BR9810181A - Processo para preparação de uma solução aquosa de hidroxilamina de alta pureza - Google Patents
Processo para preparação de uma solução aquosa de hidroxilamina de alta purezaInfo
- Publication number
- BR9810181A BR9810181A BR9810181-1A BR9810181A BR9810181A BR 9810181 A BR9810181 A BR 9810181A BR 9810181 A BR9810181 A BR 9810181A BR 9810181 A BR9810181 A BR 9810181A
- Authority
- BR
- Brazil
- Prior art keywords
- hydroxylamine
- preparing
- aqueous hydroxylamine
- hydroxylamine solution
- purity
- Prior art date
Links
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 title abstract 8
- 238000004519 manufacturing process Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 238000011031 large-scale manufacturing process Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1481—Purification
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1445—Preparation of hydoxylamine from its salts
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1463—Concentration
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
Abstract
"PROCESSO PARA PREPARAçãO DE UMA SOLUçãO AQUOSA DE HIDROXILAMINA DE ALTA PUREZA" A invenção refere-se a um método para a produção de soluções aquosas de hidroxilamina de alta pureza, a partir de hidroxilamina livre, onde a solução aquosa diluída de hidroxilamina é concentrada em uma coluna, o vapor que contem a hidroxilamina é removido do fundo da coluna através de um fluxo lateral, e a hidroxilamina de alta pureza é produzida por condensação desses vapores. O processo é simples e suave, pode ser utilizado em produções de larga escala, e produz hidroxilamina "grau eletrónico".
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19725851A DE19725851A1 (de) | 1997-06-18 | 1997-06-18 | Verfahren zur Herstellung hochreiner, wässriger Hydroxylaminlösungen |
| PCT/EP1998/003714 WO1998057886A1 (de) | 1997-06-18 | 1998-06-18 | Verfahren zur herstellung hochreiner, wässriger hydroxylaminlösungen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR9810181A true BR9810181A (pt) | 2000-08-08 |
Family
ID=7832900
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR9810181-1A BR9810181A (pt) | 1997-06-18 | 1998-06-18 | Processo para preparação de uma solução aquosa de hidroxilamina de alta pureza |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US6153799A (pt) |
| EP (1) | EP0989952B1 (pt) |
| JP (1) | JP4183286B2 (pt) |
| KR (1) | KR100494065B1 (pt) |
| CN (1) | CN1113036C (pt) |
| AU (1) | AU8439098A (pt) |
| BR (1) | BR9810181A (pt) |
| CA (1) | CA2293319C (pt) |
| DE (2) | DE19725851A1 (pt) |
| ES (1) | ES2164445T3 (pt) |
| MY (1) | MY118793A (pt) |
| TW (1) | TW383296B (pt) |
| WO (1) | WO1998057886A1 (pt) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19936594A1 (de) | 1999-08-04 | 2001-02-08 | Basf Ag | Verfahren zur Herstellung von hochreinen stabilisierten Hydroxylaminlösungen |
| DE10004818A1 (de) * | 2000-02-04 | 2001-08-09 | Basf Ag | Verfahren zum Recycling hydroxylaminhaltiger Stripperlösungen |
| JP3503115B2 (ja) * | 2000-06-27 | 2004-03-02 | 東レ・ファインケミカル株式会社 | フリーヒドロキシルアミン水溶液の製造方法 |
| DE10131787A1 (de) * | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
| DE10131788A1 (de) * | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
| DE10134389A1 (de) | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
| EP1663862A2 (en) | 2003-08-13 | 2006-06-07 | Showa Denko K.K. | Process for producing hydroxylamine |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE621960A (pt) * | 1961-08-31 | |||
| US4147623A (en) * | 1977-10-28 | 1979-04-03 | Allied Chemical Corporation | Hydroxylamine purification via ion exclusion |
| US4202765A (en) * | 1977-10-28 | 1980-05-13 | Allied Chemical Corporation | Hydroxylamine purification via cation exchange |
| EP0108294B1 (en) * | 1982-11-01 | 1991-02-06 | AlliedSignal Inc. | Preparation from hydroxylammonium sulfate of alcoholic hydroxylamine solutions and of oximes, hydroxamic acids and other hydroxylammonium salts via alcoholic hydroxylamine solutions |
