CN105106834A - Huoluo oil and preparation method thereof - Google Patents

Abstract

The invention relates to an active collateral oil and a preparation method thereof, and belongs to the technical field of medicinal oil preparation; the active collateral oil is prepared from the following components in parts by weight: 25-30 parts of rice fermentation product filtrate, 10-16 parts of mugwort leaf extract, red 5-14 parts of flower extract, 12-13 parts of Panax notoginseng root extract, 10-11 parts of Sperantoides extract, 8-9 parts of Ginkgo biloba extract, 6-7 parts of oat germ oil, 6 parts of Salvia root extract -7 parts, 5-6 parts of peppermint leaf oil, 4-5 parts of angelica root extract, 3-4 parts of turmeric root oil; the above components are crushed, soaked, and specially treated to make it; The oil has the functions of relaxing tendons and activating collaterals, dispelling wind and stasis, warming meridians and dispelling cold, expelling wind and dehumidification, promoting blood circulation and relieving pain. Moreover, the active oil is designed with a ball, which is easy to use and can be used by drivers.

Description

A kind of activating collateral oil and preparation method thereof

technical field

The invention relates to a activating collateral oil and a preparation method thereof, in particular to an activating collateral oil using pure natural plant components, which has low irritation and no toxic and side effects and a preparation method thereof, and belongs to the technical field of medicated oil production.

Background technique

Huoluo Oil is a product composed of a variety of essential oils and menthol, which has the functions of relaxing tendons and activating collaterals, dispelling wind and blood stasis, warming meridians and dispelling cold, expelling wind and dampness, promoting blood circulation and relieving pain. It can be used for muscle soreness, rheumatic bone pain, old and new sprains, arthritis pain, mosquito bites, sprains and swelling, swelling and pain in hands and feet, waist and hamstring pain, bone spurs, sciatica, muscle and bone pain, lumbar tingling, old bruises, Small sores, swelling and pain, itchy skin, mosquito bites, boat and car motion sickness, dizziness and abdominal pain, with a wide range of effects.

There are a variety of activating effects on the market, their functions are uneven, there are many effects, and they can be used in a wide range of places. The site of use is wide, and the pertinence is not strong enough, resulting in differences in the effect of the product during use, and in more serious cases, it may not play the role mentioned by the product. Moreover, the existing products are highly irritating, and are accompanied by a burning sensation when used. In severe cases, the skin will be burned; the smell is pungent, the smell of medicine is strong, and the packaging is simple, so it is not suitable for use in public places. Therefore, it is of great significance to develop a kind of activating oil that has no irritating smell, has the most effective treatment to specific parts, and avoids the difference in efficacy when different parts are used.

Chinese patent, patent number: 200710090374.7; a medicinal composition of activating collateral oil, which is developed by crushing and heating 21 kinds of Chinese herbal medicines such as borneol, menthol, Liao Diaozhu, jingucao, zedoary, false lychee, and Caulis Spatholobus into. Although it has the effects of anti-inflammation and swelling, strengthening tendons and collaterals, promoting blood circulation and removing blood stasis, reducing swelling and relieving pain, there may be differences in the effect of the product during use. Therefore, it is necessary to develop a kind of active oil that can effectively treat specific parts very important.

The invention adopts pure natural plant ingredients, has low irritation, and has no toxic and side effects; it can not only effectively improve the problems of cervical muscle tension and cervical stiffness, but also promote local blood flow, supplement brain oxygen, and have the effect of refreshing and warming the brain. Cotton is soft, gradually penetrates, improves comfort, activates oxygen and refreshes the brain, and brings people a new feeling; this product adopts a ball-shaped design, with a small and exquisite appearance, easy to use, and easy to carry.

Contents of the invention

The purpose of the present invention is to use the unique Chinese medicine extraction process to effectively retain the drug ingredients, novel formula concept and exquisite outer packaging, so as to achieve special treatment and the most effective treatment of specific parts, avoiding the existence of different parts when used. The difference in efficacy, low irritation and better protection of the skin. The appearance is small and exquisite, the smell is fragrant and charming, and it is easy to carry and use.

In order to solve the problems of traditional Huoluo oil with strong irritation, poor appearance and packaging materials, inconvenient to carry and use, and pungent smell, the present invention develops an innovative Huoluo oil preparation process through process innovation. The adopted technical scheme is:

An innovative active oil, which consists of the following components in parts by weight: 25-30 parts of rice fermentation product filtrate, 10-16 parts of mugwort leaf extract, 5-14 parts of safflower extract, and 12-13 parts of Panax notoginseng root extract , 10-11 parts of bone grass extract, 8-9 parts of ginkgo biloba extract, 6-7 parts of oat germ oil, 6-7 parts of salvia root extract, 5-6 parts of peppermint leaf oil, 4 parts of angelica root extract -5 parts, turmeric root oil 3-4 parts.

