CN104611007B - A kind of waste lubricating oil refines petrol and diesel oil device - Google Patents
A kind of waste lubricating oil refines petrol and diesel oil device Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G53/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more refining processes
- C10G53/02—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more refining processes plural serial stages only
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/10—Feedstock materials
- C10G2300/1037—Hydrocarbon fractions
- C10G2300/1062—Lubricating oils
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
- C10G2400/02—Gasoline
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
- C10G2400/04—Diesel oil
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- General Chemical & Material Sciences (AREA)
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- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
本发明涉及化工技术领域,尤其是一种废润滑油提炼汽柴油装置,包括沉降罐,高温油泵,闪蒸罐,气化釜,气化釜过滤塔,引风机,烟气净化装置,固定床催化塔,分馏塔,汽油用水冷却器,柴油用水冷却器,柴油中间罐,齿轮油泵,柴油贮罐,还包括真空泵组,油气分离罐,回流泵,汽油贮罐,干气缓冲罐,干气脱硫脱氯塔,干气柜,熔盐加热炉,熔盐泵,熔盐罐;所述的沉降罐,高温油泵,闪蒸罐,气化釜,气化釜过滤塔,固定床催化塔,分馏塔依次连接,分馏塔分别连接汽油提炼装置和柴油提炼装置,熔盐加热炉为整套装置提供热源。该装置全自动,无污染,零能耗,环保,低耗、易操作,对润滑油的处理能够实现完全无害化、无污染及最优资源化利用。
The invention relates to the technical field of chemical engineering, in particular to a device for refining gasoline and diesel oil from waste lubricating oil, including a settling tank, a high-temperature oil pump, a flash tank, a gasification kettle, a gasification kettle filter tower, an induced draft fan, a flue gas purification device, and a fixed bed Catalytic tower, fractionation tower, gasoline water cooler, diesel water cooler, diesel intermediate tank, gear oil pump, diesel storage tank, also includes vacuum pump group, oil and gas separation tank, reflux pump, gasoline storage tank, dry gas buffer tank, dry gas Desulfurization and dechlorination tower, dry gas cabinet, molten salt heating furnace, molten salt pump, molten salt tank; the settling tank, high temperature oil pump, flash tank, gasification kettle, gasification kettle filter tower, fixed bed catalytic tower, The fractionation towers are connected in sequence, and the fractionation towers are respectively connected to the gasoline refining unit and the diesel refining unit, and the molten salt heating furnace provides the heat source for the whole set of units. The device is fully automatic, pollution-free, zero energy consumption, environmental protection, low consumption, easy to operate, and the treatment of lubricating oil can be completely harmless, pollution-free and optimal resource utilization.
Description
技术领域 technical field
本发明涉及化工技术领域,尤其是一种废润滑油提炼汽柴油装置。 The invention relates to the technical field of chemical industry, in particular to a device for refining gasoline and diesel oil from waste lubricating oil.
背景技术 Background technique
随着石油工业突飞猛进的发展,以石油为原材料的润滑油产品在国民经济各个领域得到广泛的运用,润滑油制品在给人们的生活带来方便的同时,也产生了日益严重的污染,却很少有回收利用,换下的废润滑油绝大部分是就地倒掉或焚烧,既浪费了大量资源又造成了严重环境污染; With the rapid development of the petroleum industry, lubricating oil products using petroleum as raw materials have been widely used in various fields of the national economy. While lubricating oil products bring convenience to people's lives, they also produce increasingly serious pollution. There is little recycling, and most of the used lubricating oil that is replaced is dumped or incinerated on the spot, which not only wastes a lot of resources but also causes serious environmental pollution;
目前,国内许多废润滑油设备的炼油方法,不能连续生产,能耗高,安全性差,经常出现爆炸问题,并且未能解决处理中排放有毒废气,废水和废渣问题,从而产生二次污染。 At present, the oil refining methods of many waste lubricating oil equipment in China cannot be continuously produced, have high energy consumption, poor safety, frequent explosion problems, and fail to solve the problem of toxic waste gas, waste water and waste residue during treatment, resulting in secondary pollution.
发明内容 Contents of the invention
为了解决现有技术的不足,本发明提供了一种采用废润滑油提炼汽柴油装置,该装置环保无污染,减少了废气的排放,能连续生产,降低能耗,易操作。 In order to solve the deficiencies of the prior art, the present invention provides a device for refining gasoline and diesel using waste lubricating oil. The device is environmentally friendly and pollution-free, reduces waste gas emissions, can be continuously produced, reduces energy consumption, and is easy to operate.
本发明解决其技术问题所采用的技术方案是:一种采用废润滑油提炼汽柴油装置,包括沉降罐,高温油泵,闪蒸罐,汽化釜,汽化釜过滤塔,引风机,烟气净化装置,固定床催化塔,分馏塔,汽油用水冷却器,柴油用水冷却器,柴油中间罐,齿轮油泵,柴油贮罐,还包括真空泵组,油气分离罐,回流泵,汽油贮罐,干气缓冲罐,干气脱硫脱氯塔,干气柜,熔盐加热炉,熔盐泵,熔盐罐; The technical solution adopted by the present invention to solve the technical problem is: a device for refining gasoline and diesel oil using waste lubricating oil, including a settling tank, a high-temperature oil pump, a flash tank, a vaporization kettle, a vaporization kettle filter tower, an induced draft fan, and a flue gas purification device , fixed bed catalytic tower, fractionation tower, gasoline water cooler, diesel water cooler, diesel intermediate tank, gear oil pump, diesel storage tank, also includes vacuum pump group, oil and gas separation tank, reflux pump, gasoline storage tank, dry gas buffer tank , dry gas desulfurization and dechlorination tower, dry gas cabinet, molten salt heating furnace, molten salt pump, molten salt tank;
所述的沉降罐一端通入废润滑油,一端连接高温油泵; One end of the settling tank is filled with waste lubricating oil, and the other end is connected to a high-temperature oil pump;
所述的高温油泵另一端连接闪蒸罐,闪蒸罐内设置有搅拌装置,目的是对润滑油进行脱水及将废润滑油轻组分馏出;闪蒸罐另一端连接高温油泵; The other end of the high-temperature oil pump is connected to a flash tank, and a stirring device is installed in the flash tank for dehydrating the lubricating oil and distilling off the light components of the waste lubricating oil; the other end of the flash tank is connected to a high-temperature oil pump;
所述的高温油泵另一端连接汽化釜,汽化釜设置有排渣装置,用于排除经汽化釜催化裂解后油气里的粉状炭黑残留物; The other end of the high-temperature oil pump is connected to a vaporization kettle, and the vaporization kettle is provided with a slagging device for removing powdery carbon black residues in the oil and gas after catalytic cracking by the vaporization kettle;
所述的汽化釜的另一端连接汽化釜过滤塔,用于过滤油气中的碳粉;汽化釜过滤塔和固定床催化塔连接,固定床催化塔的另一端连接分馏塔; The other end of the vaporization kettle is connected to the vaporization kettle filter tower for filtering the carbon powder in the oil and gas; the vaporizer filter tower is connected to the fixed-bed catalytic tower, and the other end of the fixed-bed catalytic tower is connected to the fractionation tower;
所述的固定床催化塔连接引风机,引风机另一端连接烟气净化装置; The fixed-bed catalytic tower is connected with an induced draft fan, and the other end of the induced draft fan is connected with a flue gas purification device;
所述的分馏塔分别连接柴油用水冷却器和汽油用水冷却器; Described fractionation tower is respectively connected diesel water cooler and gasoline water cooler;
所述的柴油用水冷却器依次连接柴油中间罐,齿轮油泵和柴油贮罐; The diesel water cooler is sequentially connected with a diesel intermediate tank, a gear oil pump and a diesel storage tank;
所述的汽油用水冷却器依次连接油气分离罐,齿轮油泵和汽油贮罐; The gasoline water cooler is sequentially connected with the oil-gas separation tank, the gear oil pump and the gasoline storage tank;
所述的油气分离罐又依次连接真空泵组,干气缓冲罐,干气脱硫脱氯净化装置,干气柜和熔盐加热炉; The oil-gas separation tank is sequentially connected with a vacuum pump group, a dry gas buffer tank, a dry gas desulfurization and dechlorination purification device, a dry gas cabinet and a molten salt heating furnace;
所述的油气分离罐连接回流泵,回流泵连接分馏塔; The oil-gas separation tank is connected with a reflux pump, and the reflux pump is connected with a fractionation tower;
所述的熔盐加热炉连接熔盐泵,熔盐泵连接熔盐罐,熔盐加热炉通过管道连接闪蒸罐,汽化釜和固定床催化塔; The molten salt heating furnace is connected to a molten salt pump, the molten salt pump is connected to a molten salt tank, and the molten salt heating furnace is connected to a flash tank, a vaporizer and a fixed-bed catalytic tower through pipelines;
所述的熔盐罐通过管道与汽化釜和闪蒸罐连接; The molten salt tank is connected with the vaporizer and the flash tank through pipelines;
所述的闪蒸罐通过管道连接汽油用水冷却器,用于将闪蒸罐中的废润滑油轻组通入汽油用水冷却器进行冷却; The flash tank is connected to the gasoline water cooler through a pipeline, and is used to pass the waste lubricating oil light group in the flash tank into the gasoline water cooler for cooling;
所述的汽化釜是一个密闭的卧式容器,容器内部有螺旋推进器,螺旋推进器上面均匀布满刮片; The vaporization kettle is a closed horizontal container with a screw propeller inside the container, and the screw propeller is evenly covered with scrapers;
所述的闪蒸罐,汽化釜,固定床催化塔,分馏塔,油气分离罐,熔盐加热炉均设置有现场温度计,现场压力表和远传温度计,远传压力表,柴油中间罐和油气分离罐均设置有液位控制计和液位显示计。 The flash tank, vaporizer, fixed-bed catalytic tower, fractionation tower, oil-gas separation tank, and molten salt heating furnace are all equipped with on-site thermometers, on-site pressure gauges and remote thermometers, remote pressure gauges, diesel intermediate tanks and oil-gas The separation tanks are all equipped with liquid level control gauges and liquid level display gauges.
本发明的有益效果是,一种采用废润滑油提炼汽柴油装置,该装置使得废润滑油得到充分的再次利用,且环保无污染,减少了废气的排放,能连续生产,降低能耗,易操作,对润滑油的处理能够实现完全无害化、无污染及最优资源化利用。 The beneficial effect of the present invention is that a device adopts waste lubricating oil to refine gasoline and diesel oil, which can fully reuse the waste lubricating oil, is environmentally friendly and pollution-free, reduces waste gas emissions, can be continuously produced, reduces energy consumption, and is easy to use. Operation, the treatment of lubricating oil can achieve complete harmlessness, no pollution and optimal resource utilization.
附图说明 Description of drawings
下面结合复合和实施例对本发明进一步说明。 Below in conjunction with composite and embodiment the present invention is further described.
图1为本发明的结构示意图。 Fig. 1 is a structural schematic diagram of the present invention.
图中1.沉降罐,2.高温油泵,3.闪蒸罐,4.汽化釜,5.汽化釜过滤塔,6.固定床催化塔,7.分馏塔,8.引风机,9.烟气净化装置,10柴油用水冷却器,11.柴油中间罐,12.齿轮油泵,13.柴油贮罐,14.回流泵,15.汽油用水冷却器,16.油气分离罐,17.汽油贮罐,18.真空泵组,19.干气缓冲罐,20.干气脱硫脱氯塔,21.干气柜,22.熔盐加热炉,23.熔盐泵,24.熔盐罐。 In the figure 1. Settling tank, 2. High temperature oil pump, 3. Flash tank, 4. Vaporization tank, 5. Vaporization tank filter tower, 6. Fixed bed catalytic tower, 7. Fractionation tower, 8. Induced fan, 9. Smoke Gas purification device, 10 diesel water cooler, 11. diesel intermediate tank, 12. gear oil pump, 13. diesel storage tank, 14. return pump, 15. gasoline water cooler, 16. oil-gas separation tank, 17. gasoline storage tank , 18. Vacuum pump group, 19. Dry gas buffer tank, 20. Dry gas desulfurization and dechlorination tower, 21. Dry gas cabinet, 22. Molten salt heating furnace, 23. Molten salt pump, 24. Molten salt tank.
具体实施方式 detailed description
参照附图,一种采用废润滑油提炼汽柴油装置,包括沉降罐1,高温油泵2,闪蒸罐3,汽化釜4,汽化釜过滤塔5,固定床催化塔6,分馏塔7,引风机8,烟气净化装置9,柴油用水冷却器10,柴油中间罐11,齿轮油泵12,柴油贮罐13,还包括回流泵14,汽油用水冷却器15,油气分离罐16,汽油贮罐17,真空泵组18,干气缓冲罐19,干气脱硫脱氯塔20,干气柜21,熔盐加热炉22,熔盐泵23,熔盐罐24。 Referring to the accompanying drawings, a device for refining gasoline and diesel oil using waste lubricating oil includes a settling tank 1, a high-temperature oil pump 2, a flash tank 3, a vaporization kettle 4, a vaporization kettle filter tower 5, a fixed-bed catalytic tower 6, a fractionation tower 7, and Fan 8, flue gas purification device 9, diesel water cooler 10, diesel intermediate tank 11, gear oil pump 12, diesel storage tank 13, return pump 14, gasoline water cooler 15, oil-gas separation tank 16, gasoline storage tank 17 , vacuum pump group 18, dry gas buffer tank 19, dry gas desulfurization and dechlorination tower 20, dry gas cabinet 21, molten salt heating furnace 22, molten salt pump 23, molten salt tank 24.
所述的沉降罐1一端通入废润滑油,一端连接高温油泵2,沉降罐1的目的是将废润滑油进行抽检分离处理,降低含水量及沉淀除杂; One end of the settling tank 1 is filled with waste lubricating oil, and the other end is connected to the high-temperature oil pump 2. The purpose of the settling tank 1 is to conduct random inspection and separation of the waste lubricating oil, reduce water content and remove impurities from precipitation;
所述的高温油泵2另一端连接闪蒸罐3,闪蒸罐3内设置有搅拌装置,目的是对润滑油进行脱水及将废润滑油轻组分馏出;闪蒸罐3另一端连接高温油泵2; The other end of the high-temperature oil pump 2 is connected to the flash tank 3, and the flash tank 3 is provided with a stirring device for dehydrating the lubricating oil and distilling the light components of the waste lubricating oil; the other end of the flash tank 3 is connected to the high-temperature oil pump 2;
所述的高温油泵2另一端连接汽化釜4,汽化釜4设置有排渣装置,用于排除经汽化釜4催化裂解后油气里的粉状炭黑残留物; The other end of the high-temperature oil pump 2 is connected to the vaporization kettle 4, and the vaporization kettle 4 is provided with a slagging device for removing powdery carbon black residues in the oil gas after catalytic cracking by the vaporization kettle 4;
所述的汽化釜4的另一端连接汽化釜过滤塔5,用于过滤油气中的碳粉;汽化釜过滤塔5和固定床催化塔6连接,固定床催化塔6的另一端连接分馏塔7; The other end of the vaporization kettle 4 is connected to the vaporization kettle filter tower 5 for filtering the carbon powder in the oil and gas; the vaporizer kettle filter tower 5 is connected to the fixed-bed catalytic tower 6, and the other end of the fixed-bed catalytic tower 6 is connected to the fractionation tower 7 ;
所述的固定床催化塔6连接引风机8,引风机8另一端连接烟气净化装置9; The fixed bed catalytic tower 6 is connected with an induced draft fan 8, and the other end of the induced draft fan 8 is connected with a flue gas purification device 9;
所述的分馏塔7分别连接柴油用水冷却器10和汽油用水冷却器15; Described fractionation tower 7 is respectively connected diesel water cooler 10 and gasoline water cooler 15;
所述的柴油用水冷却器10依次连接柴油中间罐11,齿轮油泵12和柴油贮罐13; Described diesel water cooler 10 is connected successively with diesel intermediate tank 11, gear oil pump 12 and diesel storage tank 13;
所述的汽油用水冷却器15依次连接油气分离罐16,齿轮油泵12和汽油贮罐17; Described gasoline water cooler 15 is connected successively with oil-gas separation tank 16, gear oil pump 12 and gasoline storage tank 17;
所述的油气分离罐16又依次连接真空泵组18,干气缓冲罐19,干气脱硫脱氯净化装置20,干气柜21和熔盐加热炉22; The oil-gas separation tank 16 is connected in turn to a vacuum pump group 18, a dry gas buffer tank 19, a dry gas desulfurization and dechlorination purification device 20, a dry gas cabinet 21 and a molten salt heating furnace 22;
所述的油气分离罐16连接回流泵14,回流泵14连接分馏塔7,目的是起到回流作用,用于控制分馏塔塔顶温度; The oil-gas separation tank 16 is connected to the reflux pump 14, and the reflux pump 14 is connected to the fractionation tower 7, and the purpose is to play a reflux effect for controlling the temperature at the top of the fractionation tower;
所述的熔盐加热炉22连接熔盐泵23,熔盐泵23连接熔盐罐24,熔盐加热炉22通过管道连接闪蒸罐3,汽化釜4和固定床催化塔6; The molten salt heating furnace 22 is connected to the molten salt pump 23, and the molten salt pump 23 is connected to the molten salt tank 24, and the molten salt heating furnace 22 is connected to the flash tank 3, the vaporization kettle 4 and the fixed bed catalytic tower 6 through pipelines;
所述的熔盐罐24通过管道与汽化釜4和闪蒸罐3连接; Described molten salt tank 24 is connected with vaporizer 4 and flash tank 3 by pipeline;
所述的闪蒸罐3通过管道连接汽油用水冷却器15,用于将闪蒸罐3中的废润滑油轻组通入汽油用水冷却器15进行冷却。 The flash tank 3 is connected to the gasoline water cooler 15 through pipelines, and is used to pass the waste lubricating oil light group in the flash tank 3 into the gasoline water cooler 15 for cooling.
所述的汽化釜4是一个密闭的卧式容器,容器内部有螺旋推进器,螺旋推进器上面均匀布满刮片。 The vaporization kettle 4 is an airtight horizontal container with a screw propeller inside the container, and the screw propeller is evenly covered with scrapers.
所述的闪蒸罐3,汽化釜4,固定床催化塔6,分馏塔7,油气分离罐16,熔盐加热炉22均设置有现场温度计,现场压力表和远传温度计,远传压力表,柴油中间罐11和油气分离罐16均设置有液位控制计和液位显示计。 Described flash tank 3, vaporizer 4, fixed-bed catalytic tower 6, fractionation tower 7, oil-gas separation tank 16, molten salt heating furnace 22 are all provided with on-site thermometer, on-site pressure gauge and remote transmission thermometer, remote transmission pressure gauge , The diesel intermediate tank 11 and the oil-gas separation tank 16 are equipped with a liquid level control gauge and a liquid level display gauge.
Claims (3)
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510086437.6A CN104611007B (en) | 2015-02-25 | 2015-02-25 | A kind of waste lubricating oil refines petrol and diesel oil device |
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| KR100213986B1 (en) * | 1997-02-04 | 1999-08-02 | 최수현 | Process for producing high quality fuel oil by simultaneous pyrolysis of waste lubricant and waste plastic in a continuous process |
| CN1107109C (en) * | 2000-10-26 | 2003-04-30 | 中国石油化工股份有限公司 | Process for recovering waste oil |
| CN1236016C (en) * | 2003-04-25 | 2006-01-11 | 谢福胜 | Method and device for producing vapour, coal, diesel oil using waste plastic, rubber, machine oil |
| CN1854272A (en) * | 2005-04-26 | 2006-11-01 | 李平 | Method for reducing finished product mobile oil and refining gasoline and diesel from waste mobile oil and its apparatus thereof |
| SG161129A1 (en) * | 2008-10-31 | 2010-05-27 | Annda Energy Pte Ltd | Process and system for regeneration of spent lubrication oil |
| CN204455012U (en) * | 2015-02-25 | 2015-07-08 | 烟台荣盛压力容器制造有限公司 | A kind of waste lubricating oil refines petrol and diesel oil device |
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