of sodium chloride, 15 parts of cinnamic acid, 7 parts of polyferric chloride, 10 parts of green vitriol, 8 parts of bentonite, 8 parts of sodium gluconate.
5. a kind of a kind of preparation method of industrial sewage treating agent according to claim 1, it is characterised in that：Including as follows
Step：
Step one, raw material are measured according to above-mentioned mass fraction, check mixer, add secondary water；
Step 2, sodium acetate is slowly added in mixer, records mixing time, fed intake end to sodium acetate from mixer is opened
Required time is 5～10 minutes；
Step 3, by polymeric aluminum sulfate silicate be slowly added in mixer stir；
Bentonite is slowly put under step 4, normal pressure, control maximum temperature is less than 60 DEG C, when reaction temperature rises comparatively fast
When, slow down charging rate, until charging terminates, whole course of reaction was completed in 40 minutes；
Surplus stock is slowly put under step 5, normal pressure, control maximum temperature is less than 60 DEG C, when reaction temperature rises comparatively fast
When, slow down charging rate, until charging terminates, whole course of reaction was completed in 40 minutes, and pH is controlled between 3～6, was stopped
Mixer, examination and test of products packaging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611157728.0A CN106629909A (en) | 2016-12-15 | 2016-12-15 | Industrial sewage treatment agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611157728.0A CN106629909A (en) | 2016-12-15 | 2016-12-15 | Industrial sewage treatment agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106629909A true CN106629909A (en) | 2017-05-10 |
Family
ID=58822680
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611157728.0A Pending CN106629909A (en) | 2016-12-15 | 2016-12-15 | Industrial sewage treatment agent and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN106629909A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108821410A (en) * | 2018-07-02 | 2018-11-16 | 安庆丰源化工有限公司 | A kind of efficient industrial sewage treating agent and preparation method thereof |
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