CA1169289A - Process for the production of a syrup having a high fructose concentration - Google Patents
Process for the production of a syrup having a high fructose concentrationInfo
- Publication number
- CA1169289A CA1169289A CA000389989A CA389989A CA1169289A CA 1169289 A CA1169289 A CA 1169289A CA 000389989 A CA000389989 A CA 000389989A CA 389989 A CA389989 A CA 389989A CA 1169289 A CA1169289 A CA 1169289A
- Authority
- CA
- Canada
- Prior art keywords
- glucose
- syrup
- product
- fructose
- crystallisation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000006188 syrup Substances 0.000 title claims abstract description 52
- 235000020357 syrup Nutrition 0.000 title claims abstract description 52
- 239000005715 Fructose Substances 0.000 title claims abstract description 46
- 229930091371 Fructose Natural products 0.000 title claims abstract description 45
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 title claims abstract description 45
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 65
- 239000008103 glucose Substances 0.000 claims abstract description 65
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims abstract description 59
- 239000013078 crystal Substances 0.000 claims abstract description 28
- 238000002425 crystallisation Methods 0.000 claims abstract description 20
- 238000010899 nucleation Methods 0.000 claims abstract description 13
- 239000000463 material Substances 0.000 claims abstract description 8
- 102000004195 Isomerases Human genes 0.000 claims abstract description 6
- 108090000769 Isomerases Proteins 0.000 claims abstract description 6
- 238000001704 evaporation Methods 0.000 claims abstract description 5
- 239000000047 product Substances 0.000 claims abstract 15
- 238000001816 cooling Methods 0.000 claims abstract 2
- 239000012456 homogeneous solution Substances 0.000 claims abstract 2
- 239000000203 mixture Substances 0.000 claims description 19
- 238000001914 filtration Methods 0.000 claims description 4
- 238000004064 recycling Methods 0.000 claims description 4
- 230000008020 evaporation Effects 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims 1
- 238000000926 separation method Methods 0.000 claims 1
- 229960001031 glucose Drugs 0.000 abstract description 57
- 235000001727 glucose Nutrition 0.000 abstract description 55
- 229960002737 fructose Drugs 0.000 abstract description 40
- 238000002156 mixing Methods 0.000 abstract description 3
- 244000052616 bacterial pathogen Species 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 150000001720 carbohydrates Chemical class 0.000 description 11
- 235000021433 fructose syrup Nutrition 0.000 description 10
- 235000000346 sugar Nutrition 0.000 description 5
- 238000006317 isomerization reaction Methods 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 238000005342 ion exchange Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 235000013681 dietary sucrose Nutrition 0.000 description 2
- 235000019534 high fructose corn syrup Nutrition 0.000 description 2
- 229960004793 sucrose Drugs 0.000 description 2
- 108010093096 Immobilized Enzymes Proteins 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000002441 reversible effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Seasonings (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DK488880A DK145582B (da) | 1980-11-14 | 1980-11-14 | Fremgangsmaade til fremstilling af sirup med hoejt fruktoseindhold |
| DK4888/80 | 1980-11-14 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CA1169289A true CA1169289A (en) | 1984-06-19 |
Family
ID=8137559
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CA000389989A Expired CA1169289A (en) | 1980-11-14 | 1981-11-13 | Process for the production of a syrup having a high fructose concentration |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS57118796A (es) |
| AR (1) | AR224976A1 (es) |
| AU (1) | AU544659B2 (es) |
| BE (1) | BE891093A (es) |
| CA (1) | CA1169289A (es) |
| DE (1) | DE3145185A1 (es) |
| DK (1) | DK145582B (es) |
| FI (1) | FI72742B (es) |
| FR (1) | FR2494088B1 (es) |
| GB (1) | GB2087400B (es) |
| HU (1) | HU182414B (es) |
| YU (1) | YU43049B (es) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4634472A (en) * | 1985-08-23 | 1987-01-06 | A. E. Staley Manufacturing Company | Enrichment of fructose syrups |
| WO2007076640A1 (fr) * | 2006-01-06 | 2007-07-12 | Bioright Worldwide Company Ltd. | Methode permettant de preparer simultanement des sirops presentant une teneur elevee en fructose (55 % et 42%) |
| WO2007079606A1 (fr) * | 2006-01-06 | 2007-07-19 | Bioright Worldwide Company Ltd. | Procédé de préparation par cristallisation d'un sirop à haute teneur en fructose contenant du fructose hautement concentré |
| CN110904170B (zh) * | 2019-12-12 | 2022-01-28 | 山东省鲁洲食品集团有限公司 | 一种f-55果葡糖浆的制备方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI46631C (fi) * | 1971-03-11 | 1973-05-08 | Suomen Sokeri Oy | Menetelmä fruktoosin kiteyttämiseksi väkevöidystä vesiliuoksesta |
| FR2245765B1 (es) * | 1973-09-27 | 1976-06-18 | Rhone Poulenc Ind | |
| IT1104769B (it) * | 1977-07-05 | 1985-10-28 | Snam Progetti | Procedimento per la produzione di fruttosio e sciroppi contenenti fruttosio e glucosid e mezzi adatti per la realizzazione del procedimento stesso |
-
1980
- 1980-11-14 DK DK488880A patent/DK145582B/da unknown
-
1981
- 1981-11-11 FI FI813576A patent/FI72742B/fi not_active Application Discontinuation
- 1981-11-11 GB GB8134020A patent/GB2087400B/en not_active Expired
- 1981-11-12 AU AU77438/81A patent/AU544659B2/en not_active Ceased
- 1981-11-12 BE BE0/206523A patent/BE891093A/fr not_active IP Right Cessation
- 1981-11-13 DE DE19813145185 patent/DE3145185A1/de not_active Withdrawn
- 1981-11-13 CA CA000389989A patent/CA1169289A/en not_active Expired
- 1981-11-13 HU HU339781A patent/HU182414B/hu unknown
- 1981-11-13 YU YU268281A patent/YU43049B/xx unknown
- 1981-11-13 FR FR8121306A patent/FR2494088B1/fr not_active Expired
- 1981-11-13 JP JP18295781A patent/JPS57118796A/ja active Pending
- 1981-11-18 AR AR28745481A patent/AR224976A1/es active
Also Published As
| Publication number | Publication date |
|---|---|
| FR2494088B1 (fr) | 1985-08-09 |
| DE3145185A1 (de) | 1982-08-05 |
| DK488880A (da) | 1982-05-15 |
| HU182414B (en) | 1984-01-30 |
| GB2087400A (en) | 1982-05-26 |
| DK145582B (da) | 1982-12-13 |
| FI813576L (fi) | 1982-05-15 |
| FR2494088A1 (fr) | 1982-05-21 |
| BE891093A (fr) | 1982-03-01 |
| JPS57118796A (en) | 1982-07-23 |
| AR224976A1 (es) | 1982-01-29 |
| AU544659B2 (en) | 1985-06-06 |
| GB2087400B (en) | 1984-05-31 |
| FI72742B (fi) | 1987-03-31 |
| YU268281A (en) | 1983-09-30 |
| AU7743881A (en) | 1982-05-20 |
| YU43049B (en) | 1989-02-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MKEX | Expiry |