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CN105496812B - A kind of clear aqueous discoloration BB frost and preparation method of oil-containing - Google Patents

A kind of clear aqueous discoloration BB frost and preparation method of oil-containing Download PDF

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Publication number
CN105496812B
CN105496812B CN201510981376.XA CN201510981376A CN105496812B CN 105496812 B CN105496812 B CN 105496812B CN 201510981376 A CN201510981376 A CN 201510981376A CN 105496812 B CN105496812 B CN 105496812B
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Prior art keywords
phase
frost
oil
discoloration
revolving speed
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CN201510981376.XA
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CN105496812A (en
Inventor
侯剑峰
孙晋喜
秦福燕
林莉
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Bio R & D Center (suzhou Industrial Park) Co Ltd
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Bio R & D Center (suzhou Industrial Park) Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • A61K8/585Organosilicon compounds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of clear aqueous discoloration BB of oil-containing frosts and preparation method, the BB frost to be mixed and be prepared by A oil phase, B water phase, C phase and D, and oil-in-water clear gel system is made.The clear aqueous discoloration BB frost of oil-containing provided by the invention, performance is mild, reaches the moist degree of general lotion or cream, also has the function of the sliding skin sense of silk and concealing while using, repairs face discoloration.

Description

A kind of clear aqueous discoloration BB frost and preparation method of oil-containing
Technical field
The present invention relates to cosmetic technical field, in particular to the clear aqueous discoloration BB frost of a kind of oil-containing and preparation side Method.
Background technique
The BB frost of market is many kinds of, and more and more consumers wishes that BB frost possesses more functions.Traditional BB frost Mainly based on Water-In-Oil or silicon Water-In-Oil, the disadvantage is that spreadability is poor, appearance is not novel enough.The gel BB of aqueous transparent White system can be dry and astringent with rear skin because not containing oil, itches, the clear aqueous gel of oil-containing, can be living containing a large amount of surface Property agent, certain irritation may be brought to consumer skin, and oil content is not high, it is general to moisten degree, the present invention therefore and Come.
Summary of the invention
One of the object of the invention is to provide a kind of clear aqueous discoloration BB frost of oil-containing, is used with solving BB frost in the prior art Skin is dry and astringent afterwards, the problems such as itching.
It is a further object of the present invention to provide a kind of preparation methods of the clear aqueous discoloration BB frost of oil-containing.
Based on the above issues, technical solution provided by the invention first is that:
A kind of clear aqueous discoloration BB frost of oil-containing, is mixed by A phase, B phase, C phase and D and is prepared,
Wherein, A phase is oily phase, by weight percentage includes following components:
Silicone oil: 9.00%~30.00%,
Dimethicone/Vinyl Dimethicone cross-linked polymer: 0.50%~2.00%,
Hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers: 0.50~2.00%,
Wherein, B phase is water phase, by weight percentage includes following components:
Purified water: 15.00%~76.00%
Propylene glycol: 20.00%~50.00%,
1,3-PD: 1.00%~10.00%,
Ammonium acryloyl taurate/VP copolymer: 0.10%~2.00%;
Wherein, C phase includes following components according to weight percent:
Essence: 0.03%~0.5%,
PE9010:0.50%~1.00%,
Algae extract: 0.50%~5.00%,
Glycine betaine: 0.50%~2.00%.
Sodium Hyaluronate: 0.001%~0.05%
Wherein, D phase is discoloration BB frost particle: 1.00%~10.00%,
The sum of above each raw material weight percentage is 100%.
In one of them embodiment, the silicone oil is cyclic silicone oils or low viscous dimethicone.
In one of them embodiment, the discoloration BB frost particle is by CI 77492, CI 77491, CI 77499, CI 77891 and coating composition.
It is provided by the invention another solution is that
A kind of preparation method of the clear aqueous discoloration BB frost of oil-containing, comprising the following steps:
(1) it is added after mixing A phase each component according to dosage part in oily phase pot, is stirred with the revolving speed of 10~50rpm/min 10~60min is to stirring evenly;
(2) by B phase each component purified water, propylene glycol, 1,3-PD, ammonium acryloyl taurate/VP copolymer It is sequentially added in vacuum emulsification pot according to dosage part, 10~60min is stirred with the revolving speed of 30~35rpm/min, keeps vacuum, so Afterwards with homogeneous 10~60min of speed homogeneous of 2600~3100rpm/min to be uniformly mixed;
(3) raw material of oily phase pot is pumped into vacuum emulsification pot by strainer valve, is stirred with the revolving speed of 25~35rpm/min 10~30min forms transparent and homogeneous gel;
(4) C phase each component essence, PE9010, algae extract, glycine betaine are sequentially added into vacuum emulsification pot according to dosage part In, 10~60min is stirred with the revolving speed of 10~50rpm/min, is discharged after mixing evenly;
(5) mixture made from step (4) is placed in open storage tank, is stirred in the revolving speed of 100~150rpm/min Under the conditions of, D phase is added and changes colour BB particle, inspection after mixing evenly;
(6) it is filling after detection is qualified.
Compared with prior art, the invention has the advantages that
1. using technical solution of the present invention, which is oil-in-water clear gel system, is added in formula water phase polynary The moisture-keeping efficacy of product can be improved in alcohol, glycine betaine and Sodium Hyaluronate, and the discoloration BB frost particle being in addition added in formula makes Used time has color changeable effect, plays the role of concealing, repairs face discoloration;
2. using technical solution of the present invention, oil content with higher, but the surfactant contained is few, performance temperature It is sliding with skin sense silk.
Specific embodiment
Above scheme is described further below in conjunction with specific embodiment.It should be understood that these embodiments are for illustrating The present invention and be not limited to limit the scope of the invention.Implementation condition used in the examples can be done according to the condition of specific producer Further adjustment, the implementation condition being not specified is usually the condition in routine experiment.
Embodiment 1
BB frost is mixed by A phase, B phase, C phase and D and is prepared in the present embodiment,
A phase is oily phase, includes following components according to weight seniority in the family ratio:
Cyclic silicone oils: 13.5%,
Dimethicone/Vinyl Dimethicone cross-linked polymer: 0.75%,
Hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers: 0.75%;
B phase is water phase, includes following components according to weight percent:
Purified water: 45.05%,
Propylene glycol: 25.00%,
1,3-PD: 5.00%,
Ammonium acryloyl taurate/VP copolymer: 1.00%;
C phase, includes following components according to weight percent:
Essence: 0.10%,
PE9010 (Phenoxyethanol+Sensiva SC50): 0.80%,
Algae extract: 5.00%,
Glycine betaine: 2.00%,
Sodium Hyaluronate: 0.05%;
D phase:
Change colour BB frost particle, and 1.00%, discoloration BB frost particle is by CI 77492, CI 77491, CI 77499, CI 77891 and coating composition.
In the present embodiment BB frost the preparation method comprises the following steps:
(1) it is added after mixing A phase each component according to dosage part in oily phase pot, is stirred with the revolving speed of 10~50rpm/min 10~60min is to stirring evenly;
(2) by B phase each component purified water, propylene glycol, 1,3-PD, ammonium acryloyl taurate/VP copolymer It is sequentially added in vacuum emulsification pot according to dosage part, 10~60min is stirred with the revolving speed of 30~35rpm/min, keeps vacuum, then With homogeneous 10~60min of speed homogeneous of 2600~3100rpm/min to be uniformly mixed;
(3) raw material of oily phase pot is pumped into vacuum emulsification pot by strainer valve, is stirred with the revolving speed of 25~35rpm/min 10~30min forms transparent and homogeneous gel;
(4) C phase each component essence, PE9010, algae extract, glycine betaine are sequentially added into vacuum emulsification pot according to dosage part In, 10~60min is stirred with the revolving speed of 10~50rpm/min, is discharged after mixing evenly;
(5) mixture made from step (4) is placed in wide-mouth storage tank, is stirred in the revolving speed of 100~150rpm/min Under the conditions of, D phase is added and changes colour BB particle, inspection after mixing evenly;
(6) it is filling after detection is qualified.
The every Testing index of BB frost obtained in this example are as follows:
Lotion appearance: the clear gel with electrochromic particles;
Smell: consistent with essence smell;
Stability: heat-resisting 50 DEG C, 1 month stable testing;It is -15 DEG C to -5 DEG C cold-resistant, 4 freeze thawing, a month low-temperature stabilization;
Use feeling: when smearing on the skin, skin sense silk is sliding, moistens moisturizing, has color changeable effect at once, corrects the colour of skin, Nature dressing is presented.
Embodiment 2
BB frost is mixed by A phase, B phase, C phase and D and is prepared in the present embodiment,
A phase is oily phase, includes following components according to weight seniority in the family ratio:
Low viscous dimethicone: 27%,
Dimethicone/Vinyl Dimethicone cross-linked polymer: 1.5%,
Hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers: 1.5%;
B phase is water phase, includes following components according to weight percent:
Purified water: 23.20%,
Propylene glycol: 30.00%,
1,3-PD: 10.00%,
Ammonium acryloyl taurate/VP copolymer: 0.10%;
C phase, includes following components according to weight percent:
Essence: 0.08%,
PE9010:0.60%,
Algae extract: 2.00%,
Glycine betaine: 1.00%,
Sodium Hyaluronate: 0.02%;
D phase:
Change colour BB frost particle, and 3.00%, discoloration BB frost particle is by CI 77492, CI 77491, CI 77499, CI 77891 and coating composition.
The preparation method of BB frost in the present embodiment is same as Example 1.
Every Testing index of BB frost obtained in this example are as follows:
Lotion appearance: the clear gel with electrochromic particles;
Smell: consistent with essence smell;
Stability: heat-resisting 50 DEG C, 1 month stable testing;It is -15 DEG C to -5 DEG C cold-resistant, 4 freeze thawing, a month low-temperature stabilization;
Use feeling: when smearing on the skin, moistening moisturizing, and skin sense silk is sliding, has color changeable effect at once, corrects the colour of skin, Nature dressing is presented.
The foregoing examples are merely illustrative of the technical concept and features of the invention, its object is to allow the person skilled in the art to be It cans understand the content of the present invention and implement it accordingly, it is not intended to limit the scope of the present invention.It is all smart according to the present invention The equivalent transformation or modification that refreshing essence is done, should be covered by the protection scope of the present invention.

Claims (3)

1. a kind of clear aqueous discoloration BB frost of oil-containing, it is characterised in that: it is mixed and is prepared by A phase, B phase, C phase and D,
Wherein, A phase is oily phase, by weight percentage includes following components:
Silicone oil: 9.00%~30.00%,
Dimethicone/Vinyl Dimethicone cross-linked polymer: 0.50%~2.00%,
Hydroxy-ethyl acrylate/sodium acryloyldimethyl taurate copolymers: 0.50~2.00%;
Wherein, B phase is water phase, by weight percentage includes following components:
Purified water: 15.00%~76.00%,
Propylene glycol: 20.00%~50.00%,
1,3-PD: 1.00%~10.00%,
Ammonium acryloyl taurate/VP copolymer: 0.10%~2.00%;
Wherein, C phase includes following components according to weight percent:
Essence: 0.03%~0.5%,
PE9010: 0.50%~1.00%,
Algae extract: 0.50%~5.00%,
Glycine betaine: 0.50%~2.00%,
Sodium Hyaluronate: 0.001%~0.05%;
Wherein, D phase is discoloration BB frost particle: 1.00%~10.00%;
The sum of above each raw material weight percentage is 100%;
The silicone oil is cyclic silicone oils or low viscous dimethicone.
2. oil-containing according to claim 1 clear aqueous discoloration BB frost, it is characterised in that: the discoloration BB frost particle by CI 77492, CI 77491, CI 77499, CI 77891 and coating composition.
3. a kind of preparation method of the clear aqueous discoloration BB frost of oil-containing, it is characterised in that the following steps are included:
(1) be added after mixing A phase each component according to dosage part in oily phase pot, with the revolving speed stirring 10 of 10~50rpm/min~ 60min is to stirring evenly;
(2) by B phase each component purified water, propylene glycol, 1,3-PD, ammonium acryloyl taurate/VP copolymer according to Dosage part sequentially adds in vacuum emulsification pot, stirs 10~60min with the revolving speed of 30~35rpm/min, keeps vacuum, then with Homogeneous 10~60min of speed homogeneous of 2600~3100rpm/min to be uniformly mixed;
(3) raw material of oily phase pot is pumped into vacuum emulsification pot by strainer valve, with the revolving speed of 25~35rpm/min stirring 10~ 30min forms transparent and homogeneous gel;
(4) C phase each component essence, PE9010, algae extract, glycine betaine are sequentially added in vacuum emulsification pot according to dosage part, 10~60min is stirred with the revolving speed of 10~50rpm/min, is discharged after mixing evenly;
(5) mixture made from step (4) is placed in open storage tank, in the revolving speed stirring condition of 100~150rpm/min Under, D phase is added and changes colour BB particle, inspection after mixing evenly;
(6) it is filling after detection is qualified.
CN201510981376.XA 2015-12-24 2015-12-24 A kind of clear aqueous discoloration BB frost and preparation method of oil-containing Active CN105496812B (en)

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Application Number Priority Date Filing Date Title
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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103857412A (en) * 2011-10-11 2014-06-11 詹尼克公司 Emulsified hydrogel composition and a production method therefor
CN104434719A (en) * 2014-11-04 2015-03-25 广州卡迪莲化妆品有限公司 Application of snail secretion filtrate in improving skin pasting performance of make-up products
FR3021533A1 (en) * 2014-05-28 2015-12-04 Oreal COSMETIC COMPOSITION OF GEL TYPE

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10344660A1 (en) * 2003-09-25 2005-04-28 Merck Patent Gmbh Encapsulated pigments

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103857412A (en) * 2011-10-11 2014-06-11 詹尼克公司 Emulsified hydrogel composition and a production method therefor
FR3021533A1 (en) * 2014-05-28 2015-12-04 Oreal COSMETIC COMPOSITION OF GEL TYPE
CN104434719A (en) * 2014-11-04 2015-03-25 广州卡迪莲化妆品有限公司 Application of snail secretion filtrate in improving skin pasting performance of make-up products

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
Aristoflex AVC;独霸松松;《百度百科(http://baike.baidu.com/history/aristoflex%20AVC/96132710)》;20151204;1-2
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