A preparation method of innovative active oil, comprising the steps of:

(1) Preparation of the extract: clean the raw materials of mugwort leaf, safflower, Panax notoginseng, Speranium, Ginkgo biloba, Salvia miltiorrhiza, and Angelica root, dry and dehydrate at 50-60°C, crush them with liquid nitrogen at low temperature, and then use 45- 55-degree sorghum wine is soaked in a low-temperature sealed pot for 10-20 days, and the leachate is extracted, filtered, and concentrated using traditional reflux extraction technology. After the appearance and microorganisms are qualified, it is sealed and stored at low temperature until use;

(2) Preparation of the rice fermentation product filtrate: ferment the rice with Acetobacter and Lactobacillus plantarum, and filter the fermentation liquid to obtain the rice fermentation product filtrate;

(3) Use sterilized water at 80-100°C to clean the cylinders, containers, and valve-related utensils used in production, and then disinfect them with 75% alcohol for later use;

(4) Weigh 25-30 parts of rice fermentation product filtrate, 10-16 parts of mugwort leaf extract, 5-14 parts of safflower extract, 12-13 parts of Panax notoginseng root extract, and 10-11 parts of Sperantosporum extract , 8-9 parts of Ginkgo biloba extract, 6-7 parts of Danshen root extract, 4-5 parts of Angelica root extract, add to the production container, stir evenly to obtain group A materials; weigh 6-7 parts of oat germ oil, Add 5-6 parts of mint leaf oil and 3-4 parts of turmeric root oil to the materials of group A, stir evenly, check the appearance and microorganisms, and then pack.

The traditional reflux extraction conditions described in step (1) are: temperature 50-60°C, solid-liquid ratio 1:10-1:50g/ml.

The medium and low temperature of the low-temperature sealing immersion described in step (1) is 3°C-8°C.

The compounding ratio of Acetobacterium and Lactobacillus plantarum described in step (2) is 1:2, and the addition amount is 3-5%; the fermentation conditions are fermentation temperature 25-35°C, pH 5.5-6.5, fermentation time 24- 36h.

The beneficial effect of the present invention relative to prior art is:

The invention uses pure natural plant ingredients, low irritation, no toxic and side effects, and is based on the principle of staying away from danger and being safe and unique. A conscientious work for patients, business trips, tourists, inspectors, etc.; it can not only effectively improve cervical muscle tension, cervical stiffness and other problems, but also promote local blood flow, supplement brain oxygen, and have a refreshing effect Efficacy, warm and soft, gradually penetrates, enhances comfort, activates oxygen and refreshes the brain, and brings people a new feeling; this product adopts a ball-shaped design, with a small and exquisite appearance, easy to use, and easy to carry.

The experimental results of this product are as follows:

According to the latest data from Sakura Nair, 50%-60% of users will have bright eyes and concentrated attention after applying it for 3-10 minutes; while natural plants endow the energy liquid with a refreshing, non-greasy, and aromatic smell Charming (there are a variety of natural plant fragrances to choose from); it can be applied emphatically on the upper and lower sides of the cervical spine at 5-8 cm above and below, on the left and right temples in circles, between the upper lip and the lower nose, and the effect is most obvious. Conscience Quality, the effect of the medicine can last for 1-2 hours (depending on the individual's physique and the amount of application), and after three days of use, it has a unique effect on improving symptoms.

The present invention is compared with domestic multiple similar well-known products in experiments. The experimental data is the average data of the clinical trial data of the number of people tested. The statistical data are as follows:

Detailed ways

The present invention will be described in further detail below through examples, these examples are only used to illustrate the present invention, do not limit the scope of the present invention, and the specific embodiment of the present invention is carried out through two aspects of preparation and application.

Example 1

An innovative active oil, which consists of the following components in parts by weight: 25 parts of rice fermentation product filtrate, 10 parts of mugwort leaf extract, 5 parts of safflower extract, 10 parts of Panax notoginseng root extract, and 10 parts of Sperantosporum extract , Ginkgo biloba extract 8 parts, Oat germ oil 6 parts, Salvia root extract 6 parts, Peppermint leaf oil 5 parts, Angelica root extract 4 parts, Turmeric root oil 3 parts.

A preparation method of innovative active oil, comprising the steps of:

(1) Preparation of the extract: clean the raw materials of mugwort leaf, safflower, Panax notoginseng, Speranium, Ginkgo, Salvia miltiorrhiza, and angelica root, dry and dehydrate at 50°C, and then pulverize with liquid nitrogen at low temperature, and then use 45% sorghum wine Soak in a low-temperature pottery pot at 3°C for 20 days, and use traditional reflux extraction technology to extract, filter, and concentrate the leachate at a temperature of 60°C and a ratio of solid to liquid of 1:50g/ml. , sealed and stored at low temperature, ready for use;

(2) Preparation of rice fermentation product filtrate: ferment rice with Acetobacter and plantaractobacillus (combination ratio: 1:2), the addition amount is 3%, the fermentation conditions are fermentation temperature 35°C, pH 6.5, fermentation time 36h; fermented liquid was filtered to obtain rice fermentation product filtrate;

(3) Use sterilized water at 80°C to clean the cylinders, containers, and valve-related utensils used in production, and then disinfect them with 75% alcohol for later use;

(4) Weigh 25 parts of rice fermentation product filtrate, 10 parts of mugwort leaf extract, 5 parts of safflower extract, 10 parts of Panax notoginseng root extract, 10 parts of Speranthema extract, 8 parts of Ginkgo biloba extract, Salvia root Add 6 parts of extract and 4 parts of angelica root extract into the production container, and stir evenly to obtain the materials of group A; weigh 6 parts of oat germ oil, 5 parts of mint leaf oil, and 3 parts of turmeric root oil, and add them to the materials of group A. Stir evenly, check the appearance and microorganisms, and then pack.

Example 2

An innovative active oil, consisting of the following components in parts by weight: 30 parts of rice fermented product filtrate, 16 parts of mugwort leaf extract, 14 parts of safflower extract, 13 parts of Panax notoginseng root extract, 11 parts of Sperantosporum extract , Ginkgo Biloba Leaf Extract 9 parts, Oat Germ Oil 7 parts, Salvia Root Extract 7 parts, Peppermint Leaf Oil 6 parts, Angelica Root Extract 5 parts, Turmeric Root Oil 4 parts.

A preparation method of innovative active oil, comprising the steps of:

(1) Preparation of the extract: clean the raw materials of mugwort leaf, safflower, Panax notoginseng, Speranthum, Ginkgo, Salvia miltiorrhiza, and angelica root, dry and dehydrate at 60°C, and then pulverize with liquid nitrogen at low temperature, and then use 55% sorghum wine Soak in a low-temperature pottery pot at 8°C for 10 days, and use traditional reflux extraction technology to extract, filter, and concentrate the leachate at a temperature of 50°C and a ratio of material to liquid of 1:10g/ml, and then check the appearance and microorganisms. , sealed and stored at low temperature, ready for use;

(2) Preparation of rice fermentation product filtrate: ferment rice with Acetobacter and plantarum (combination ratio: 1:2), the addition amount is 5%, the fermentation conditions are fermentation temperature 25°C, pH 5.5, fermentation time 24h; fermented liquid was filtered to obtain rice fermentation product filtrate;

(3) Use 100°C sterilized water to clean the cylinders, containers, and valve-related utensils used in production, and then disinfect them with 75% alcohol for later use;

(4) Weigh 30 parts of rice fermentation product filtrate, 16 parts of mugwort leaf extract, 14 parts of safflower extract, 13 parts of Panax notoginseng root extract, 11 parts of Speranthema extract, 9 parts of Ginkgo biloba extract, Salvia root Add 7 parts of extract and 5 parts of angelica root extract into the production container, and stir evenly to obtain the materials of group A; weigh 7 parts of oat germ oil, 6 parts of peppermint leaf oil, and 4 parts of turmeric root oil, and add them to the materials of group A. Stir evenly, check the appearance and microorganisms, and then pack.

Example 3

An innovative active oil, which consists of the following components in parts by weight: 28 parts of rice fermentation product filtrate, 14 parts of mugwort leaf extract, 10 parts of safflower extract, 12.5 parts of Panax notoginseng root extract, and 10.5 parts of Speranca officinalis extract , 8.5 parts of ginkgo leaf extract, 6.5 parts of oat germ oil, 6.5 parts of salvia root extract, 5.5 parts of peppermint leaf oil, 4.5 parts of angelica root extract, 3.5 parts of turmeric root oil.

