CN1052239A - Sanitary insect pest applicating agent for killing pest and control the worm method - Google Patents
Sanitary insect pest applicating agent for killing pest and control the worm method Download PDFInfo
- Publication number
- CN1052239A CN1052239A CN 89108906 CN89108906A CN1052239A CN 1052239 A CN1052239 A CN 1052239A CN 89108906 CN89108906 CN 89108906 CN 89108906 A CN89108906 A CN 89108906A CN 1052239 A CN1052239 A CN 1052239A
- Authority
- CN
- China
- Prior art keywords
- pest
- agent
- applicating
- sanitary insect
- insect pest
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 241000607479 Yersinia pestis Species 0.000 title claims abstract description 51
- 241000238631 Hexapoda Species 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 21
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 24
- 239000004094 surface-active agent Substances 0.000 claims abstract description 10
- 239000002917 insecticide Substances 0.000 claims abstract description 8
- 239000000853 adhesive Substances 0.000 claims abstract description 7
- 230000001070 adhesive effect Effects 0.000 claims abstract description 7
- 210000002784 stomach Anatomy 0.000 claims abstract description 4
- 231100000419 toxicity Toxicity 0.000 claims abstract description 4
- 230000001988 toxicity Effects 0.000 claims abstract description 4
- 239000002131 composite material Substances 0.000 claims abstract description 3
- 238000007598 dipping method Methods 0.000 claims abstract description 3
- 239000002728 pyrethroid Substances 0.000 claims description 7
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 5
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 5
- 230000009545 invasion Effects 0.000 claims description 4
- 239000005946 Cypermethrin Substances 0.000 claims description 3
- -1 EXTHIN Chemical compound 0.000 claims description 3
- KAATUXNTWXVJKI-UHFFFAOYSA-N cypermethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OC(C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-UHFFFAOYSA-N 0.000 claims description 3
- 229960005424 cypermethrin Drugs 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 3
- RLLPVAHGXHCWKJ-IEBWSBKVSA-N (3-phenoxyphenyl)methyl (1s,3s)-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(Cl)Cl)[C@@H]1C(=O)OCC1=CC=CC(OC=2C=CC=CC=2)=C1 RLLPVAHGXHCWKJ-IEBWSBKVSA-N 0.000 claims description 2
- 108010010803 Gelatin Proteins 0.000 claims description 2
- OWZREIFADZCYQD-NSHGMRRFSA-N deltamethrin Chemical compound CC1(C)[C@@H](C=C(Br)Br)[C@H]1C(=O)O[C@H](C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 OWZREIFADZCYQD-NSHGMRRFSA-N 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- 239000003292 glue Substances 0.000 claims description 2
- 241001465754 Metazoa Species 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- 231100000957 no side effect Toxicity 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 14
- 241000255925 Diptera Species 0.000 description 5
- 241000257159 Musca domestica Species 0.000 description 5
- 239000003814 drug Substances 0.000 description 5
- 239000011521 glass Substances 0.000 description 5
- 241001674044 Blattodea Species 0.000 description 4
- 241000256113 Culicidae Species 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 231100000225 lethality Toxicity 0.000 description 4
- 238000010998 test method Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000000443 aerosol Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 241000144210 Culex pipiens pallens Species 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000012467 final product Substances 0.000 description 2
- 239000000077 insect repellent Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 231100000820 toxicity test Toxicity 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 241000283973 Oryctolagus cuniculus Species 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000001739 density measurement Methods 0.000 description 1
- 238000000151 deposition Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000000749 insecticidal effect Effects 0.000 description 1
- 229940040145 liniment Drugs 0.000 description 1
- 239000000865 liniment Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000002504 physiological saline solution Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 238000009602 toxicology test Methods 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
According to the life habit of sanitary insect pest, use the slowly-releasing control technology, with pyrethoid insecticides and surfactant, the composite a kind of aqua type sanitary insect pest applicating agent for killing pest that forms of adhesive.Have nontoxic to people and animals, have no side effect, efficient, quick-acting, long-acting, safety, health, economy, characteristics easy to use.Applicating agent for killing pest with the method for smearing (or dipping), is executed being distributed on the sanitary insect pest roost body surface, reach tag, stomach toxicity, the purpose of refusing to keep away sanitary insect pest.
Description
A kind ofly be used to kill sanitary insect pest applicating agent for killing pest such as mosquitos and flies, cockroach and control the worm method.
In technique known, pyrethroid insecticides become the control sanitary insect pest main medicine, its superiority is proved, and is promoted the use of in practice.Generally be to kill sanitary insect pests such as mosquitos and flies, cockroach with the method for mosquito-repellent incense, spray or aerosol jar.Mosquito-repellent incense is that insecticidal materials is admixed in the combustible, by burning, generate smog, distribute medicine, prevent and treat the invasion and attack of sanitary insect pest with the means of refusing to keep away, therefore need often light, and little the environment Use Limitation fruit that air flows, its toxic smoke also has bad reaction to people and animals, and spray or aerosol jar are to spray on the sanitary insect pest body insecticide or its zone of action with sprayer or aerosol jar, mainly to tag, the means of refusing to keep away reach the purpose of control sanitary insect pest.But its duration of efficacy is shorter, generally also needs with killing with spraying medicament, and is particularly more inconvenient to the control of sanitary insect pest with noctural habit, need dispose sprayer or gas tank in addition, so cost is higher.
The objective of the invention is to:
Life habit characteristics according to sanitary insect pests such as mosquitos and flies, cockroaches, use the slowly-releasing control technology, can be to seek insecticide securely attached on the various objects, long period discharges drug effect, reach efficient, quick-acting, long-acting, safety, economy, control sanitary insect pest easy to use, invented this applicating agent for killing pest and controlled the worm method.
Content of the present invention is: applicating agent for killing pest is by one or more pyrethroid insecticideses and a kind of adhesive, surfactant and anhydrous industrial alcohol, the composite aqua type liquid that forms of water.
The composition scope of this applicating agent for killing pest is:
Pyrethroid insecticides (one or more) is not less than 0.12%(weight)
Surfactant: be not less than 3.5%(weight)
Adhesive: 0.1%-0.5%(weight)
Anhydrous industrial alcohol: 15%-20%(weight)
Water
The each component summation is a 100%(weight)
Composition selection preferably is:
1., pyrethroid insecticides: cypermethrin, decis, EXTHIN, Permanone.
2., adhere to Ji: gelatin, 107 glue, polyvinyl alcohol, the polyvinyl alcohol semialdehyde that contracts.
3., surfactant: nonionic surface active agent.
The manufacture method of this applicating agent for killing pest is:
Take by weighing by the valid density measurement criteria and to be not less than 0.12% pyrethroid insecticides (one or more) and to add and be not less than 3.5% surfactant and the anhydrous industrial alcohol of 15%-20%, the adhesive that adds 0.1%-0.5% while stirring, after putting 15-20 minute, thin up is 100% and gets final product.(above all be weight percentage)
The worm method of controlling of this applicating agent for killing pest is: according to the life habit of sanitary insect pest, dip in this applicating agent for killing pest with small brushes or other adsorbable thing, be applied on the body surface that maybe need prevent the sanitary insect pest invasion and attack on the body surface of roost of sanitary insect pest or around the zone.Locate as indoor corner, wall, screen window, screen door, kitchen cabinet, wardrobe, door glass etc., can tag, stomach toxicity, the invasion and attack of refusing to keep away sanitary insect pest.Also the method for available dipping attached on some body surface, is suspended on the movable place of sanitary insect pest possibility, to trap and kill it with this applicating agent for killing pest.As mosquito net, door curtain, lamp cord etc.
The advantage and the good effect of this applicating agent for killing pest are described below in conjunction with embodiment:
Non-limiting examples of the present invention:
1, the preparation of this applicating agent for killing pest:
1., take by weighing 0.1 kilogram cypermethrin, 0.02 kilogram EXTHIN, 3.5 kilograms TX-10 surfactant, 15 kilograms anhydrous industrial alcohol, mixing stirring.
2., when stirring said mixture, add 0.1 kilogram polyvinyl alcohol, place 20 minutes then, standby.
Adding the dilution of 81.28 kg of water when 3., using gets final product.
2, toxicology test:
1., anxious toxicity test: adopt the Hols method, choose 40 of the heavy healthy Kunming of 18-22g kind small white mouses, male and female half and half.With equilibrium at random three-step approach be divided into 4 groups.Every group 10, male and female half and half.Dosage is designed to: 2.15g/kg, 4.64g/kg, 10g/kg, 21.5g/kg per os are once irritated stomach, the death condition after two weeks of observation.
As follows:
| Dosage | Number of animals | Death toll | |
| (g/kg) | (only) | Female | Male |
| 2.15 | 10 | 0/5 | 0/5 |
| 4.64 | 10 | 0/5 | 0/5 |
| 10.00 | 10 | 0/5 | 0/5 |
| 21.50 | 10 | 5/5 | 5/5 |
Table look-up: LD50 and 95% credible being limited to:
Male: LD50=11.00g/kg(6.61-18.3g/kg)
Female: LD50=14.70g/kg(12.30-23.3g/kg)
According to toxicity grading: the invention belongs to the non-toxic type material.
2., skin irritation test:
Choose three of 2-3Kg health large ear rabbits, in its unhairing baring skin 4 districts, backbone both sides, back, every district area is 6cm * 4cm, observes 24 hours intact persons of skin and tests.Get this applicating agent for killing pest of 0.5ml, be applied to intersection two districts, all the other two districts are coated with physiological saline, topped subsequently smear zone.With warm water being coated with thing is cleaned after 6 hours, observed 72 hours, each distinguishes skin not show spot or bubble formation, and willful murder worm liniment is non-stimulated to skin, and use is safe and reliable.
3, speed is killed test: carry out in 26 ± 2 ℃ thermostatic chamber, mosquitos and flies speed is killed test adopt the unified method of testing in the whole nation.(40 * 25 * 20cm) carry out cockroach in special glass chamber.Its result is as follows:
| The test insect | Quantity (only) | KT50 | 24 hours lethality | Test method |
| Culex pipiens pallens | 30 | 5′18″ | 100 | Bell jar process |
| Housefly | 30 | 2′05″ | 100 | Bell jar process |
| Groton bug | 20 | 7′46″ | 100 | The glass box method |
Show through biological test: the test insect was all killed no anabiosis in 24 hours.So this applicating agent for killing pest has quick-acting effects.
4, hold and imitate test: with the applicating agent for killing pest of depositing 12 months under the normal temperature, by the dose of 30ml/m be applied on the plastic window sarong respectively and glass box in, place at normal temperatures, the routine observation result is as follows:
| The test insect | Apart from the processing time | KT50 | Lethality 100% in 24 hours | Test method |
| Culex pipiens pallens | 1 6 12 | 5′25″ 11′13″ 21′07″ | 100 100 100 | Bell jar process |
| Housefly | 1 6 12 | 3′42″ 5′27″ 8′48″ | 100 100 100 | Bell jar process |
| Groton bug | 1 6 12 | 8′24″ 12′26″ 24′19″ | 100 100 100 | The glass box method |
The result shows: the time of handling along with medication increases, and it is gradually slow that it knocks down speed, lasts 12 months and still has the power of killing, and visible applicating agent for killing pest of the present invention has control slow release method characteristic, is long-acting, and dispensers in three months of its use are once for well.
5, adhesion test: will test cage and be placed on the rain place 20 minutes, rainfall is 30 millimeters, fetches in the laboratory that to compare the result as follows with the contrast cage:
| The medication fate | The rain time (minute) | Rainwater PH | The test worm | Quantity (only) | KT20 | 24 hours lethality (%) | |
| The test cage | 4 | 20 | 7.5 | Housefly | 20 | 5′24″ | 100 |
| The contrast cage | 4 | － | ” | 20 | 3′25″ | 100 |
Illustrate: have very strong adhesive force, but firm attachment is at body surface.
6, stability experiment: place the insulating box of 35 ℃ and 50 ℃ to store respectively 225 days this applicating agent for killing pest, undertaken by the biological efficacy test method, the result is as follows:
| The test worm | Storage temperature | Deposit fate | KT50 | 24 hours lethality |
| Housefly | 35℃ | 15 75 150 225 | 3′33″ 4′14″ 6′14″ 7′34″ | 100 100 100 100 |
| Housefly | 50℃ | 1 5 9 14 | 4′42″ 6′04″ 6′43″ 8′52″ | 100 100 100 100 |
This shows that the present invention can once prepare, the long-term use, generally with a term for well.
In addition, this applicating agent for killing pest is aqua type liquid, thus do not fire, not quick-fried, tasteless, do not pollute operating environment, cost low, control the easy advantage of worm method.
Claims (3)
1, a kind of applicating agent for killing pest that is used for sanitary insect pest is characterized in that described applicating agent for killing pest is by one or more pyrethroid insecticideses and a kind of surfactant, the aqua type liquid that adhesive is mutually composite.
2, applicating agent for killing pest according to claim 1 is characterized in that:
1., pyrethroid insecticides is: cypermethrin, decis, EXTHIN, Permanone.
2., adhesive is: gelatin, 107 glue, polyvinyl alcohol, the polyvinyl alcohol semialdehyde that contracts.
3., surfactant is: nonionic surface active agent.
3, a kind of worm method of controlling that is used for the applicating agent for killing pest of sanitary insect pest, it is characterized in that life habit according to sanitary insect pest, with applicating agent for killing pest with the method for smearing (or dipping) execute be distributed on the sanitary insect pest roost body surface or execute be distributed on the body surface that need prevent the sanitary insect pest invasion and attack and around the zone, tag to reach, stomach toxicity, the purpose of refusing to keep away sanitary insect pest.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 89108906 CN1027031C (en) | 1989-11-29 | 1989-11-29 | Sanitary pest-killing smearing agent and pest-controlling method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 89108906 CN1027031C (en) | 1989-11-29 | 1989-11-29 | Sanitary pest-killing smearing agent and pest-controlling method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1052239A true CN1052239A (en) | 1991-06-19 |
| CN1027031C CN1027031C (en) | 1994-12-21 |
Family
ID=4857791
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 89108906 Expired - Fee Related CN1027031C (en) | 1989-11-29 | 1989-11-29 | Sanitary pest-killing smearing agent and pest-controlling method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1027031C (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1037657C (en) * | 1993-01-09 | 1998-03-11 | 周承显 | Long effect domestic hygiene and injurious insect pesticide and preparing process thereof |
| CN1070026C (en) * | 1998-04-27 | 2001-08-29 | 蔡荣昌 | Hygienic biocide composition |
| CN102232379A (en) * | 2010-05-06 | 2011-11-09 | 福建省金鹿日化股份有限公司 | Water-based electrothermal liquid mosquito-repellent incense and preparation method thereof |
| CN102475090A (en) * | 2010-11-30 | 2012-05-30 | 住友化学株式会社 | Pesticidal composition and method of controlling pests |
| CN103444787A (en) * | 2013-08-23 | 2013-12-18 | 湖南亨通生物技术有限公司 | Extraction method of cedar oil and cedar oil anophelifuge prepared from cedar oil |
-
1989
- 1989-11-29 CN CN 89108906 patent/CN1027031C/en not_active Expired - Fee Related
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1037657C (en) * | 1993-01-09 | 1998-03-11 | 周承显 | Long effect domestic hygiene and injurious insect pesticide and preparing process thereof |
| CN1070026C (en) * | 1998-04-27 | 2001-08-29 | 蔡荣昌 | Hygienic biocide composition |
| CN102232379A (en) * | 2010-05-06 | 2011-11-09 | 福建省金鹿日化股份有限公司 | Water-based electrothermal liquid mosquito-repellent incense and preparation method thereof |
| CN102232379B (en) * | 2010-05-06 | 2014-03-26 | 福建省金鹿日化股份有限公司 | Water-based electrothermal liquid mosquito-repellent incense and preparation method thereof |
| CN102475090A (en) * | 2010-11-30 | 2012-05-30 | 住友化学株式会社 | Pesticidal composition and method of controlling pests |
| CN103444787A (en) * | 2013-08-23 | 2013-12-18 | 湖南亨通生物技术有限公司 | Extraction method of cedar oil and cedar oil anophelifuge prepared from cedar oil |
| CN103444787B (en) * | 2013-08-23 | 2016-03-30 | 湖南亨通生物技术有限公司 | A kind of cedar oil extracting method and cedar oil culicifuge thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1027031C (en) | 1994-12-21 |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |