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CH466818A - Process for treating a liquid by means of a gaseous fluid and installation for carrying out this process - Google Patents

Process for treating a liquid by means of a gaseous fluid and installation for carrying out this process

Info

Publication number
CH466818A
CH466818A CH1725667A CH1725667A CH466818A CH 466818 A CH466818 A CH 466818A CH 1725667 A CH1725667 A CH 1725667A CH 1725667 A CH1725667 A CH 1725667A CH 466818 A CH466818 A CH 466818A
Authority
CH
Switzerland
Prior art keywords
liquid
gas
basin
treated
propeller
Prior art date
Application number
CH1725667A
Other languages
French (fr)
Inventor
Bendel Henri
Original Assignee
Pista Sa
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Pista Sa filed Critical Pista Sa
Priority to CH1725667A priority Critical patent/CH466818A/en
Priority to FR1554378D priority patent/FR1554378A/fr
Priority to GB2035868A priority patent/GB1221022A/en
Publication of CH466818A publication Critical patent/CH466818A/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/24Treatment of water, waste water, or sewage by flotation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/232Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles
    • B01F23/2326Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles adding the flowing main component by suction means, e.g. using an ejector
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/232Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using flow-mixing means for introducing the gases, e.g. baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/233Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements
    • B01F23/2331Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements characterised by the introduction of the gas along the axis of the stirrer or along the stirrer elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/233Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements
    • B01F23/2331Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements characterised by the introduction of the gas along the axis of the stirrer or along the stirrer elements
    • B01F23/23312Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements characterised by the introduction of the gas along the axis of the stirrer or along the stirrer elements through a conduit surrounding the stirrer axis
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/233Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements
    • B01F23/2334Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements provided with stationary guiding means surrounding at least partially the stirrer
    • B01F23/23342Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements provided with stationary guiding means surrounding at least partially the stirrer the stirrer being of the centrifugal type, e.g. with a surrounding stator
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20Mixing gases with liquids
    • B01F23/23Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/233Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements
    • B01F23/2336Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements characterised by the location of the place of introduction of the gas relative to the stirrer
    • B01F23/23363Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids using driven stirrers with completely immersed stirring elements characterised by the location of the place of introduction of the gas relative to the stirrer the gas being introduced above the stirrer
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/72Treatment of water, waste water, or sewage by oxidation
    • C02F1/76Treatment of water, waste water, or sewage by oxidation with halogens or compounds of halogens
    • C02F1/763Devices for the addition of such compounds in gaseous form
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/02Aerobic processes
    • C02F3/12Activated sludge processes
    • C02F3/20Activated sludge processes using diffusers
    • C02F3/205Moving, e.g. rotary, diffusers; Stationary diffusers with moving, e.g. rotary, distributors
    • C02F3/207Moving, e.g. rotary, diffusers; Stationary diffusers with moving, e.g. rotary, distributors with axial thrust propellers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/111Centrifugal stirrers, i.e. stirrers with radial outlets; Stirrers of the turbine type, e.g. with means to guide the flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/113Propeller-shaped stirrers for producing an axial flow, e.g. shaped like a ship or aircraft propeller
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/19Stirrers with two or more mixing elements mounted in sequence on the same axis
    • B01F27/192Stirrers with two or more mixing elements mounted in sequence on the same axis with dissimilar elements
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00Technologies for wastewater treatment
    • Y02W10/10Biological treatment of water, waste water, or sewage

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Microbiology (AREA)
  • Earth Drilling (AREA)
  • Physical Water Treatments (AREA)

Description

Procédé de traitement d'un liquide au moyen d'un fluide gazeux et installation pour la mise en oeuvre de ce procédé Dans differentes industries et, notamment, dans le domaine du traitement des eaux, il est souvent necessaire de gazéifier un liquide pour obtenir des reactions chimiques ou biologiques particulières, pour saturer le liquide avec un gaz, ou encore pour eliminer des matie- res en suspension vers la surface du liquide par flottai soll, etc. Process for treating a liquid by means of a gaseous fluid and installation for carrying out this process In various industries and, in particular, in the field of water treatment, it is often necessary to gasify a liquid to obtain specific chemical or biological reactions, to saturate the liquid with a gas, or even to eliminate suspended matter. towards the surface of the liquid by flotai sol, etc.

Generalement, cette gazeification est réalisée par in sufflation de gaz sous pression dans la masse liquide ou par projection du liquide dans une ambiance gazeuse ou encore à l'aide d'agitateurs rotatifs en combinaison avec une insufflation de gaz sous pression en dessous des pales de l'agitateur. Generally, this gasification is carried out by insufflation of gas under pressure in the liquid mass or by projection of the liquid in a gaseous atmosphere or even using rotary agitators in combination with an insufflation of gas under pressure below the blades of the agitator.

La presente invention a pour objet un procédé de traitement d'un liquide au moyen d'un fluide gazeux caractérisé en ce qu'on diffuse le fluide gazeux directement dans un volume reduit de la masse liquide à traiter et en ce qu'on propulse ce volume reduit de liquide traite dans le reste de la masse liquide brute. The subject of the present invention is a process for treating a liquid by means of a gaseous fluid characterized in that the gaseous fluid is diffused directly into a reduced volume of the liquid mass to be treated and in that this is propelled reduced volume of treated liquid in the rest of the gross liquid mass.

L'invention a egalement pour objet une installation pour la mise en ceuvre du procédé indiqué ci-dessus, installation comprenant un bassin destine à contenir le liquide à traiter, une conduite d'amenée du liquide brut au bassin et une conduite d'évacuation du liquide traité, une pompe rotative centrifuge pour disperser le fluide gazeux dans le liquide, un organe de brassage en forme d'hélice disposé sous la pompe et entraîné parle même arbre à partir du meme moteur, la conduite d'amenée de fluide gazeux à la pompe formant un tube de guidage autour de l'arbre plongeant dans le liquide. L'installation selon l'invention est caractérisée par le fait qu'elle comprend une virole entourant la pompe avec jeu et dont un prolongement tubulaire vers le bas entoure l'organe de brassage, cette virole etant entièrement noyée dans le bassin, le tout etant dispoé de maniere que la pompe n'injecte directement du fluide gazeux que dans un volume reduit du liquide à traiter, limité par la virole, ce volume reduit etant ensuite propulsé par l'hélice dans le reste du bassin. The invention also relates to an installation for the implementation of the method indicated above, installation comprising a basin intended to contain the liquid to be treated, a pipe for supplying the raw liquid to the basin and a pipe for discharging the treated liquid, a centrifugal rotary pump for dispersing the gaseous fluid in the liquid, a propeller-shaped stirring member arranged under the pump and driven by the same shaft from the same motor, the gaseous fluid supply pipe to the pump forming a guide tube around the shaft dipping into the liquid. The installation according to the invention is characterized in that it comprises a ferrule surrounding the pump with clearance and of which a downward tubular extension surrounds the brewing member, this ferrule being entirely embedded in the basin, the whole being arranged so that the pump directly injects gaseous fluid only into a reduced volume of the liquid to be treated, limited by the shell, this reduced volume then being propelled by the propeller into the rest of the basin.

Le dessin annexé represente, schematiquement et à titre d'exemple, une forme d'exécution de 1' installation selon l'invention. The accompanying drawing represents, schematically and by way of example, one embodiment of the installation according to the invention.

La figure unique de ce dessin montre 1' installation selon une vue en coupe axiale. The single figure in this drawing shows the installation in an axial section view.

En référence au dessin, cette installation comprend un bassin, ou cuve, 1 destine à contenir le liquide 2 à traiter. Cette cuve 1 est de préférence de section cir- culaire. Au centre de la cuve 1 est disposee une virole 3 ouverte à sa partie supérieure et dont le bord 4 se trouve en dessous du niveau constant 5 du liquide 2. Le fond 6 de la virole 3 est de forme tronconique et aboutit en son centre à un prolongement tubulaire 7 dirigé vers le fond 8 de la cuve 1 qui est en forme de tremie egalement tronconique dans la forme d'exécution représentée. La virole 3 qui peut, par exemple, etre construite en tôle ou en element de ciment ou autre matiere, est concentrique à un tube de guidage 9 disposé dans l'axe du bassin 1. La virole 3 est relief au tube de guidage 9 par des supports 10. A l'intérieur du tube de guidage 9 est loge un arbre 11 destine à etre entraîné par un moteur electrique 12 porte par l'extrémité supérieure du tube 9. Le tube de guidage 9 est muni d'une ouverture 13 d'aspiration de gaz situee au-dessus du niveau 5 du liquide 2. A sa partie inférieure, le tube de guidage 9 presente une collerette 14 portant à sa périphérie un certain nombre de nervures 15 destindes à constituer le diffuseur d'une pompe centrifuge dont la roue 16 est partie par l'arbre 11. Cette collerette 14 et le diffuseur 15 constituent, en fait, un demi-corps de pompe. La roue 16 est en forme de disque muni à sa face supérieure de nervures radiales 17. En bout de l'arbre 11, au-dessous de la roue 16, est disposde une helice 18 constituant un organe de brassage ou de propulsion du liquide. With reference to the drawing, this installation comprises a basin, or tank, 1 intended to contain the liquid 2 to be treated. This tank 1 is preferably of circular section. In the center of the tank 1 is arranged a shell 3 open at its upper part and whose edge 4 is below the constant level 5 of the liquid 2. The bottom 6 of the shell 3 is of frustoconical shape and ends in its center at a tubular extension 7 directed towards the bottom 8 of the tank 1 which is in the form of a hopper, also frustoconical in the embodiment shown. The ferrule 3 which can, for example, be constructed of sheet metal or a cement element or other material, is concentric with a guide tube 9 arranged in the axis of the basin 1. The ferrule 3 is raised to the guide tube 9 by supports 10. Inside the guide tube 9 is housed a shaft 11 intended to be driven by an electric motor 12 carried by the upper end of the tube 9. The guide tube 9 is provided with an opening 13 d gas suction located above the level 5 of the liquid 2. At its lower part, the guide tube 9 has a flange 14 carrying at its periphery a number of ribs 15 intended to constitute the diffuser of a centrifugal pump whose the impeller 16 is part by the shaft 11. This collar 14 and the diffuser 15 constitute, in fact, a pump half-body. The wheel 16 is in the form of a disc provided on its upper face with radial ribs 17. At the end of the shaft 11, below the wheel 16, is disposed a propeller 18 constituting a member for mixing or propelling the liquid.

