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BR9710947A - Partìcula de fornecimento deagente de lavanderia, composição de detergentegranular e processo para a produção dapartìcula de lavanderia - Google Patents

Partìcula de fornecimento deagente de lavanderia, composição de detergentegranular e processo para a produção dapartìcula de lavanderia

Info

Publication number
BR9710947A
BR9710947A BR9710947-9A BR9710947A BR9710947A BR 9710947 A BR9710947 A BR 9710947A BR 9710947 A BR9710947 A BR 9710947A BR 9710947 A BR9710947 A BR 9710947A
Authority
BR
Brazil
Prior art keywords
laundry
particle
porous
release inhibitor
production
Prior art date
Application number
BR9710947-9A
Other languages
English (en)
Inventor
Lois Sara Gallon
Janet Sue Littig
Original Assignee
Procter & Gamble
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Procter & Gamble filed Critical Procter & Gamble
Publication of BR9710947A publication Critical patent/BR9710947A/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes
    • C11D3/502—Protected perfumes
    • C11D3/505—Protected perfumes encapsulated or adsorbed on a carrier, e.g. zeolite or clay
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0034—Fixed on a solid conventional detergent ingredient
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/12—Water-insoluble compounds
    • C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246—Silicates, e.g. diatomaceous earth
    • C11D3/128—Aluminium silicates, e.g. zeolites

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Detergent Compositions (AREA)
  • Fats And Perfumes (AREA)

Abstract

Patente de Invenção: "PARTìCULA DE FORNECIMENTO DEAGENTE DE LAVANDERIA, COMPOSIçãO DE DETERGENTEGRANULAR E PROCESSO PARA A PRODUçãO DAPARTìCULA DE LAVANDERIA". São providas uma partícula defornecimento de agente de lavanderia e composições granularesincluindo a partícula. A partícula compreende um veículo porososelecionada do grupo que consiste de zeólito X, zeólito Y e suasmisturas com o veículo poroso incluindo numerosas aberturas deporo. O inibidor de liberação de lavanderia é então incorporado noveículo poroso de modo que a área seção transversal do inibidorde liberação é maior do que a área de seção transversal dasaberturas de poro do veículo poroso. O inibidor de liberação delavanderia inclui o resíduo de um agente fornecível tal como umcomponente de perfume. O agente fornecível é então aprisionadono veículo poroso até que o inibidor de liberação seja hidrolisado,desse modo liberando o agente fornecível e o permitindo-lheescapar do veículo poroso.
BR9710947-9A 1996-03-22 1997-03-05 Partìcula de fornecimento deagente de lavanderia, composição de detergentegranular e processo para a produção dapartìcula de lavanderia BR9710947A (pt)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US1394896P 1996-03-22 1996-03-22
PCT/US1997/003283 WO1997034981A1 (en) 1996-03-22 1997-03-05 Delivery system having release inhibitor loaded zeolite and method for making same

Publications (1)

Publication Number Publication Date
BR9710947A true BR9710947A (pt) 2001-11-27

Family

ID=21762669

Family Applications (1)

Application Number Title Priority Date Filing Date
BR9710947-9A BR9710947A (pt) 1996-03-22 1997-03-05 Partìcula de fornecimento deagente de lavanderia, composição de detergentegranular e processo para a produção dapartìcula de lavanderia

Country Status (13)

Country Link
US (1) US6245732B1 (pt)
EP (1) EP0888431B1 (pt)
JP (1) JP3378014B2 (pt)
CN (1) CN1130451C (pt)
AR (1) AR006348A1 (pt)
AT (1) ATE259410T1 (pt)
AU (1) AU2063697A (pt)
BR (1) BR9710947A (pt)
CA (1) CA2249291A1 (pt)
DE (1) DE69727557T2 (pt)
ES (1) ES2216129T3 (pt)
WO (1) WO1997034981A1 (pt)
ZA (1) ZA972143B (pt)