| US4956168A (en) * | 1983-01-28 | 1990-09-11 | The United States Of America As Represented By The Secretary Of The Navy | Synthesis of hydroxylamine salts |
| DE3347259A1 (de) * | 1983-12-28 | 1985-07-11 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von waessrigen hydroxylaminloesungen |
| DE3528463A1 (de) * | 1985-08-08 | 1987-02-19 | Basf Ag | Verfahren zur herstellung von waessrigen loesungen von freiem hydroxylamin |
| DE3601803A1 (de) * | 1986-01-22 | 1987-07-23 | Basf Ag | Verfahren zur herstellung von waessrigen loesungen von freiem hydroxylamin |
| DE3608495A1 (de) * | 1986-03-14 | 1987-09-17 | Basf Ag | Verfahren zur herstellung von waessrigen loesungen von hydroxylamin |
| US5266290A (en) * | 1992-07-10 | 1993-11-30 | Thiokol Corporation | Process for making high purity hydroxylammonium nitrate |
| US5510097A (en) * | 1994-05-19 | 1996-04-23 | Olin Corporation | Hydroxylammonium nitrate free of ammonium nitrate |
| US5837107A (en) * | 1995-12-20 | 1998-11-17 | Basf Aktiengesellschaft | Process for production of aqueous solutions of free hydroxylamine |
| HRP960601B1 (en) * | 1995-12-20 | 2001-12-31 | Basf Ag | Process for separating medium boiling substances from a mixture of low, medium and high boiling substances |
-
1997
- 1997-06-18 DE DE19725851A patent/DE19725851A1/de not_active Withdrawn
-
1998
- 1998-06-16 TW TW087109527A patent/TW383296B/zh not_active IP Right Cessation
- 1998-06-18 CA CA002293319A patent/CA2293319C/en not_active Expired - Fee Related
- 1998-06-18 DE DE59801534T patent/DE59801534D1/de not_active Expired - Lifetime
- 1998-06-18 ES ES98934975T patent/ES2164445T3/es not_active Expired - Lifetime
- 1998-06-18 CN CN98806279A patent/CN1113036C/zh not_active Expired - Fee Related
- 1998-06-18 BR BR9810181-1A patent/BR9810181A/pt not_active IP Right Cessation
- 1998-06-18 WO PCT/EP1998/003714 patent/WO1998057886A1/de not_active Ceased
- 1998-06-18 AU AU84390/98A patent/AU8439098A/en not_active Abandoned
- 1998-06-18 EP EP98934975A patent/EP0989952B1/de not_active Expired - Lifetime
- 1998-06-18 KR KR10-1999-7011936A patent/KR100494065B1/ko not_active Expired - Fee Related
- 1998-06-18 MY MYPI98002744A patent/MY118793A/en unknown
- 1998-06-18 US US09/445,186 patent/US6153799A/en not_active Expired - Fee Related
- 1998-06-18 JP JP50376799A patent/JP4183286B2/ja not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| ES2164445T3 (es) | 2002-02-16 |
| EP0989952A1 (de) | 2000-04-05 |
| EP0989952B1 (de) | 2001-09-19 |
| JP2002504062A (ja) | 2002-02-05 |
| CN1113036C (zh) | 2003-07-02 |
| CA2293319C (en) | 2008-11-25 |
| DE19725851A1 (de) | 1998-12-24 |
| AU8439098A (en) | 1999-01-04 |
| TW383296B (en) | 2000-03-01 |
| KR20010013914A (ko) | 2001-02-26 |
| CA2293319A1 (en) | 1998-12-23 |
| KR100494065B1 (ko) | 2005-06-10 |
| DE59801534D1 (de) | 2001-10-25 |
| US6153799A (en) | 2000-11-28 |
| CN1260762A (zh) | 2000-07-19 |
| JP4183286B2 (ja) | 2008-11-19 |
| WO1998057886A1 (de) | 1998-12-23 |
| MY118793A (en) | 2005-01-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B06A | Notification to applicant to reply to the report for non-patentability or inadequacy of the application [chapter 6.1 patent gazette] | ||
| B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
| B16A | Patent or certificate of addition of invention granted |
Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 18/06/1998, OBSERVADAS AS CONDICOES LEGAIS. |
|
| B24H | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi) | ||
| B24F | Patent annual fee: publication cancelled |
Free format text: ANULADA A PUBLICACAO CODIGO 24.8 NA RPI NO 2257 DE 08/04/2014 POR TER SIDO INDEVIDA. |
|
| B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE AS 14A, 15A, 16A, 17A, 18A, 19A E 20A ANUIDADES. |
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| B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2606 DE 15-12-2020 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |