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BRPI0417856A - processo para monitorar, controlar e/ou regular as reações de uma mistura de reação fluida, e para incorporar um dispositivo, e, dispositivo para executar o processo - Google Patents

processo para monitorar, controlar e/ou regular as reações de uma mistura de reação fluida, e para incorporar um dispositivo, e, dispositivo para executar o processo

Info

Publication number
BRPI0417856A
BRPI0417856A BRPI0417856-4A BRPI0417856A BRPI0417856A BR PI0417856 A BRPI0417856 A BR PI0417856A BR PI0417856 A BRPI0417856 A BR PI0417856A BR PI0417856 A BRPI0417856 A BR PI0417856A
Authority
BR
Brazil
Prior art keywords
reaction mixture
fluid reaction
reactions
monitoring
gaps
Prior art date
Application number
BRPI0417856-4A
Other languages
English (en)
Inventor
Gerhard Olbert
Claus Hechler
Dietmar Loewen
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE2003161515 external-priority patent/DE10361515A1/de
Application filed by Basf Ag filed Critical Basf Ag
Publication of BRPI0417856A publication Critical patent/BRPI0417856A/pt
Publication of BRPI0417856B1 publication Critical patent/BRPI0417856B1/pt

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/248—Reactors comprising multiple separated flow channels
    • B01J19/249—Plate-type reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/001—Controlling catalytic processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0285—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/00044—Temperature measurement
    • B01J2208/00061—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015—Plates; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00628—Controlling the composition of the reactive mixture
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00946—Features relating to the reactants or products
    • B01J2208/00955—Sampling of the particulate material, the reactants or the products
    • B01J2208/00964—Reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00946—Features relating to the reactants or products
    • B01J2208/00955—Sampling of the particulate material, the reactants or the products
    • B01J2208/00973—Products
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B01J2219/00063—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00191—Control algorithm
    • B01J2219/00193—Sensing a parameter
    • B01J2219/00195—Sensing a parameter of the reaction system
    • B01J2219/002—Sensing a parameter of the reaction system inside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2451—Geometry of the reactor
    • B01J2219/2453—Plates arranged in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2451—Geometry of the reactor
    • B01J2219/2456—Geometry of the plates
    • B01J2219/2459—Corrugated plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2461—Heat exchange aspects
    • B01J2219/2462—Heat exchange aspects the reactants being in indirect heat exchange with a non reacting heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2461—Heat exchange aspects
    • B01J2219/2462—Heat exchange aspects the reactants being in indirect heat exchange with a non reacting heat exchange medium
    • B01J2219/2464—Independent temperature control in various sections of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2476—Construction materials
    • B01J2219/2477—Construction materials of the catalysts
    • B01J2219/2481—Catalysts in granular from between plates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2476—Construction materials
    • B01J2219/2483—Construction materials of the plates
    • B01J2219/2485—Metals or alloys
    • B01J2219/2486—Steel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/245—Plate-type reactors
    • B01J2219/2491—Other constructional details
    • B01J2219/2497—Size aspects, i.e. concrete sizes are being mentioned in the classified document

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Monitoring And Testing Of Nuclear Reactors (AREA)

Abstract

"PROCESSO PARA MONITORAR, CONTROLAR E/OU REGULAR AS REAçõES DE UMA MISTURA DE REAçãO FLUIDA, E PARA INCORPORAR UM DISPOSITIVO, E, DISPOSITIVO PARA EXECUTAR O PROCESSO". é proposto um processo para monitorar, controlar e/ou regular as reações de uma mistura de reação fluida na presença de um catalisador heterogêneo em particulas em um reator que possui duas ou mais chapas térmicas (1) dispostas na vertical e paralelamente entre si, em cada caso deixando uma folga (2), o catalisador heterogêneo em partículas estando instalado nas folgas (2), e a mistura de reação fluida sendo conduzida através das folgas (2), que compreende selecionar, como um parâmetro de monitoramento, controle e/ou regulagem, uma ou mais temperaturas que são medidas em uma ou mais folgas (2), em um ou mais pontos de medição que estão distribuidos pela altura de cada folga (2).
BRPI0417856-4A 2003-12-23 2004-12-21 Processo para monitorar, controlar e/ou regular as reações de uma mistura de reação fluida, e para incorporar um dispositivo, e, dispositivo para executar o processo BRPI0417856B1 (pt)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US53167803P 2003-12-23 2003-12-23
US60/531,678 2003-12-23
DE10361515.6 2003-12-23
DE2003161515 DE10361515A1 (de) 2003-12-23 2003-12-23 Verfahren zur Überwachung, Steuerung und/oder Regelung von Reaktionen eines fluiden Reaktionsgemisches in einem Reaktor mit Thermoblechplatten
PCT/EP2004/014532 WO2005063374A1 (de) 2003-12-23 2004-12-21 Verfahren zur überwachung, steuerung und/oder regelung von reaktionen eines fluiden reaktionsgemisches in einem reaktor mit thermoblechplatten

Publications (2)

Publication Number Publication Date
BRPI0417856A true BRPI0417856A (pt) 2007-04-27
BRPI0417856B1 BRPI0417856B1 (pt) 2015-03-17