A preparation method of innovative active oil, comprising the steps of:

(1) Preparation of the extract: clean the raw materials of mugwort leaf, safflower, Panax notoginseng, Speranium, Ginkgo biloba, Salvia miltiorrhiza, and Angelica root, dry and dehydrate at 55°C, and then pulverize with liquid nitrogen at low temperature, and then use 50°C sorghum wine Soak for 15 days in a low-temperature pottery pot at 5°C, and use traditional reflux extraction technology to extract, filter, and concentrate the leachate at a temperature of 55°C and a material-to-liquid ratio of 1:25g/ml, and then inspect the appearance and microorganisms. , sealed and stored at low temperature, ready for use;

(2) Preparation of rice fermentation product filtrate: ferment rice with Acetobacter and plantarum (combination ratio: 1:2), the addition amount is 4%, the fermentation conditions are fermentation temperature 30°C, pH 6.0, fermentation time 30h; fermented liquid was filtered to obtain rice fermentation product filtrate;

(3) Use sterilized water at 90°C to clean the cylinders, containers, and valve-related utensils used in production, and then disinfect them with 75% alcohol for later use;

(4) Weigh 28 parts of rice fermentation product filtrate, 14 parts of mugwort leaf extract, 10 parts of safflower extract, 12.5 parts of Panax notoginseng root extract, 10.5 parts of Speranza extract, 8.5 parts of Ginkgo biloba extract, angelica root Add 4.5 parts of the extract into the production container, stir evenly to obtain the materials of group A; weigh 6.5 parts of oat germ oil, 5.5 parts of mint leaf oil, and 3.5 parts of turmeric root oil, add them to the materials of group A, stir evenly, and detect the appearance and microorganisms After passing, pack.

Example 4

An innovative active oil, which consists of the following components in parts by weight: 27 parts of rice fermented product filtrate, 16 parts of Artemisia argyi leaf extract, 8 parts of safflower extract, 12 parts of Panax notoginseng root extract, and 10 parts of Sperantosporum extract , Ginkgo biloba extract 8 parts, Oat germ oil 6 parts, Salvia root extract 6 parts, Peppermint leaf oil 5 parts, Angelica root extract 4 parts, Turmeric root oil 3 parts.

A preparation method of innovative active oil, comprising the steps of:

(1) Preparation of the extract: clean the raw materials of mugwort leaf, safflower, Panax notoginseng, Speranium, Ginkgo biloba, Salvia miltiorrhiza, and angelica root, dry and dehydrate at 50°C, and then pulverize with liquid nitrogen at low temperature, and then use 50°C sorghum wine Soak in a low-temperature pottery pot at 5°C for 10 days, use traditional reflux extraction technology to extract, filter, and concentrate the leachate at a temperature of 55°C and a material-to-liquid ratio of 1:30g/ml, and then check the appearance and microorganisms to pass the test , sealed and stored at low temperature, ready for use;

(2) Preparation of rice fermentation product filtrate: ferment rice with Acetobacter and plantarum (combination ratio: 1:2), the addition amount is 5%, the fermentation conditions are fermentation temperature 30°C, pH 6.5, fermentation time 28h; the fermentation liquid was filtered to obtain the rice fermentation product filtrate;

(3) Use 100°C sterilized water to clean the cylinders, containers, and valve-related utensils used in production, and then disinfect them with 75% alcohol for later use;

(4) Weigh 27 parts of rice fermentation product filtrate, 16 parts of Artemisia argyi leaf extract, 8 parts of safflower extract, 12 parts of Panax notoginseng root extract, 10 parts of Speranthemus extract, 8 parts of Ginkgo biloba extract, Angelica root Add 4 parts of the extract into the production container, stir evenly to obtain the materials of group A; weigh 6 parts of oat germ oil, 5 parts of mint leaf oil, and 3 parts of turmeric root oil, add them to the materials of group A, stir evenly, and detect the appearance and microorganisms After passing, pack.

Example 5

An innovative active oil, consisting of the following components in parts by weight: 26 parts of rice fermented product filtrate, 12 parts of mugwort leaf extract, 5 parts of safflower extract, 13 parts of Panax notoginseng root extract, and 10 parts of Sperantosporum extract , Ginkgo biloba extract 8 parts, Oat germ oil 6 parts, Salvia root extract 6 parts, Peppermint leaf oil 5 parts, Angelica root extract 4 parts, Turmeric root oil 4 parts.

A preparation method of innovative active oil, comprising the steps of:

(1) Preparation of the extract: clean the raw materials of mugwort leaf, safflower, Panax notoginseng, Speranium, Ginkgo biloba, Salvia miltiorrhiza, and angelica root, dry and dehydrate at 50°C, and then pulverize with liquid nitrogen at low temperature, and then use 50°C sorghum wine Soak in a low-temperature clay pot at 8°C for 15 days, and use traditional reflux extraction technology to extract, filter, and concentrate the leachate at a temperature of 55°C and a material-to-liquid ratio of 1:20g/ml, and then inspect the appearance and microorganisms. , sealed and stored at low temperature, ready for use;

(2) Preparation of rice fermentation product filtrate: ferment rice with Acetobacter and plantarum (combination ratio: 1:2), the addition amount is 4%, the fermentation conditions are fermentation temperature 30°C, pH 6.0, fermentation time 30h; fermented liquid was filtered to obtain rice fermentation product filtrate;

(3) Use sterilized water at 85°C to clean the cylinders, containers, and valve-related utensils used in production, and then disinfect them with 75% alcohol for later use;

(4) Weigh 26 parts of rice fermentation product filtrate, 12 parts of mugwort leaf extract, 5 parts of safflower extract, 13 parts of Panax notoginseng root extract, 10 parts of Speranthemus extract, 8 parts of ginkgo leaf extract, angelica root Add 4 parts of the extract into the production container, stir evenly to obtain the materials of group A; weigh 6 parts of oat germ oil, 5 parts of mint leaf oil, and 4 parts of turmeric root oil, add them to the materials of group A, stir evenly, and detect the appearance and microorganisms After passing, pack.

Claims (5)

1. An active oil, characterized in that: it is made by the weight of the following components: 25-30 parts of rice fermentation product filtrate, 10-16 parts of Artemisia argyi leaf extract, 5-14 parts of safflower extract, Radix Notoginseng root 12-13 parts of extract, 10-11 parts of Speranza extract, 8-9 parts of Ginkgo biloba extract, 6-7 parts of oat germ oil, 6-7 parts of Danshen root extract, 5-6 parts of peppermint leaf oil , 4-5 parts of angelica root extract, 3-4 parts of turmeric root oil. 2. A method for preparing the active oil according to claim 1, characterized in that: comprising the steps of: (1) Preparation of the extract: clean the raw materials of mugwort leaf, safflower, Panax notoginseng, Sperantosporum, Ginkgo biloba, Salvia miltiorrhiza, and angelica root, dry and dehydrate at 50-60°C, and then pulverize with liquid nitrogen at low temperature, and then use 45- 55-degree sorghum wine is soaked in a low-temperature sealed pot for 10-20 days, and the leachate is extracted, filtered, and concentrated using traditional reflux extraction technology. After the appearance and microorganisms are qualified, it is sealed and stored at low temperature until use; (2) Preparation of the rice fermentation product filtrate: ferment the rice with Acetobacter and Lactobacillus plantarum, and filter the fermentation liquid to obtain the rice fermentation product filtrate; (3) Use sterilized water at 80-100°C to clean the cylinders, containers, and valve-related utensils used in production, and then disinfect them with 75% alcohol for later use; (4) Weigh 25-30 parts of rice fermentation product filtrate, 10-16 parts of mugwort leaf extract, 5-14 parts of safflower extract, 12-13 parts of Panax notoginseng root extract, and 10-11 parts of Sperantosporum extract , 8-9 parts of Ginkgo biloba extract, 6-7 parts of Danshen root extract, 4-5 parts of Angelica root extract, add to the production container, stir evenly to obtain group A materials; weigh 6-7 parts of oat germ oil, Add 5-6 parts of peppermint leaf oil and 3-4 parts of turmeric root oil to the materials of group A, stir evenly, check the appearance and microorganisms, and then pack. 3. The preparation method of Huoluo oil according to claim 2, characterized in that the traditional reflux extraction conditions in step (1) are: temperature 50-60°C, solid-liquid ratio 1:10-1:50g /ml. 4. The method for preparing activating oil according to claim 2, characterized in that the low temperature in the low-temperature sealing soaking in step (1) is 3°C-8°C. 5. The preparation method of a kind of activating oil according to claim 2, characterized in that: the compounding ratio of Acetobacter and plantarum in step (2) is 1:2, and the addition amount is 3-5% ; The fermentation conditions are a fermentation temperature of 25-35° C., a pH of 5.5-6.5, and a fermentation time of 24-36 hours.