Le liquide à traiter est amene dans le bassin 1 par une conduite 19 débouchant à l'intérieur de la virole 3. The liquid to be treated is brought into the basin 1 by a pipe 19 opening inside the shell 3.

Une conduite d'évacuation 20 du liquide traité est raccordée à la partie inférieure du bassin 1, c'est-ä-dire à proximite du fond 8 de celui-ci. La hauteur du trop-plein 21 que forme cette conduite d'évacuation 20 détermine le niveau 5 du liquide 2 dans le bassin 1. An evacuation pipe 20 for the treated liquid is connected to the lower part of the tank 1, that is to say close to the bottom 8 of the latter. The height of the overflow 21 formed by this discharge pipe 20 determines the level 5 of the liquid 2 in the basin 1.

La virole 3, le tube de guidage 9 et le moteur 12 d'entrainement de l'arbre 11, de la roue 16 et de l'hélice 18, sont supportes au centre du bassin 1 par des entretoises, ou rails de support, 23 disposees diamétralement au-dessus du bassin 1. The ferrule 3, the guide tube 9 and the motor 12 driving the shaft 11, the wheel 16 and the propeller 18, are supported at the center of the basin 1 by spacers, or support rails, 23 arranged diametrically above pool 1.

Le fonctionnement de l'installation décrite ci-dessus est le suivant : le liquide à gazéifier s'écoule par la conduite 19 à l'intérieur de la virole 3. Le niveau 5 du liquide 2 à traiter correspond à la hauteur du trop-plein 21. Le gaz à introduire dans le liquide 2 est amené à l'ouverture d'aspiration 13 aménagée dans le tube 9. Lorsque le moteur 12 tourne, ilmet en rotation la roue de pompe 16, d'une part, et l'hélice 18, d'autre part. Selon le sens de rotation du moteur 12, le liquide est refoulé du fond du bassin 1 vers l'intérieur de la virole 3 à travers le prolongement tubulaire 7 entourant l'hélice 18 (dans le sens indiqué par les flèches en trait plein représentées sur la moitié gauche de la figure). Le liquide passe ainsi par un espace reduit 22 entourant le diffuseur 15. Lors de ce passage dans cet espace reduit 22, le gaz projeté par la roue de pompe 16 et ses ailettes 17 à travers le diffuseur 15, est finement disperse dans l'espace 22 dans lequel le liquide à traiter est obligé de passer. Il s'ensuit donc un mélange intime du gaz et du liquide, mélange qui monte à l'intérieur de la virole 3. Le gaz non dissous dans le liquide s'échappe alors à la surface 5 du liquide. La duree de contact gazliquide depend ainsi de la distance entre l'espace 22 et la surface 5 du liquide 2. si l'on désire prolonger la durée de contact gaz-liquide, on fait fonctionner le moteur 12 en sens inverse comme représenté sur le cote droit de la figure (flèches en pointillé). Le sens du courant résultant de la propulsion de l'hélice 18 est alors inversé. Le liquide entre par le haut de la virole 3, passe dans l'es- pace reduit 22 pour etre gazéifié, le melange gaz-liquide etant ensuite refoulé par l'hélice 18 vers le fond 8 du bassin 1. On remarque ainsi que plus le prolongement tubulaire 7 sera long et le fond 8 du bassin 1 à plus grande distance de l'espace 22, plus grande sera la durée de contact du melange gaz-liquide. En effet, le gaz non dissous dans le liquide doit remonter entre la virole 3 et le bassin 1 avant d'arriver à la surface 5 où il peut s'échapper. The operation of the installation described above is as follows: the liquid to be gasified flows through the pipe 19 inside the shroud 3. The level 5 of the liquid 2 to be treated corresponds to the height of the overflow 21. The gas to be introduced into the liquid 2 is brought to the suction opening 13 provided in the tube 9. When the motor 12 rotates, it rotates the pump wheel 16, on the one hand, and the propeller 18, on the other hand. According to the direction of rotation of the motor 12, the liquid is discharged from the bottom of the basin 1 towards the inside of the ferrule 3 through the tubular extension 7 surrounding the propeller 18 (in the direction indicated by the solid line arrows represented on the left half of the figure). The liquid thus passes through a reduced space 22 surrounding the diffuser 15. During this passage through this reduced space 22, the gas projected by the pump wheel 16 and its fins 17 through the diffuser 15, is finely dispersed in the space. 22 in which the liquid to be treated is forced to pass. This therefore results in an intimate mixture of the gas and the liquid, a mixture which rises inside the shroud 3. The gas not dissolved in the liquid then escapes to the surface 5 of the liquid. The gas-liquid contact time thus depends on the distance between the space 22 and the surface 5 of the liquid 2. if it is desired to extend the gas-liquid contact time, the motor 12 is operated in the opposite direction as shown on the right side of the figure (dotted arrows). The direction of the current resulting from the propulsion of the propeller 18 is then reversed. The liquid enters through the top of the shroud 3, passes into the reduced space 22 to be gasified, the gas-liquid mixture then being pushed back by the propeller 18 towards the bottom 8 of the basin 1. It is thus noted that more the tubular extension 7 will be long and the bottom 8 of the basin 1 at a greater distance from the space 22, the greater will be the duration of contact of the gas-liquid mixture. Indeed, the gas not dissolved in the liquid must rise between the shell 3 and the basin 1 before reaching the surface 5 where it can escape.