Family

ID=34740518

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI0417856-4A BRPI0417856B1 (pt) 2003-12-23 2004-12-21 Processo para monitorar, controlar e/ou regular as reações de uma mistura de reação fluida, e para incorporar um dispositivo, e, dispositivo para executar o processo

Country Status (11)

Country Link
US (1) US20050158217A1 (pt)
EP (1) EP1699550B1 (pt)
JP (1) JP4970953B2 (pt)
KR (1) KR101196082B1 (pt)
CN (1) CN100548461C (pt)
BR (1) BRPI0417856B1 (pt)
CA (1) CA2548360C (pt)
RU (1) RU2356617C2 (pt)
SG (1) SG149877A1 (pt)
WO (1) WO2005063374A1 (pt)
ZA (1) ZA200605103B (pt)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007028332A1 (de) * 2007-06-15 2008-12-18 Basf Se Verfahren zum Beschicken eines Reaktors mit einem Katalysatorfestbett, das wenigstens ringförmige Katalysatorformkörper K umfasst
DE102007061477A1 (de) 2007-12-20 2009-07-02 Man Dwe Gmbh Rohrbündelreaktor
DE102009031765B4 (de) 2009-06-25 2012-10-11 Chemieanlagenbau Chemnitz Gmbh Konverter zur Durchführung exothermer katalytischer Reaktionen
US8746605B2 (en) 2011-04-19 2014-06-10 Great Stuff, Inc. Systems and methods for spooling and unspooling linear material
FR2975922B1 (fr) 2011-06-06 2013-05-31 Arkema France Reacteur a plaques avec injection in situ
EP2594328B1 (en) * 2011-11-21 2014-08-20 ITS Reaktortechnik GmbH Process for the removal of hydrogen sulfide from a gas stream
US20140021284A1 (en) 2012-07-20 2014-01-23 Great Stuff, Inc. Reel with manually actuated retraction system
JP2018094457A (ja) 2016-12-08 2018-06-21 株式会社Ihi 反応装置
CN114062425B (zh) * 2021-10-26 2025-02-18 上海交通大学 一种流体换热试验装置

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2156463A (en) * 1984-03-22 1985-10-09 Nat Nuclear Corp Ltd Pipe junction-internal insulation
SU1328346A1 (ru) * 1986-03-03 1987-08-07 Калининское Специальное Проектно-Конструкторское Бюро Средств Управления Способ автоматического управлени процессом синтеза малеинового ангидрида
SU1741880A1 (ru) * 1989-12-26 1992-06-23 Одесский Политехнический Институт Способ контрол состо ни реактора с неподвижным слоем катализатора
SU1736600A1 (ru) * 1990-04-18 1992-05-30 Ленинградский Технологический Институт Им.Ленсовета Способ автоматического управлени температурным режимом технологического процесса в реакторе смешени
RU2071961C1 (ru) * 1994-07-07 1997-01-20 Акционерное общество открытого типа "Пигмент" Способ автоматического управления процессом приготовления растворов в реакторах полунепрерывного действия и устройство для его осуществления
DE19754185C1 (de) * 1997-12-06 1999-02-04 Deg Engineering Gmbh Reaktor für die katalytische Umsetzung von Reaktionsmedien, insbesondere von gasförmigen Reaktionsmedien
DE19952964A1 (de) * 1999-11-03 2001-05-10 Basf Ag Verfahren zur katalytischen Gasphasenoxidation zu (Meth)Acrolein und/oder (Meth)Acrylsäure
DE10000584A1 (de) * 2000-01-10 2001-07-12 Basf Ag Verfahren zur katalytischen Gasphasenoxidation zu Maleinsäureanhydrid
DE10110847A1 (de) 2001-03-07 2002-09-12 Gerhard Olbert Meßverfahren und -einrichtung zur Überwachung und Steuerung von Reaktionen in Kontaktrohrbündelreaktoren
JP4212888B2 (ja) * 2002-12-26 2009-01-21 三菱化学エンジニアリング株式会社 プレート型触媒反応器
EP1699749B1 (de) * 2003-12-23 2015-09-09 Basf Se Verfahren zur herstellung von (meth)acrolein und/oder (meth)acrylsäure durch heterogen katalysierte partialoxidation von c3 und/oder c4-vorlä uferverbindungen

Also Published As

Publication number Publication date
KR20060115754A (ko) 2006-11-09
US20050158217A1 (en) 2005-07-21
BRPI0417856B1 (pt) 2015-03-17
WO2005063374A1 (de) 2005-07-14
JP4970953B2 (ja) 2012-07-11
KR101196082B1 (ko) 2012-11-01
EP1699550A1 (de) 2006-09-13
RU2006126514A (ru) 2008-01-27
CA2548360C (en) 2015-07-07
CN1898014A (zh) 2007-01-17
CN100548461C (zh) 2009-10-14
JP2007519508A (ja) 2007-07-19
ZA200605103B (en) 2008-01-08
RU2356617C2 (ru) 2009-05-27
CA2548360A1 (en) 2005-07-14
SG149877A1 (en) 2009-02-27
EP1699550B1 (de) 2013-02-20

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Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
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