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BRPI1009459A2 - método e sistema para controlar uma unidade de leito adsorvente. - Google Patents

método e sistema para controlar uma unidade de leito adsorvente.

Info

Publication number
BRPI1009459A2
BRPI1009459A2 BRPI1009459A BRPI1009459A BRPI1009459A2 BR PI1009459 A2 BRPI1009459 A2 BR PI1009459A2 BR PI1009459 A BRPI1009459 A BR PI1009459A BR PI1009459 A BRPI1009459 A BR PI1009459A BR PI1009459 A2 BRPI1009459 A2 BR PI1009459A2
Authority
BR
Brazil
Prior art keywords
controlling
adsorbent bed
bed unit
unit
adsorbent
Prior art date
Application number
BRPI1009459A
Other languages
English (en)
Inventor
Andrew C Rosinski
Mohamed Safdar Allie Baksh
Paul W Belanger
Pretti Chandra
Original Assignee
Praxair Technology Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Praxair Technology Inc filed Critical Praxair Technology Inc
Publication of BRPI1009459A2 publication Critical patent/BRPI1009459A2/pt
Publication of BRPI1009459B1 publication Critical patent/BRPI1009459B1/pt
Publication of BRPI1009459B8 publication Critical patent/BRPI1009459B8/pt

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/047Pressure swing adsorption
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • B01D53/0462Temperature swing adsorption
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/30Controlling by gas-analysis apparatus
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/56Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/102Carbon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/104Alumina
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/106Silica or silicates
    • B01D2253/108Zeolites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2256/00Main component in the product gas stream after treatment
    • B01D2256/16Hydrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/10Single element gases other than halogens
    • B01D2257/102Nitrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/50Carbon oxides
    • B01D2257/502Carbon monoxide
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/50Carbon oxides
    • B01D2257/504Carbon dioxide
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/70Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702Hydrocarbons
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/40007Controlling pressure or temperature swing adsorption
    • B01D2259/40009Controlling pressure or temperature swing adsorption using sensors or gas analysers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/40Further details for adsorption processes and devices
    • B01D2259/414Further details for adsorption processes and devices using different types of adsorbents
    • B01D2259/4141Further details for adsorption processes and devices using different types of adsorbents within a single bed
    • B01D2259/4145Further details for adsorption processes and devices using different types of adsorbents within a single bed arranged in series
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02Processes for making hydrogen or synthesis gas
    • C01B2203/0205Processes for making hydrogen or synthesis gas containing a reforming step
    • C01B2203/0227Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step
    • C01B2203/0233Processes for making hydrogen or synthesis gas containing a reforming step containing a catalytic reforming step the reforming step being a steam reforming step
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/02Processes for making hydrogen or synthesis gas
    • C01B2203/0283Processes for making hydrogen or synthesis gas containing a CO-shift step, i.e. a water gas shift step
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0485Composition of the impurity the impurity being a sulfur compound
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02CCAPTURE, STORAGE, SEQUESTRATION OR DISPOSAL OF GREENHOUSE GASES [GHG]
    • Y02C20/00Capture or disposal of greenhouse gases
    • Y02C20/40Capture or disposal of greenhouse gases of CO2
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/151Reduction of greenhouse gas [GHG] emissions, e.g. CO2

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Separation Of Gases By Adsorption (AREA)
BRPI1009459A 2009-03-25 2010-03-12 método e sistema para controlar uma unidade de leito adsorvente BRPI1009459B8 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US12/410,523 2009-03-25
US12/410,523 US8016914B2 (en) 2009-03-25 2009-03-25 Adsorption control method and controller
PCT/US2010/027089 WO2010111049A1 (en) 2009-03-25 2010-03-12 Cyclic adsorption control method and controller

Publications (3)

Publication Number Publication Date
BRPI1009459A2 true BRPI1009459A2 (pt) 2016-03-01
BRPI1009459B1 BRPI1009459B1 (pt) 2020-03-10
BRPI1009459B8 BRPI1009459B8 (pt) 2020-03-31

Family

ID=42200054

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI1009459A BRPI1009459B8 (pt) 2009-03-25 2010-03-12 método e sistema para controlar uma unidade de leito adsorvente

Country Status (6)

Country Link
US (1) US8016914B2 (pt)
EP (1) EP2411119A1 (pt)
BR (1) BRPI1009459B8 (pt)
CA (1) CA2756517C (pt)
MX (1) MX2011010063A (pt)
WO (1) WO2010111049A1 (pt)

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NL1020603C2 (nl) * 2002-05-15 2003-11-18 Tno Werkwijze voor het drogen van een product met behulp van een regeneratief adsorbens.
US8263524B1 (en) * 2009-05-11 2012-09-11 Nei, Corp. Environmentally benign sorbents for removing mercury from flue gas
AU2011211028B2 (en) * 2010-01-26 2014-11-27 Osaka Gas Co., Ltd. Combustible gas enrichment apparatus
US8551217B2 (en) 2011-01-11 2013-10-08 Praxair Technology, Inc. Six bed pressure swing adsorption process operating in normal and turndown modes
US8435328B2 (en) 2011-01-11 2013-05-07 Praxair Technology, Inc. Ten bed pressure swing adsorption process operating in normal and turndown modes
US8496733B2 (en) 2011-01-11 2013-07-30 Praxair Technology, Inc. Large scale pressure swing adsorption systems having process cycles operating in normal and turndown modes
US8491704B2 (en) 2011-01-11 2013-07-23 Praxair Technology, Inc. Six bed pressure swing adsorption process operating in normal and turndown modes
US8394171B2 (en) 2011-03-17 2013-03-12 Uop Llc Methods for controlling impurity buildup on adsorbent for pressure swing adsorption processes
JP5770040B2 (ja) * 2011-07-28 2015-08-26 愛三工業株式会社 蒸発燃料処理装置
EP2746884B1 (en) 2012-12-24 2015-04-15 Air Products And Chemicals, Inc. Apparatus and methods to monitor and control cyclic process units in a steady plant environment
US9802149B1 (en) 2015-12-16 2017-10-31 The United States Of America As Represented By The Administrator Of Nasa Sorbent-based atmosphere revitalization system
US10427090B2 (en) * 2017-10-18 2019-10-01 Praxair Technology, Inc. Control of swing adsorption process cycle time with ambient CO2 monitoring
US11442437B2 (en) * 2018-06-20 2022-09-13 Lehigh University Multivariable model predictive controller
US10850225B2 (en) * 2018-07-17 2020-12-01 Uop Llc Processes for removing heavy hydrocarbons and water from a stream of natural gas
CN112654414A (zh) * 2018-09-25 2021-04-13 积水化学工业株式会社 气体处理方法和气体处理装置
CN121068408A (zh) * 2025-11-06 2025-12-05 重庆医药高等专科学校附属第一医院 医疗实验室有毒气体分级吸附的实时监测系统

Family Cites Families (25)

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US3703068A (en) 1971-03-26 1972-11-21 Union Carbide Corp Control system for selective adsorption process
US4127395A (en) 1976-10-18 1978-11-28 Pall Corporation Adsorbent fractionator with fail-safe automatic cycle control and process
US4552570A (en) * 1980-05-02 1985-11-12 Pall Corporation Adsorbent fractionator with automatic cycle control and process
US4546442A (en) * 1982-11-24 1985-10-08 Pall Corporation Microcomputer control system for desiccant dryer
US4693730A (en) * 1986-07-24 1987-09-15 Union Carbide Corporation Pressure swing adsorption product purity control method and apparatus
US4859217A (en) 1987-06-30 1989-08-22 Uop Process for separating nitrogen from mixtures thereof with less polar substances
FR2642668B1 (fr) * 1989-02-06 1993-09-17 Trepaud Pierre Procede de regeneration d'un adsorbeur d'une installation de dessiccation d'un gaz et installation permettant de le mettre en oeuvre
US5174979A (en) 1989-10-06 1992-12-29 Uop Mixed ion-exchanged zeolites and processes for the use thereof in gas separations
US5258056A (en) 1991-09-27 1993-11-02 The Boc Group, Inc. PSA system with product turndown and purity control
US5698013A (en) 1994-03-18 1997-12-16 Uop Nitrogen-selective zeolitic adsorbent for use in air separation process
US5454857A (en) 1994-03-18 1995-10-03 Uop Air separation process
US5529607A (en) 1995-03-15 1996-06-25 The Boc Group, Inc. PSA process with dynamic purge control
US5674311A (en) 1995-10-20 1997-10-07 Praxair Technology, Inc. Adsorption process and system using multilayer adsorbent beds
US6179324B1 (en) * 1999-01-11 2001-01-30 Trw Vehicle Safety Systems Inc. Vehicle inflatable side curtain assembly
US6340382B1 (en) 1999-08-13 2002-01-22 Mohamed Safdar Allie Baksh Pressure swing adsorption process for the production of hydrogen
US6503299B2 (en) 1999-11-03 2003-01-07 Praxair Technology, Inc. Pressure swing adsorption process for the production of hydrogen
US6277174B1 (en) 2000-01-07 2001-08-21 Praxair Technology, Inc. Low pressure ratio VPSA plant tuning and balancing system
US6454838B1 (en) 2000-06-21 2002-09-24 Air Products And Chemicals, Inc. Six bed pressure swing adsorption process with four steps of pressure equalization
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FR2835932B1 (fr) 2002-02-13 2004-03-19 Air Liquide Procede de commande d'une installation de traitement d'un gaz par adsorption et installation de traitement correspondante
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Also Published As

Publication number Publication date
CA2756517A1 (en) 2010-09-30
WO2010111049A1 (en) 2010-09-30
US20100242722A1 (en) 2010-09-30
BRPI1009459B1 (pt) 2020-03-10
EP2411119A1 (en) 2012-02-01
CA2756517C (en) 2017-02-28
CN102834159A (zh) 2012-12-19
MX2011010063A (es) 2011-10-14
BRPI1009459B8 (pt) 2020-03-31
US8016914B2 (en) 2011-09-13

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Legal Events

Date Code Title Description
B06T Formal requirements before examination [chapter 6.20 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 12/03/2010, OBSERVADAS AS CONDICOES LEGAIS.

B16C Correction of notification of the grant [chapter 16.3 patent gazette]

Free format text: REF. RPI 2566 DE 10/03/2020 QUANTO AO QUADRO REIVINDICATORIO.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

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B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)

Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2662 DE 11-01-2022 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013.