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BR9812760A - Composição detergente que contém tensoativos ramificados de cadeia intermediária e um eletrólitro para desempenho melhorado - Google Patents

Composição detergente que contém tensoativos ramificados de cadeia intermediária e um eletrólitro para desempenho melhorado

Info

Publication number
BR9812760A
BR9812760A BR9812760-8A BR9812760A BR9812760A BR 9812760 A BR9812760 A BR 9812760A BR 9812760 A BR9812760 A BR 9812760A BR 9812760 A BR9812760 A BR 9812760A
Authority
BR
Brazil
Prior art keywords
detergent composition
intermediate chain
improved performance
electrolyte
branched intermediate
Prior art date
Application number
BR9812760-8A
Other languages
English (en)
Other versions
BR9812760B1 (pt
Inventor
Frank Andrez Kvietok
Gabor Heltovics
Rinko Katsuda
Phillip Kyle Vinson
Robert Allen Godfroid
Original Assignee
Procter & Gamble
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter & Gamble filed Critical Procter & Gamble
Publication of BR9812760A publication Critical patent/BR9812760A/pt
Publication of BR9812760B1 publication Critical patent/BR9812760B1/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/046—Salts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/37—Mixtures of compounds all of which are anionic
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/65—Mixtures of anionic with cationic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/83—Mixtures of non-ionic with anionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/86—Mixtures of anionic, cationic, and non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/04—Carboxylic acids or salts thereof
    • C11D1/06—Ether- or thioether carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/123—Sulfonic acids or sulfuric acid esters; Salts thereof derived from carboxylic acids, e.g. sulfosuccinates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/16—Sulfonic acids or sulfuric acid esters; Salts thereof derived from divalent or polyvalent alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/18—Sulfonic acids or sulfuric acid esters; Salts thereof derived from amino alcohols
    • C11D1/20—Fatty acid condensates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/22—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aromatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/28—Sulfonation products derived from fatty acids or their derivatives, e.g. esters, amides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/29—Sulfates of polyoxyalkylene ethers
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/34—Derivatives of acids of phosphorus
    • C11D1/345—Phosphates or phosphites
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/52—Carboxylic amides, alkylolamides or imides or their condensation products with alkylene oxides
    • C11D1/525—Carboxylic amides (R1-CO-NR2R3), where R1, R2 or R3 contain two or more hydroxy groups per alkyl group, e.g. R3 being a reducing sugar rest
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38—Cationic compounds
    • C11D1/62—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/667—Neutral esters, e.g. sorbitan esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/75—Amino oxides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/90—Betaines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Cosmetics (AREA)

Abstract

Patente de Invenção: <B>"COMPOSIçãO DETERGENTE QUE CONTéM TENSOATIVOS RAMIFICADOS DE CADEIA INTERMEDIáRIA E UM ELETRóLITRO PARA DESEMPENHO MELHORADO"<D>. é divulgada uma composição detergente que contém uma mistura de tensoativo alquilbenzeno sulfonato linear e tensoativo ramificado de cadeia intermediária e um eletrolito. A composição detergente inclui um tensoativo alquil sulfato primário ramificado de cadeia intermediária e um eletrolito capaz de aumentar a resistência iónica das composições resultando em desempenho melhorado, especialmente sob as condições de lavagem à baixa temperatura da água. Os eletrolitos típicos incluem cloreto de sódio, sulfato de magnésio, carbonato de cálcio e similares.
BRPI9812760-8A 1997-10-10 1998-10-09 composiÇço detergente que compreende tensoativos ramificados de cadeia intermediÁria e eletràlitro para desempenho melhorado, e processo para lavar tecidos sujos. BR9812760B1 (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US6187997P 1997-10-10 1997-10-10
PCT/US1998/021359 WO1999019430A1 (en) 1997-10-10 1998-10-09 Detergent composition containing mid-chain branched surfactants and an electrolyte for improved performance

Publications (2)

Publication Number Publication Date
BR9812760A true BR9812760A (pt) 2000-08-29
BR9812760B1 BR9812760B1 (pt) 2008-11-18

Family

ID=22038729

Family Applications (1)

Application Number Title Priority Date Filing Date
BRPI9812760-8A BR9812760B1 (pt) 1997-10-10 1998-10-09 composiÇço detergente que compreende tensoativos ramificados de cadeia intermediÁria e eletràlitro para desempenho melhorado, e processo para lavar tecidos sujos.

Country Status (13)

Country Link
US (1) US6232282B1 (pt)
EP (1) EP1032624A1 (pt)
JP (1) JP2001520258A (pt)
KR (1) KR100404818B1 (pt)
CN (1) CN1179027C (pt)
AU (1) AU740980B2 (pt)
BR (1) BR9812760B1 (pt)
CA (1) CA2305327C (pt)
HU (1) HUP0003925A3 (pt)
MA (1) MA24673A1 (pt)
TR (1) TR200000938T2 (pt)
WO (1) WO1999019430A1 (pt)
ZA (1) ZA989157B (pt)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1253547C (zh) 1999-07-16 2006-04-26 宝洁公司 包含两性离子型聚胺和中链支链表面活性剂的洗衣用洗涤剂组合物
US6677289B1 (en) * 1999-07-16 2004-01-13 The Procter & Gamble Company Laundry detergent compositions comprising polyamines and mid-chain branched surfactants
US6696401B1 (en) * 1999-11-09 2004-02-24 The Procter & Gamble Company Laundry detergent compositions comprising zwitterionic polyamines
US6797685B2 (en) * 2002-04-26 2004-09-28 Unilever Home & Personal Care Usa, Division Of Conopco, Inc. Liquid laundry detergent with emulsion layer
WO2004020563A1 (en) * 2002-08-30 2004-03-11 The Procter & Gamble Company Detergent compositions comprising hydrophobically modified polyamines
MX265444B (es) * 2002-09-12 2009-03-26 Procter & Gamble Sistemas polimericas y composiciones limpiadoras que los comprenden.
CN1894307A (zh) * 2003-12-19 2007-01-10 宝洁公司 疏水多胺乙氧基化物
US8318654B2 (en) * 2006-11-30 2012-11-27 Kimberly-Clark Worldwide, Inc. Cleansing composition incorporating a biocide, heating agent and thermochromic substance
DE102007028310A1 (de) * 2007-06-20 2008-12-24 Clariant International Ltd. Tensidmischungen mit synergistischen Eigenschaften
MY155216A (en) * 2008-05-23 2015-09-30 Colgate Palmolive Co Liquid cleaning compositions and manufacture
JP5700469B2 (ja) * 2012-12-28 2015-04-15 花王株式会社 衣料用粉末洗剤組成物
CN105358667B (zh) * 2013-07-11 2018-02-06 宝洁公司 衣物洗涤剂组合物
CN105358668A (zh) * 2013-07-11 2016-02-24 宝洁公司 衣物洗涤剂组合物
PL3039110T3 (pl) 2013-08-26 2018-01-31 Procter & Gamble Kompozycje zawierające alkoksylowane polialkilenoiminy charakteryzujące się niskimi temperaturami topnienia
JP6607715B2 (ja) * 2015-07-03 2019-11-20 ライオン株式会社 液体洗浄剤
BR112018073596A2 (pt) * 2016-05-16 2019-02-26 Unilever Nv composição aquosa para remoção de manchas, produto embalado, uso de uma composição e método de clareamento de manchas em tecidos
EP3538108A4 (en) 2016-11-10 2020-06-17 Oyagen, Inc. METHODS OF TREATING AND INHIBITING EBOLA VIRUS INFECTION
WO2020089812A1 (en) * 2018-11-02 2020-05-07 Johnson & Johnson Consumer Inc. Foamable solid cleanser
WO2021158248A1 (en) 2020-02-04 2021-08-12 Oyagen, Inc. Method for treating coronavirus infections

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA1044983A (en) * 1974-03-21 1978-12-26 The Procter And Gamble Company Liquid detergent compositions
US4137197A (en) * 1977-11-10 1979-01-30 Lever Brothers Company Powdered detergent compositions containing a calcium salt of an anionic surfactant
GB9001404D0 (en) * 1990-01-22 1990-03-21 Unilever Plc Detergent composition
US5707948A (en) * 1993-03-19 1998-01-13 The Procter & Gamble Company Stable and clear concentrated cleaning compositions comprising at least one short chain surfactant
CN1065563C (zh) * 1993-05-20 2001-05-09 普罗格特-甘布尔公司 用于手洗或其它低水洗涤体系的包括n－酰基己内酰胺的漂白组合物
US5562866A (en) * 1995-06-20 1996-10-08 Albemarle Corporation Formulated branched chain alcohol ether sulfate compounds
PH11997056158B1 (en) * 1996-04-16 2001-10-15 Procter & Gamble Mid-chain branched primary alkyl sulphates as surfactants
MA24137A1 (fr) * 1996-04-16 1997-12-31 Procter & Gamble Fabrication d'agents de surface ramifies .
EG21623A (en) * 1996-04-16 2001-12-31 Procter & Gamble Mid-chain branced surfactants
EG22088A (en) * 1996-04-16 2002-07-31 Procter & Gamble Alkoxylated sulfates
US6093856A (en) * 1996-11-26 2000-07-25 The Procter & Gamble Company Polyoxyalkylene surfactants

Also Published As

Publication number Publication date
AU9796098A (en) 1999-05-03
MA24673A1 (fr) 1999-07-01
CN1281496A (zh) 2001-01-24
EP1032624A1 (en) 2000-09-06
BR9812760B1 (pt) 2008-11-18
HUP0003925A3 (en) 2001-12-28
CA2305327A1 (en) 1999-04-22
US6232282B1 (en) 2001-05-15
CN1179027C (zh) 2004-12-08
CA2305327C (en) 2003-07-29
WO1999019430A1 (en) 1999-04-22
AU740980B2 (en) 2001-11-15
TR200000938T2 (tr) 2000-08-21
JP2001520258A (ja) 2001-10-30
ZA989157B (en) 1999-04-12
KR100404818B1 (ko) 2003-11-07
KR20010015735A (ko) 2001-02-26
HUP0003925A2 (hu) 2001-04-28

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 16/12/2008, OBSERVADAS AS CONDICOES LEGAIS.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time
B24J Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12)