Il est évident qu'en variant la vitesse de rotation du moteur 12, on peut régler le volume d'introduction de gaz et le debit de brassage du liquide. It is obvious that by varying the speed of rotation of the motor 12, it is possible to adjust the volume of introduction of gas and the flow rate of mixing of the liquid.

Le bassin, ou cuve, 1 peut être fermé à sa partie sup6rieure si la nature des gaz à introduire dans la masse liquide l'exige. Ceci peut être le cas par exemple si le gaz est un gaz toxique, un gaz rare ou un gaz explosif à récupérer et à faire circuler en circuit fermé à l'intérieur de l'installation. Par contre, si 1' installation n'est utilisee que pour une simple aération d'une masse liquide, le bassin 1 peut etre ouvert. The basin, or tank, 1 can be closed at its upper part if the nature of the gases to be introduced into the liquid mass so requires. This may be the case, for example, if the gas is a toxic gas, a rare gas or an explosive gas to be recovered and circulated in a closed circuit inside the installation. On the other hand, if the installation is only used for a simple aeration of a liquid mass, the basin 1 can be open.

L'avantage du procédé décrit ci-dessus reside en particulier dans le fait que le liquide à traiter est oblige de circuler et de passer à proximité directe de l'injection du gaz en assurant ainsi une gazeification uniforme de la masse liquide, sans créer des zones préférentielles de gazéification, comme c'est le cas avec les procédés classiques. Cet avantage est d'autant plus marqué que seul un volume réduit de la masse liquide 2 est traité à la fois par diffusion de gaz, c'est-ä-dire uniquement le volume contenu à l'intérieur de la virole 3. Le traitement se poursuit bien entendu par la propulsion de cette masse liquide primaire traitée dans la masse liquide secondaire 2 encore à l'état brut. The advantage of the method described above resides in particular in the fact that the liquid to be treated is forced to circulate and pass in direct proximity to the gas injection, thus ensuring uniform gasification of the liquid mass, without creating preferential gasification zones, as is the case with conventional processes. This advantage is all the more marked in that only a reduced volume of the liquid mass 2 is treated at a time by gas diffusion, that is to say only the volume contained inside the shroud 3. The treatment continues of course with the propulsion of this treated primary liquid mass in the secondary liquid mass 2 still in its raw state.

En outre, selon le sens de circulation du liquide propulsé par l'hélice 18 on peut, selon les conditions de traitement désirées, raccourcir ou prolonger la durée de contact entre le liquide et le gaz, ceci simplement en faisant circuler le liquide dans le sens montant ou dans le sens descendant à l'intérieur de la virole 3. Bien entendu, le moteur electrique 12 devra etre prdvu pour pouvoir fonctionner dans les deux sens de rotation et, éventuellement, à différents régimes de rotation selon le degré de diffusion de gaz que l'on désire obtenir. In addition, depending on the direction of circulation of the liquid propelled by the propeller 18, it is possible, depending on the desired treatment conditions, to shorten or prolong the duration of contact between the liquid and the gas, this simply by causing the liquid to circulate in the direction amount or in the downward direction inside the ferrule 3. Of course, the electric motor 12 must be provided to be able to operate in both directions of rotation and, possibly, at different rotation speeds depending on the degree of gas diffusion that we want to obtain.

REVENDICATIONS I. Procédé de traitement d'un liquide au moyen d'un fluide gazeux, caractérisé en ce qu'on diffuse le fluide gazeux directement dans un volume réduit de la masse liquide (2) à traiter et en ce qu'on propulse ce volume reduit de liquide traite dans le reste de la masse liquide brute. CLAIMS I. Process for treating a liquid by means of a gaseous fluid, characterized in that the gaseous fluid is diffused directly into a reduced volume of the liquid mass (2) to be treated and in that this is propelled reduced volume of treated liquid in the rest of the gross liquid mass.

II. Installation pour la mise en uvre du procédé selon la revendication I, comprennnt un bassin (1) destine à contenir le liquide à traiter, une conduite d'amenée du liquide brut au bassin (1) et une conduite (20) d'évacuation du liquide traité, une pompe rotative centrifuge (16) pour disperser le fluide gazeux dans le liquide (2), un organe de brassage (18) en forme d'hélice disposé sous la pompe (16) et entraîné par le même arbre (11) à partir du même moteur (12), la conduite d'amenée de fluide gazeux à la pompe (16) formant un tube de guidage (9) autour de l'arbre (11) plongeant dans le liquide, caracterisee en ce qu'elle comprend une virole (3) entourant la pompe (16) avec jeu et dont un prolongement tubulaire (7) vers le bas entoure 1' organe de brassage (18), cette virole (3) étant entièrement noyée dans le bassin (1), le tout étant disposé de manière que la pompe (16) n'injecte directement du fluide gazeux que dans un volume reduit du liquide à traiter (2), limité par la virole (3), ce volume reduit etant ensuite propulsé par l'hélice (18) dans le reste du bassin (1). II. Installation for carrying out the method according to claim I, comprising a basin (1) intended to contain the liquid to be treated, a pipe for supplying the crude liquid to the basin (1) and a pipe (20) for discharging the treated liquid, a rotary centrifugal pump (16) for dispersing the gaseous fluid in the liquid (2), a stirring member (18) in the form of a propeller disposed under the pump (16) and driven by the same shaft (11) from the same motor (12), the pipe for supplying gaseous fluid to the pump (16) forming a guide tube (9) around the shaft (11) immersed in the liquid, characterized in that it comprises a shroud (3) surrounding the pump (16) with clearance and of which a downward tubular extension (7) surrounds the stirring member (18), this shroud (3) being entirely embedded in the basin (1), the whole being arranged so that the pump (16) directly injects gaseous fluid only into a reduced volume of the liquid to be treated (2), limited by the shroud (3), this reduced volume then being propelled by the propeller (18) in the rest of the basin (1).

SOUS-REVENDICATIONS 1. Instalaltion selon la revendication II, caractérisée en ce que le moteur (12) est susceptible d'entraîner la pompe (16) et l'hélice (18) dans les deux sens, le choix d'un sens de rotation permettant une mise en contact du volume reduit traite avec le liquide brut (2) sur un plus long chemin que dans le sens inverse. SUB-CLAIMS 1. Installation according to claim II, characterized in that the motor (12) is capable of driving the pump (16) and the propeller (18) in both directions, the choice of a direction of rotation allowing a setting in contact of the reduced volume deals with the raw liquid (2) over a longer path than in the opposite direction.

2. Installation selon la revendication II et la sons- revendication 1, caractérisée en ce que la conduite (19) d'amenée du liquide brut (2) debouche à l'Intérieur de la virole (3), la conduite (20) d'évacuation ayant son entre à proximité du fond (8) du bassin (1). 2. Installation according to claim II and sub-claim 1, characterized in that the pipe (19) for supplying the raw liquid (2) opens inside the shell (3), the pipe (20) d evacuation having its entry near the bottom (8) of the basin (1).

**WARNUNG** Ende DESC Feld konnte Anfang CLMS uberlappen**. **WARNUNG** Ende DESC Feld konnte Anfang CLMS uberlappen**.

Claims (5)

WARNUNG* Anfang CLMS Feld konnte Ende DESC uberlappen *.WARNUNG* Anfang CLMS Feld konnte Ende DESC uberlappen *. disposde une helice 18 constituant un organe de brassage ou de propulsion du liquide. has a propeller 18 constituting a liquid stirring or propulsion member. Le liquide à traiter est amene dans le bassin 1 par une conduite 19 débouchant à l'intérieur de la virole 3.The liquid to be treated is brought into the basin 1 by a pipe 19 opening inside the shell 3. Une conduite d'évacuation 20 du liquide traité est raccordée à la partie inférieure du bassin 1, c'est-ä-dire à proximite du fond 8 de celui-ci. La hauteur du trop-plein 21 que forme cette conduite d'évacuation 20 détermine le niveau 5 du liquide 2 dans le bassin 1.An evacuation pipe 20 for the treated liquid is connected to the lower part of the tank 1, that is to say close to the bottom 8 of the latter. The height of the overflow 21 formed by this discharge pipe 20 determines the level 5 of the liquid 2 in the basin 1. La virole 3, le tube de guidage 9 et le moteur 12 d'entrainement de l'arbre 11, de la roue 16 et de l'hélice 18, sont supportes au centre du bassin 1 par des entretoises, ou rails de support, 23 disposees diamétralement au-dessus du bassin 1.The ferrule 3, the guide tube 9 and the motor 12 driving the shaft 11, the wheel 16 and the propeller 18, are supported at the center of the basin 1 by spacers, or support rails, 23 arranged diametrically above basin 1. Le fonctionnement de l'installation décrite ci-dessus est le suivant : le liquide à gazéifier s'écoule par la conduite 19 à l'intérieur de la virole 3. Le niveau 5 du liquide 2 à traiter correspond à la hauteur du trop-plein 21. Le gaz à introduire dans le liquide 2 est amené à l'ouverture d'aspiration 13 aménagée dans le tube 9. Lorsque le moteur 12 tourne, ilmet en rotation la roue de pompe 16, d'une part, et l'hélice 18, d'autre part. Selon le sens de rotation du moteur 12, le liquide est refoulé du fond du bassin 1 vers l'intérieur de la virole 3 à travers le prolongement tubulaire 7 entourant l'hélice 18 (dans le sens indiqué par les flèches en trait plein représentées sur la moitié gauche de la figure). Le liquide passe ainsi par un espace reduit 22 entourant le diffuseur 15. Lors de ce passage dans cet espace reduit 22, le gaz projeté par la roue de pompe 16 et ses ailettes 17 à travers le diffuseur 15, est finement disperse dans l'espace 22 dans lequel le liquide à traiter est obligé de passer. Il s'ensuit donc un mélange intime du gaz et du liquide, mélange qui monte à l'intérieur de la virole 3. Le gaz non dissous dans le liquide s'échappe alors à la surface 5 du liquide. La duree de contact gazliquide depend ainsi de la distance entre l'espace 22 et la surface 5 du liquide 2. si l'on désire prolonger la durée de contact gaz-liquide, on fait fonctionner le moteur 12 en sens inverse comme représenté sur le cote droit de la figure (flèches en pointillé). Le sens du courant résultant de la propulsion de l'hélice 18 est alors inversé. Le liquide entre par le haut de la virole 3, passe dans l'es- pace reduit 22 pour etre gazéifié, le melange gaz-liquide etant ensuite refoulé par l'hélice 18 vers le fond 8 du bassin 1. On remarque ainsi que plus le prolongement tubulaire 7 sera long et le fond 8 du bassin 1 à plus grande distance de l'espace 22, plus grande sera la durée de contact du melange gaz-liquide. En effet, le gaz non dissous dans le liquide doit remonter entre la virole 3 et le bassin 1 avant d'arriver à la surface 5 où il peut s'échapper. The operation of the installation described above is as follows: the liquid to be gasified flows through the pipe 19 inside the shroud 3. The level 5 of the liquid 2 to be treated corresponds to the height of the overflow 21. The gas to be introduced into the liquid 2 is brought to the suction opening 13 provided in the tube 9. When the motor 12 rotates, it rotates the pump wheel 16, on the one hand, and the propeller 18, on the other hand. According to the direction of rotation of the motor 12, the liquid is discharged from the bottom of the basin 1 towards the inside of the ferrule 3 through the tubular extension 7 surrounding the propeller 18 (in the direction indicated by the solid line arrows represented on the left half of the figure). The liquid thus passes through a reduced space 22 surrounding the diffuser 15. During this passage through this reduced space 22, the gas projected by the pump wheel 16 and its fins 17 through the diffuser 15, is finely dispersed in the space. 22 in which the liquid to be treated is forced to pass. This therefore results in an intimate mixture of the gas and the liquid, a mixture which rises inside the shroud 3. The gas not dissolved in the liquid then escapes to the surface 5 of the liquid. The gas-liquid contact time thus depends on the distance between the space 22 and the surface 5 of the liquid 2. if it is desired to extend the gas-liquid contact time, the motor 12 is operated in the opposite direction as shown on the right side of the figure (dotted arrows). The direction of the current resulting from the propulsion of the propeller 18 is then reversed. The liquid enters through the top of the shroud 3, passes into the reduced space 22 to be gasified, the gas-liquid mixture then being pushed back by the propeller 18 towards the bottom 8 of the basin 1. It is thus noted that more the tubular extension 7 will be long and the bottom 8 of the basin 1 at a greater distance from the space 22, the greater will be the duration of contact of the gas-liquid mixture. Indeed, the gas not dissolved in the liquid must rise between the shell 3 and the basin 1 before reaching the surface 5 where it can escape. Il est évident qu'en variant la vitesse de rotation du moteur 12, on peut régler le volume d'introduction de gaz et le debit de brassage du liquide.It is obvious that by varying the speed of rotation of the motor 12, it is possible to adjust the volume of introduction of gas and the flow rate of mixing of the liquid. Le bassin, ou cuve, 1 peut être fermé à sa partie sup6rieure si la nature des gaz à introduire dans la masse liquide l'exige. Ceci peut être le cas par exemple si le gaz est un gaz toxique, un gaz rare ou un gaz explosif à récupérer et à faire circuler en circuit fermé à l'intérieur de l'installation. Par contre, si 1' installation n'est utilisee que pour une simple aération d'une masse liquide, le bassin 1 peut etre ouvert.The basin, or tank, 1 can be closed at its upper part if the nature of the gases to be introduced into the liquid mass so requires. This may be the case, for example, if the gas is a toxic gas, a rare gas or an explosive gas to be recovered and circulated in a closed circuit inside the installation. On the other hand, if the installation is only used for a simple aeration of a liquid mass, the basin 1 can be open. L'avantage du procédé décrit ci-dessus reside en particulier dans le fait que le liquide à traiter est oblige de circuler et de passer à proximité directe de l'injection du gaz en assurant ainsi une gazeification uniforme de la masse liquide, sans créer des zones préférentielles de gazéification, comme c'est le cas avec les procédés classiques. Cet avantage est d'autant plus marqué que seul un volume réduit de la masse liquide 2 est traité à la fois par diffusion de gaz, c'est-ä-dire uniquement le volume contenu à l'intérieur de la virole 3. Le traitement se poursuit bien entendu par la propulsion de cette masse liquide primaire traitée dans la masse liquide secondaire 2 encore à l'état brut.The advantage of the method described above resides in particular in the fact that the liquid to be treated is forced to circulate and pass in direct proximity to the gas injection, thus ensuring uniform gasification of the liquid mass, without creating preferential gasification zones, as is the case with conventional processes. This advantage is all the more marked in that only a reduced volume of the liquid mass 2 is treated at a time by gas diffusion, that is to say only the volume contained inside the shroud 3. The treatment continues of course with the propulsion of this treated primary liquid mass in the secondary liquid mass 2 still in its raw state. En outre, selon le sens de circulation du liquide propulsé par l'hélice 18 on peut, selon les conditions de traitement désirées, raccourcir ou prolonger la durée de contact entre le liquide et le gaz, ceci simplement en faisant circuler le liquide dans le sens montant ou dans le sens descendant à l'intérieur de la virole 3. Bien entendu, le moteur electrique 12 devra etre prdvu pour pouvoir fonctionner dans les deux sens de rotation et, éventuellement, à différents régimes de rotation selon le degré de diffusion de gaz que l'on désire obtenir.In addition, depending on the direction of circulation of the liquid propelled by the propeller 18, it is possible, depending on the desired treatment conditions, to shorten or prolong the duration of contact between the liquid and the gas, this simply by causing the liquid to circulate in the direction amount or in the downward direction inside the ferrule 3. Of course, the electric motor 12 must be provided to be able to operate in both directions of rotation and, possibly, at different rotation speeds depending on the degree of gas diffusion that we want to obtain. REVENDICATIONS I. Procédé de traitement d'un liquide au moyen d'un fluide gazeux, caractérisé en ce qu'on diffuse le fluide gazeux directement dans un volume réduit de la masse liquide (2) à traiter et en ce qu'on propulse ce volume reduit de liquide traite dans le reste de la masse liquide brute. CLAIMS I. Process for treating a liquid by means of a gaseous fluid, characterized in that the gaseous fluid is diffused directly into a reduced volume of the liquid mass (2) to be treated and in that this is propelled reduced volume of treated liquid in the rest of the gross liquid mass. II. Installation pour la mise en uvre du procédé selon la revendication I, comprennnt un bassin (1) destine à contenir le liquide à traiter, une conduite d'amenée du liquide brut au bassin (1) et une conduite (20) d'évacuation du liquide traité, une pompe rotative centrifuge (16) pour disperser le fluide gazeux dans le liquide (2), un organe de brassage (18) en forme d'hélice disposé sous la pompe (16) et entraîné par le même arbre (11) à partir du même moteur (12), la conduite d'amenée de fluide gazeux à la pompe (16) formant un tube de guidage (9) autour de l'arbre (11) plongeant dans le liquide, caracterisee en ce qu'elle comprend une virole (3) entourant la pompe (16) avec jeu et dont un prolongement tubulaire (7) vers le bas entoure 1' organe de brassage (18), cette virole (3) étant entièrement noyée dans le bassin (1), le tout étant disposé de manière que la pompe (16) n'injecte directement du fluide gazeux que dans un volume reduit du liquide à traiter (2), limité par la virole (3), ce volume reduit etant ensuite propulsé par l'hélice (18) dans le reste du bassin (1).II. Installation for carrying out the method according to claim I, comprising a basin (1) intended to contain the liquid to be treated, a pipe for supplying the crude liquid to the basin (1) and a pipe (20) for discharging the treated liquid, a rotary centrifugal pump (16) for dispersing the gaseous fluid in the liquid (2), a stirring member (18) in the form of a propeller disposed under the pump (16) and driven by the same shaft (11) from the same motor (12), the pipe for supplying gaseous fluid to the pump (16) forming a guide tube (9) around the shaft (11) immersed in the liquid, characterized in that it comprises a shroud (3) surrounding the pump (16) with clearance and of which a downward tubular extension (7) surrounds the stirring member (18), this shroud (3) being entirely embedded in the basin (1), the whole being arranged so that the pump (16) directly injects gaseous fluid only into a reduced volume of the liquid to be treated (2), limited by the shroud (3), this reduced volume then being propelled by the propeller (18) in the rest of the basin (1). SOUS-REVENDICATIONSSUB-CLAIMS 1. Instalaltion selon la revendication II, caractérisée en ce que le moteur (12) est susceptible d'entraîner la pompe (16) et l'hélice (18) dans les deux sens, le choix d'un sens de rotation permettant une mise en contact du volume reduit traite avec le liquide brut (2) sur un plus long chemin que dans le sens inverse. 1. Installation according to claim II, characterized in that the motor (12) is capable of driving the pump (16) and the propeller (18) in both directions, the choice of a direction of rotation allowing a setting in contact of the reduced volume deals with the raw liquid (2) over a longer path than in the opposite direction. 2. Installation selon la revendication II et la sons- revendication 1, caractérisée en ce que la conduite (19) d'amenée du liquide brut (2) debouche à l'Intérieur de la virole (3), la conduite (20) d'évacuation ayant son entre à proximité du fond (8) du bassin (1). 2. Installation according to claim II and sub-claim 1, characterized in that the pipe (19) for supplying the raw liquid (2) opens inside the shell (3), the pipe (20) d evacuation having its entry near the bottom (8) of the basin (1). 3. Installation selon la revendication II et les sousrevendications 1 et 2, caractérisée en ce que l'extrémité inférieure du tube (9) de guidage de l'arbre (11) porte une collerette évasée (14) constituant un demi-corps de pompe au-dessus de la roue de pompe (16), cette colle rette (14) etant munie de nervures radiales (15) formant un diffuseur autour de la roue de pompe (16).3. Installation according to claim II and subclaims 1 and 2, characterized in that the lower end of the tube (9) for guiding the shaft (11) carries a flared collar (14) constituting a pump half-body above the pump wheel (16), this adhesive rette (14) being provided with radial ribs (15) forming a diffuser around the pump wheel (16). 4. Installation selon la revendication II et les sousrevendications 1 à 3, caractérisée en ce que la partie principale de la virole (3), qui est en forme general de cylindre vertical, est reliee à son prolongement tubulaire (7) entourant l'hélice (18) par une partie tronconique (6).4. Installation according to claim II and subclaims 1 to 3, characterized in that the main part of the shell (3), which is in the general shape of a vertical cylinder, is connected to its tubular extension (7) surrounding the propeller (18) by a frustoconical part (6). 5. Installation selon la revendication II et les sousrevendications 1 à 4, caractérisée en ce que le fond (8) du bassin (1) est en forme de tremie dont la zone infe- rieure se trouve en regard dudit prolongement cylindrique (7). 5. Installation according to claim II and sub-claims 1 to 4, characterized in that the bottom (8) of the basin (1) is in the form of a hopper, the lower zone of which is opposite the said cylindrical extension (7).
CH1725667A 1967-12-08 1967-12-08 Process for treating a liquid by means of a gaseous fluid and installation for carrying out this process CH466818A (en)

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CH1725667A CH466818A (en) 1967-12-08 1967-12-08 Process for treating a liquid by means of a gaseous fluid and installation for carrying out this process
FR1554378D FR1554378A (en) 1967-12-08 1968-02-14
GB2035868A GB1221022A (en) 1967-12-08 1968-04-30 Treatment of a liquid by means of a gaseous fluid

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FR2336967A1 (en) * 1975-12-30 1977-07-29 Popel Franz LIQUID CARBONATION PLANT

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DE2646517C2 (en) * 1976-10-15 1984-11-29 Stelzer, Erwin, Ing.(Grad.), 3530 Warburg Gassing device
US4139579A (en) * 1977-07-15 1979-02-13 Albert Blum Apparatus for introducing air into a liquid including a liquid pump mounted within an aerator pressure chamber
DE3002429A1 (en) * 1980-01-24 1981-07-30 Ystral Gmbh Maschinenbau Und Processtechnik, 7801 Ballrechten-Dottingen Gas powder and fluid dispersing device - combines hollow rotor with jet mixer principle
DE3715331A1 (en) * 1987-05-08 1988-12-01 Berents Gmbh & Co Kg A HOMOGENIZER FOR THE PRODUCTION OF FLOWABLE PRODUCTS
GB8829220D0 (en) * 1988-12-15 1989-01-25 Thames Water Authority Sludge treatment
FR2662616B1 (en) * 1990-05-31 1994-07-08 Anjou Rech INSTALLATION FOR THE TREATMENT OF LIQUID FLOWS WITH SINGLE-PHASE CONTACTOR, AND RECIRCULATOR-DEGASSER DEVICE FOR SUCH AN INSTALLATION.
FR2672230B1 (en) * 1991-02-04 1993-04-16 Anjou Rech INSTALLATION FOR MIXING TWO FLUID PHASES BY MECHANICAL SHAKING, PARTICULARLY FOR THE TREATMENT OF WATER BY TRANSFERRING OXIDIZING GAS, AND USE OF SUCH AN INSTALLATION.
GB2294209B (en) * 1991-09-26 1996-07-03 Charles Edward Eckert Method for treating a molten metal with a gas
US5562821A (en) * 1995-07-21 1996-10-08 Commonwealth Of Puerto Rico Foam fractionator
WO2004050254A1 (en) * 2002-12-05 2004-06-17 Johannes Swanepoel Familie Trust An impeller for a froth flotation cell
FR2868335B1 (en) * 2004-04-02 2006-06-02 Air Liquide DEVICE FOR INJECTING A GAS INTO A LIQUID
FR2884442B1 (en) * 2005-04-19 2007-05-25 Air Liquide DEVICE FOR STIMULATING A LIQUID AND INJECTING A GAS IN THIS LIQUID SUITABLE FOR LOW DEPTH BASINS
DE102008050223B4 (en) * 2008-10-07 2011-07-28 Entwicklungsgesellschaft Frank Mohr u. Gerhard Krüger, jun. Gbr. 25715 Eddelak (vertretungsber. Gesellschafter: Frank Mohr, 20249 Hamburg u. Gerhard Krüger, 25767 Bunsoh), 25715 Device for cleaning waste water, in particular from livestock, and a method for using the device
CN119793375B (en) * 2025-03-12 2025-06-10 湖南维摩新材料有限公司 Reaction kettle flow control device for methyl isocyanate production

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2336967A1 (en) * 1975-12-30 1977-07-29 Popel Franz LIQUID CARBONATION PLANT

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FR1554378A (en) 1969-01-17
GB1221022A (en) 1971-02-03

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