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CN104178002A - Oil-in-oil alkyd resin multicolor internal wall paint - Google Patents

Oil-in-oil alkyd resin multicolor internal wall paint Download PDF

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Publication number
CN104178002A
CN104178002A CN201410409887.XA CN201410409887A CN104178002A CN 104178002 A CN104178002 A CN 104178002A CN 201410409887 A CN201410409887 A CN 201410409887A CN 104178002 A CN104178002 A CN 104178002A
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CN
China
Prior art keywords
parts
oil
internal wall
paint
synolac
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410409887.XA
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Chinese (zh)
Inventor
费金华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Wujiang Huacheng Composite Technology Co Ltd
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Wujiang Huacheng Composite Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Wujiang Huacheng Composite Technology Co Ltd filed Critical Wujiang Huacheng Composite Technology Co Ltd
Priority to CN201410409887.XA priority Critical patent/CN104178002A/en
Publication of CN104178002A publication Critical patent/CN104178002A/en
Pending legal-status Critical Current

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Abstract

The invention relates to an oil-in-oil alkyd resin multicolor internal wall paint is prepared from the following raw materials in parts by weight: 100 parts of rosin modified alkyd resin, 15-25 parts of trimethylolpropane triacrylate, 1-20 parts of styrene-butadiene block copolymer, 1-10 parts of 3,3',4,4'-benzophenonetetracarboxylic-acid dianhydride, 5-15 parts of tung oil, 25-45 parts of hydroquinone, 80-90 parts of deionized water, 15-35 parts of phenothiazine, 10-20 parts of pigment, 25-35 parts of tripropylene glycol diacrylate, 30-40 parts of ethyl cellulose, 10-30 parts of 2,2-dimethoxy-2-phenylacetophenone, 8-10 parts of plasticizer, 20-40 parts of acetophenone, 20-30 parts of tetrabutyl titanate and 35-45 parts of pentaerythritol triacrylate. The surface drying time of the coated film is 0.5-1.5 hours, the solid drying time is 8-12 hours, and the coated film can not expose the substrate after being scrubbed 3000-5000 times. The film-forming temperature is 5 DEG C, and the paint can not blister or shed after being immersed in 20 DEG C water for 30-50 days. The normal-temperature storage stability is 8-10 months, and the paint can resist an alkaline saturated calcium hydroxide solution for 20-40 days, and thus, can be widely produced and used instead of the existing material.

Description

A kind of oily oil-in Synolac multi-colour paint for internal wall
Technical field
The application belongs to paint field, relates in particular to a kind of oily oil-in Synolac multi-colour paint for internal wall.
Background technology
Coating, in China, tradition name is called paint.So-called coating is to be coated in protected or decorated body surface; and can form with coated article the continuous film of firm attachment, normally, taking resin or oil or emulsion as main, add or do not add pigment, filler; add corresponding additive, with organic solvent or the formulated thick liquid of tung oil.China's coating circle more authoritative " coating process " book is definition like this: " coating is a kind of material, and this material can be coated in article surface by different construction technologies, forms and adheres to firmly, has some strength, continuous solid film.The film common name film forming like this, claims again paint film or coating." paint finishing can and form the material of complete and tough and tensile protective membrane with the fine bonding of body material in body surface, is called coating.Coating and paint are identical concepts.Paint is people's custom titles used for a long time, introduces after China, just utilizes in building trade always.The effect of coating may be summarized to be three aspects: provide protection, decoration function, specific function effect.The general composition of coating: comprise filmogen, color stuffing, solvent, auxiliary agent.Rosin modified alkyd resin refers to and in the preparation process of Synolac, adds properties-correcting agent rosin, the modified resin of making through chemical reaction; Due to the modification of rosin, make this resin be soluble in esters solvent, can increase the sticking power of paint film, reduce paint film wrinkling, improve weather resistance, alkali resistance and the gloss of paint film, reduce viscosity; Due to the modification of rosin, make this resin be soluble in esters solvent, can increase the sticking power of paint film, reduce paint film wrinkling, improve weather resistance, alkali resistance and the gloss of paint film, reduce viscosity; Paint film release solvent is also very fast, and dry rate improves, and parches quickening.But itself contains conjugated double bond rosin, thus not ageing-resistant, when consumption is many, affect weathering resistance; Also can cause variable color, embrittlement.So should carry out as required to determine the consumption of Abietyl modified dose.
Coating refers to the general name that is applied to body surface and can form the material of tough and tensile protective membrane, and building coating is an important class in coating, in China, generally will be used for inner wall of building, exterior wall, and ceiling, ground, the coating of toilet is called building coating.Interior wall coating is exactly the emulsion paint of generally fitting up use.Emulsion paint is emulsion coating, according to the difference of base material, is divided into polyvinyl acetate emulsion and the large class of ACRYLIC EMULSION two.Emulsion paint is taking water as thinner, be a kind of easy construction, safe, water-fastness, good permeability coating, it can mix different color and lusters according to different scheme of colo(u)r.Kind: water-based inner wall paint, oiliness interior wall paint, dry powder type interior wall paint, belong to water-borne coatings, mainly by water, emulsion, pigment, filler, five kinds of compositions of additive form.
So-called oily oil-in Synolac multi-colour paint for internal wall is made up of inconsistent two phase compositions, wherein a phase dispersion medium is external phase, and another is disperse phase mutually, when application, by disposable spray finishing, just can obtain the colorful pattern of luxurious, attractive in appearance, oily oil-in Synolac.Interior wall paint also makes interior wall coating comprise liquid coating and powder coating, and common emulsion paint, wall paint belong to liquid coating.In the making composition of interior wall coating, be substantially made up of water, pigment, emulsion, weighting agent and various auxiliary agent, these starting material are not contain what toxicity.As emulsion paint, may be toxic be mainly that ethylene glycol in film coalescence aid is with the organic mercury in Fang Mildew agent.And universal along with humanity concept, and the formation of novel harmonious society, the oily oil-in Synolac multi-colour paint for internal wall that designs a kind of water tolerance, scrub resistance and alkali resistance excellence is very important.
Summary of the invention
The technical problem solving:
The application, for above-mentioned technical problem, provides a kind of oily oil-in Synolac multi-colour paint for internal wall, solves existing oily oil-in Synolac multi-colour paint for internal wall water tolerance and scrub resistance is poor, package stability is poor, the technical problem such as alkali corrosion resistance not.
Technical scheme:
A kind of oily oil-in Synolac multi-colour paint for internal wall, the raw materials by weight portion proportioning of described oily oil-in Synolac multi-colour paint for internal wall is as follows: 100 parts of rosin modified alkyd resins; Viscoat 295 15-25 part; Styrene-butadiene block copolymer 1-20 part; 3,3 ' 4,4 '-benzophenone tetracarboxylic dianhydride 1-10 part; Tung oil 5-15 part; Resorcinol 25-45 part; Deionized water 80-90 part; Thiodiphenylamine 15-35 part; Pigment 10-20 part; Tri (propylene glycol) diacrylate 25-35 part; Ethyl cellulose 30-40 part; Benzoin dimethylether 10-30 part; Softening agent 8-10 part; Phenyl methyl ketone 20-40 part; Tetrabutyl titanate 20-30 part; Pentaerythritol triacrylate 35-45 part.
As a preferred technical solution of the present invention: the raw materials by weight portion proportioning of described oily oil-in Synolac multi-colour paint for internal wall is as follows: 100 parts of rosin modified alkyd resins; 20 parts of Viscoat 295s; 10 parts of styrene-butadiene block copolymers; 3,3 ' 4,5 parts of 4 '-benzophenone tetracarboxylic dianhydride; 10 parts of tung oil; 35 parts of Resorcinol; 85 parts of deionized waters; 25 parts of thiodiphenylamine; 15 parts of pigment; 30 parts of tri (propylene glycol) diacrylates; 35 parts of ethyl cellulose; 20 parts of benzoin dimethylethers; 9 parts, softening agent; 30 parts of phenyl methyl ketones; 25 parts of tetrabutyl titanates; 40 parts of pentaerythritol triacrylates.
As a preferred technical solution of the present invention: described pigment adopts red iron oxide, iron oxide yellow or medium chrome yellow medium yellow.
As a preferred technical solution of the present invention: described softening agent adopts DBP.
Beneficial effect:
The oily oil-in Synolac of one of the present invention multi-colour paint for internal wall adopts above technical scheme compared with prior art, has following technique effect: 1, film surface drying 0.5-1.5h, do solid work 8-12h, and scrubbing resistance 3000-5000 time is not show-through; 2,5 DEG C of film-forming temperatures, non-foaming soak 30-50d in 20 DEG C of water after, dry linting not; 3, storage at normal temperature stability 8-10 month, the saturated aqua calcis 20-40d of alkali resistance, can the not division of history into periods of widespread production replace current material.
Embodiment
Embodiment 1:
A kind of oily oil-in Synolac multi-colour paint for internal wall, its raw materials by weight portion proportioning is as follows: 100 parts of rosin modified alkyd resins; 15 parts of Viscoat 295s; 1 part of styrene-butadiene block copolymer; 3,3 ' 4,1 part of 4 '-benzophenone tetracarboxylic dianhydride; 5 parts of tung oil; 25 parts of Resorcinol; 80 parts of deionized waters; 15 parts of thiodiphenylamine; 10 parts of medium chrome yellow medium yellows; 25 parts of tri (propylene glycol) diacrylates; 30 parts of ethyl cellulose; 10 parts of benzoin dimethylethers; DBP8 part; 20 parts of phenyl methyl ketones; 20 parts of tetrabutyl titanates; 35 parts of pentaerythritol triacrylates.
By rosin modified alkyd resin, styrene-butadiene block copolymer, 3,3 ' 4,4 '-benzophenone tetracarboxylic dianhydride, tung oil and Resorcinol add in deionized water, be heated to 40 DEG C and stir 3h, add thiodiphenylamine, tri (propylene glycol) diacrylate, ethyl cellulose, benzoin dimethylether, tetrabutyl titanate and DBP, be warming up to 50 DEG C with ball mill ball milling 10min, add Viscoat 295 and surplus stock, be warming up to 60 DEG C and both stir after 10h to obtain finished product.
Film surface drying 1.5h, does solid work 12h, and scrubbing resistance 3000 times is not show-through; Non-foaming soak 30d in 20 DEG C of water after, dry linting not; Storage at normal temperature stability 8 months, the saturated aqua calcis 20d of alkali resistance.
Embodiment 2:
A kind of oily oil-in Synolac multi-colour paint for internal wall, its raw materials by weight portion proportioning is as follows: 100 parts of rosin modified alkyd resins; 25 parts of Viscoat 295s; 20 parts of styrene-butadiene block copolymers; 3,3 ' 4,10 parts of 4 '-benzophenone tetracarboxylic dianhydride; 15 parts of tung oil; 45 parts of Resorcinol; 90 parts of deionized waters; 35 parts of thiodiphenylamine; 20 parts of iron oxide yellow; 35 parts of tri (propylene glycol) diacrylates; 40 parts of ethyl cellulose; 30 parts of benzoin dimethylethers; DBP10 part; 40 parts of phenyl methyl ketones; 30 parts of tetrabutyl titanates; 45 parts of pentaerythritol triacrylates.
By rosin modified alkyd resin, styrene-butadiene block copolymer, 3,3 ' 4,4 '-benzophenone tetracarboxylic dianhydride, tung oil and Resorcinol add in deionized water, be heated to 40 DEG C and stir 3h, add thiodiphenylamine, tri (propylene glycol) diacrylate, ethyl cellulose, benzoin dimethylether, tetrabutyl titanate and DBP, be warming up to 50 DEG C with ball mill ball milling 10min, add Viscoat 295 and surplus stock, be warming up to 60 DEG C and both stir after 10h to obtain finished product.
Film surface drying 1h, does solid work 10h, and scrubbing resistance 4000 times is not show-through; Non-foaming soak 40d in 20 DEG C of water after, dry linting not; Storage at normal temperature stability 9 months, the saturated aqua calcis 30d of alkali resistance.
Embodiment 3:
A kind of oily oil-in Synolac multi-colour paint for internal wall, its raw materials by weight portion proportioning is as follows: 100 parts of rosin modified alkyd resins; 20 parts of Viscoat 295s; 10 parts of styrene-butadiene block copolymers; 3,3 ' 4,5 parts of 4 '-benzophenone tetracarboxylic dianhydride; 10 parts of tung oil; 35 parts of Resorcinol; 85 parts of deionized waters; 25 parts of thiodiphenylamine; 15 parts of red iron oxides; 30 parts of tri (propylene glycol) diacrylates; 35 parts of ethyl cellulose; 20 parts of benzoin dimethylethers; DBP9 part; 30 parts of phenyl methyl ketones; 25 parts of tetrabutyl titanates; 40 parts of pentaerythritol triacrylates.
By rosin modified alkyd resin, styrene-butadiene block copolymer, 3,3 ' 4,4 '-benzophenone tetracarboxylic dianhydride, tung oil and Resorcinol add in deionized water, be heated to 40 DEG C and stir 3h, add thiodiphenylamine, tri (propylene glycol) diacrylate, ethyl cellulose, benzoin dimethylether, tetrabutyl titanate and DBP, be warming up to 50 DEG C with ball mill ball milling 10min, add Viscoat 295 and surplus stock, be warming up to 60 DEG C and both stir after 10h to obtain finished product.
Film surface drying 0.5h, does solid work 8h, and scrubbing resistance 5000 times is not show-through; Non-foaming soak 50d in 20 DEG C of water after, dry linting not; Storage at normal temperature stability 10 months, the saturated aqua calcis 40d of alkali resistance.
Composition all components in above embodiment all can business be bought.

Claims (4)

1. an oily oil-in Synolac multi-colour paint for internal wall, is characterized in that the raw materials by weight portion proportioning of described oily oil-in Synolac multi-colour paint for internal wall is as follows: 100 parts of rosin modified alkyd resins; Viscoat 295 15-25 part; Styrene-butadiene block copolymer 1-20 part; 3,3 ' 4,4 '-benzophenone tetracarboxylic dianhydride 1-10 part; Tung oil 5-15 part; Resorcinol 25-45 part; Deionized water 80-90 part; Thiodiphenylamine 15-35 part; Pigment 10-20 part; Tri (propylene glycol) diacrylate 25-35 part; Ethyl cellulose 30-40 part; Benzoin dimethylether 10-30 part; Softening agent 8-10 part; Phenyl methyl ketone 20-40 part; Tetrabutyl titanate 20-30 part; Pentaerythritol triacrylate 35-45 part.
2. the oily oil-in Synolac of one according to claim 1 multi-colour paint for internal wall, is characterized in that the raw materials by weight portion proportioning of described oily oil-in Synolac multi-colour paint for internal wall is as follows: 100 parts of rosin modified alkyd resins; 20 parts of Viscoat 295s; 10 parts of styrene-butadiene block copolymers; 3,3 ' 4,5 parts of 4 '-benzophenone tetracarboxylic dianhydride; 10 parts of tung oil; 35 parts of Resorcinol; 85 parts of deionized waters; 25 parts of thiodiphenylamine; 15 parts of pigment; 30 parts of tri (propylene glycol) diacrylates; 35 parts of ethyl cellulose; 20 parts of benzoin dimethylethers; 9 parts, softening agent; 30 parts of phenyl methyl ketones; 25 parts of tetrabutyl titanates; 40 parts of pentaerythritol triacrylates.
3. the oily oil-in Synolac of one according to claim 1 multi-colour paint for internal wall, is characterized in that: described pigment adopts red iron oxide, iron oxide yellow or medium chrome yellow medium yellow.
4. the oily oil-in Synolac of one according to claim 1 multi-colour paint for internal wall, is characterized in that: described softening agent adopts DBP.
CN201410409887.XA 2014-08-20 2014-08-20 Oil-in-oil alkyd resin multicolor internal wall paint Pending CN104178002A (en)

Priority Applications (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104974645A (en) * 2015-08-03 2015-10-14 苏州舒而适纺织新材料科技有限公司 Multicolor paint

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3573237A (en) * 1968-01-08 1971-03-30 John C Zola Decorative finish-producing composition and method of applying same
CN1102193A (en) * 1993-11-01 1995-05-03 韩晓根 Multi-colour paint for internal wall
CN1103092A (en) * 1993-11-26 1995-05-31 中国矿业大学 Water-in-water type multi-colour figure paint
CN1124266A (en) * 1994-12-07 1996-06-12 湖南天海林实业股份有限公司 Multi-colour paint
CN102093797A (en) * 2011-02-12 2011-06-15 郭鸿林 Water-in-water colorful exterior and interior wall architectural paint, preparation method and coating method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3573237A (en) * 1968-01-08 1971-03-30 John C Zola Decorative finish-producing composition and method of applying same
CN1102193A (en) * 1993-11-01 1995-05-03 韩晓根 Multi-colour paint for internal wall
CN1103092A (en) * 1993-11-26 1995-05-31 中国矿业大学 Water-in-water type multi-colour figure paint
CN1124266A (en) * 1994-12-07 1996-06-12 湖南天海林实业股份有限公司 Multi-colour paint
CN102093797A (en) * 2011-02-12 2011-06-15 郭鸿林 Water-in-water colorful exterior and interior wall architectural paint, preparation method and coating method thereof

Non-Patent Citations (4)

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Title
化学工业出版社组织编写: "《中国化工产品大全 第三版 中卷》", 31 January 2005, 化学工业出版社 *
彭安顺等: "《精细有机品化学》", 31 August 1996, 石油大学出版社出版 *
徐峰: "《建筑涂料与涂装技术》", 31 May 2000, 化学工业出版社 *
董翔等: "经济型聚糖改性醇酸树脂漆", 《中国涂料》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104974645A (en) * 2015-08-03 2015-10-14 苏州舒而适纺织新材料科技有限公司 Multicolor paint

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