Families Citing this family (72)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0971024A1 (en) * 1998-07-10 2000-01-12 The Procter & Gamble Company Laundry and cleaning compositions
AU3627200A (en) * 1999-03-15 2000-10-04 Procter & Gamble Company, The Perfume compositions and methods to mask amine malodors
EP1190725A3 (en) * 2000-09-25 2003-01-29 Givaudan SA Process for maintaining fragrance perception in the presence of an absorbent material
US6531444B1 (en) 2000-11-09 2003-03-11 Salvona, Llc Controlled delivery system for fabric care products
US20030045446A1 (en) * 2001-02-12 2003-03-06 Dihora Jiten Odhavji Delivery system having encapsulated porous carrier loaded with additives
WO2002090480A1 (en) 2001-05-04 2002-11-14 The Procter & Gamble Company Dryer-added fabric softening articles and methods
WO2002090481A1 (en) * 2001-05-04 2002-11-14 The Procter & Gamble Company Compositions and articles for effective deposition of perfume
ATE528386T1 (de) 2001-05-14 2011-10-15 Procter & Gamble Reinigungsmittel
WO2003018499A2 (de) * 2001-08-22 2003-03-06 Schott Glas Antimikrobielles glaspulver und dessen verwendung
DE10141117A1 (de) * 2001-08-22 2003-03-13 Schott Glas Antimikrobielles Silicatglas und dessen Verwendung
DE10141230A1 (de) 2001-08-22 2003-03-13 Schott Glas Farbzusatz umfassend ein Glas mit antimikrobieller Wirkung
WO2003018496A1 (de) * 2001-08-22 2003-03-06 Schott Glas Antimikrobielles, entzündungshemmendes, wundheilendes glaspulver und dessen verwendung
US7166549B2 (en) * 2001-08-22 2007-01-23 Schott Ag Antimicrobial, anti-inflammatory, wound-healing and disinfecting glass and use thereof
ES2318042T3 (es) 2001-09-06 2009-05-01 THE PROCTER & GAMBLE COMPANY Velas perfumadas.
US20030084914A1 (en) * 2001-11-08 2003-05-08 L'oreal Cosmetic articles having encapsulated liquid and method of making same
US7053034B2 (en) 2002-04-10 2006-05-30 Salvona, Llc Targeted controlled delivery compositions activated by changes in pH or salt concentration
US6924259B2 (en) * 2002-04-17 2005-08-02 National Starch And Chemical Investment Holding Corporation Amine copolymers for textile and fabric protection
DE60228702D1 (de) * 2002-08-07 2008-10-16 Procter & Gamble Waschmittelzusammensetzung
AU2003267295A1 (en) * 2002-10-09 2004-05-04 The Procter And Gamble Company Process for making water-soluble pouches
US7670627B2 (en) 2002-12-09 2010-03-02 Salvona Ip Llc pH triggered targeted controlled release systems for the delivery of pharmaceutical active ingredients
US7153438B2 (en) * 2003-02-21 2006-12-26 Pur Water Purification Products, Inc. Water treatment compositions with masking agent
WO2004076371A2 (de) 2003-02-25 2004-09-10 Schott Ag Antimikrobiell wirkendes phosphatglas
US20060142413A1 (en) * 2003-02-25 2006-06-29 Jose Zimmer Antimicrobial active borosilicate glass
EP1471137B1 (en) * 2003-04-23 2013-08-07 The Procter & Gamble Company A composition comprising a surface deposition enhacing cationic polymer
US20050003975A1 (en) * 2003-06-18 2005-01-06 Browne Yvonne Bridget Blooming soap bars
DE10345625A1 (de) * 2003-09-29 2005-04-28 Schott Ag Herstellungsverfahren eines Glaspulvers oder Glasproduktes mit antimikrobieller Wirkung
US7234648B2 (en) * 2003-10-31 2007-06-26 The Procter And Gamble Company Volatile substance-controlling composition
ATE342338T1 (de) * 2004-06-04 2006-11-15 Procter & Gamble Verkapselte partikel
EP1632558A1 (en) * 2004-09-06 2006-03-08 The Procter & Gamble A composition comprising a surface deposition enhancing cationic polymer
EP1661978B1 (en) * 2004-11-29 2011-03-02 The Procter & Gamble Company Detergent compositions
EP1661977A1 (en) * 2004-11-29 2006-05-31 The Procter & Gamble Company Detergent compositions
DE102005043188A1 (de) * 2005-09-09 2007-03-22 Henkel Kgaa Verbrauchsprodukte mit wechselnden Geruchsbildern
US7691400B2 (en) * 2006-05-05 2010-04-06 Medtronic Vascular, Inc. Medical device having coating with zeolite drug reservoirs
US20070275866A1 (en) * 2006-05-23 2007-11-29 Robert Richard Dykstra Perfume delivery systems for consumer goods
ATE491433T1 (de) * 2006-08-01 2011-01-15 Procter & Gamble Pflegemittel mit freisetzungspartikel
CA2675259A1 (en) * 2007-02-09 2008-08-21 The Procter & Gamble Company Perfume systems
US9357747B1 (en) * 2007-08-17 2016-06-07 Ourpet's Company Switchgrass cat litter
EP2362765B1 (en) * 2008-12-01 2020-04-08 The Procter and Gamble Company Perfume systems
US8754028B2 (en) * 2008-12-16 2014-06-17 The Procter & Gamble Company Perfume systems
EP2270124A1 (en) * 2009-06-30 2011-01-05 The Procter & Gamble Company Bleaching compositions comprising a perfume delivery system
US8288332B2 (en) 2009-07-30 2012-10-16 The Procter & Gamble Company Fabric care conditioning composition in the form of an article
US8367596B2 (en) * 2009-07-30 2013-02-05 The Procter & Gamble Company Laundry detergent compositions in the form of an article
US8309505B2 (en) * 2009-07-30 2012-11-13 The Procter & Gamble Company Hand dish composition in the form of an article
EP3434764A3 (en) 2009-12-09 2019-04-03 The Procter & Gamble Company Fabric and home care products
WO2011084463A1 (en) 2009-12-17 2011-07-14 The Procter & Gamble Company Freshening compositions comprising malodor binding polymers and malodor control components
BR112012014842A8 (pt) 2009-12-18 2017-10-03 Procter & Gamble Perfumes e encapsulados de perfume
WO2011133306A1 (en) * 2010-04-19 2011-10-27 The Procter & Gamble Company Detergent composition
IN2015DN00239A (pt) 2010-06-22 2015-06-12 Procter & Gamble
WO2011163325A1 (en) 2010-06-22 2011-12-29 The Procter & Gamble Company Perfume systems
BR112013000099A2 (pt) 2010-07-02 2016-05-17 Procter & Gamble filamentos compreendendo mantas de não tecido com agente ativo de não perfume e métodos de fabricação dos mesmos
JP5759544B2 (ja) 2010-07-02 2015-08-05 ザ プロクター アンド ギャンブルカンパニー 活性剤を送達する方法
ES2560218T3 (es) 2010-07-02 2016-02-17 The Procter & Gamble Company Proceso para fabricar películas a partir de bandas de material no tejido
MX345025B (es) 2010-07-02 2017-01-12 Procter & Gamble Producto detergente.
RU2541949C2 (ru) 2010-07-02 2015-02-20 Дзе Проктер Энд Гэмбл Компани Филаменты, содержащие активный агент, нетканые полотна и способы их получения
DE102010051226A1 (de) 2010-11-12 2012-05-31 Dental Care Innovation Gmbh Ausspültablete mit abrasiven Bestandteilen
MX336357B (es) 2011-06-23 2016-01-14 Procter & Gamble Sistemas de perfume.
US20140141126A1 (en) 2011-06-29 2014-05-22 Solae Llc Baked food compositions comprising soy whey proteins that have been isolated from processing streams
EP2800803A1 (en) 2012-01-04 2014-11-12 The Procter and Gamble Company Active containing fibrous structures with multiple regions
US12440083B2 (en) 2012-01-04 2025-10-14 The Procter & Gamble Company Fibrous structures comprising particles and methods for making same
US10694917B2 (en) 2012-01-04 2020-06-30 The Procter & Gamble Company Fibrous structures comprising particles and methods for making same
RU2605065C2 (ru) 2012-01-04 2016-12-20 Дзе Проктер Энд Гэмбл Компани Волокнистые структуры, содержащие частицы.
CA2860647C (en) 2012-01-04 2022-06-14 The Procter & Gamble Company Active containing fibrous structures with multiple regions having differing densities
WO2015088826A1 (en) 2013-12-09 2015-06-18 The Procter & Gamble Company Fibrous structures including an active agent and having a graphic printed thereon
CN109923197B (zh) 2016-11-03 2021-03-12 荷兰联合利华有限公司 包含香料和二氧化硅微粒的洗衣处理组合物
US11697905B2 (en) 2017-01-27 2023-07-11 The Procter & Gamble Company Active agent-containing articles that exhibit consumer acceptable article in-use properties
CN110177600B (zh) 2017-01-27 2023-01-13 宝洁公司 表现出消费者可接受的制品应用特性的含活性剂的制品
US11697906B2 (en) 2017-01-27 2023-07-11 The Procter & Gamble Company Active agent-containing articles and product-shipping assemblies for containing the same
US11697904B2 (en) 2017-01-27 2023-07-11 The Procter & Gamble Company Active agent-containing articles that exhibit consumer acceptable article in-use properties
KR102575843B1 (ko) 2017-02-02 2023-09-08 워어터 피이크, 인코포레이티드 치아 세정을 위한 연마제를 포함하는 정제
WO2021113568A1 (en) 2019-12-05 2021-06-10 The Procter & Gamble Company Method of making a cleaning composition
US12122981B2 (en) 2019-12-05 2024-10-22 The Procter & Gamble Company Cleaning composition
TWI856576B (zh) * 2023-03-23 2024-09-21 國立聯合大學 金屬希夫鹼電極材料及其製備方法

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3576760A (en) 1969-06-13 1971-04-27 Nat Patent Dev Corp Water soluble entrapping
US4096072A (en) 1976-02-09 1978-06-20 The Procter & Gamble Company Fabric conditioning compositions
US4209417A (en) 1976-08-13 1980-06-24 The Procter & Gamble Company Perfumed particles and detergent composition containing same
GB1587122A (en) 1976-10-29 1981-04-01 Procter & Gamble Ltd Fabric conditioning compositions
US4304675A (en) 1979-12-26 1981-12-08 Sterling Drug Inc. Antistatic zeolite composition and method for deodorizing rugs and rooms
DE3016170A1 (de) 1980-04-26 1981-10-29 Bayer Ag, 5090 Leverkusen Mikrokapseln mit definierter oeffnungstemperatur, verfahren zu deren herstellung sowie deren verwendung
US4339356A (en) 1980-12-31 1982-07-13 The Procter & Gamble Company Heavily perfumed particles
US4440663A (en) * 1981-09-14 1984-04-03 The Procter & Gamble Company Alkaline aqueous liquid detergent compositions containing normally unstable ester perfumes
US4539135A (en) 1983-06-01 1985-09-03 Colgate Palmolive Co. Perfume-containing carrier for laundry compositions
GB8329880D0 (en) 1983-11-09 1983-12-14 Unilever Plc Particulate adjuncts
US5008437A (en) 1987-12-18 1991-04-16 International Flavors & Fragrances Inc. Schiff base reaction product of ethyl vanillin and methyl anthranilate and organoleptic uses thereof
US4806363A (en) 1988-03-22 1989-02-21 International Flavors & Fragrances Inc. Flavoring with schif base reaction products of alkyl anthranilates
JPH0633438B2 (ja) 1988-04-06 1994-05-02 花王株式会社 粉末洗浄剤組成物
US4973422A (en) * 1989-01-17 1990-11-27 The Procter & Gamble Company Perfume particles for use in cleaning and conditioning compositions
US5094761A (en) 1989-04-12 1992-03-10 The Procter & Gamble Company Treatment of fabric with perfume/cyclodextrin complexes
US5137646A (en) * 1989-05-11 1992-08-11 The Procter & Gamble Company Coated perfume particles in fabric softener or antistatic agents
US5066419A (en) 1990-02-20 1991-11-19 The Procter & Gamble Company Coated perfume particles
JPH04218583A (ja) 1990-06-15 1992-08-10 Shoko Kagaku Kenkyusho:Kk 温感性徐放材
EP0466235B1 (en) * 1990-07-11 1997-02-05 Quest International B.V. Process for preparing perfumed detergent products
GB9120952D0 (en) 1991-10-02 1991-11-13 Unilever Plc Perfume particles
GB9120951D0 (en) 1991-10-02 1991-11-13 Unilever Plc Perfume particles
TR28670A (tr) * 1993-06-02 1996-12-17 Procter & Gamble Zeolitleri iceren parfüm birakma sistemi.
EP0851910B1 (en) * 1995-09-18 2003-06-04 The Procter & Gamble Company High efficiency delivery system comprising zeolites
US5656584A (en) * 1996-02-06 1997-08-12 The Procter & Gamble Company Process for producing a particulate laundry additive composition for perfume delivery
US5648328A (en) * 1996-02-06 1997-07-15 The Procter & Gamble Company Process for producing a particulate laundry additive composition for perfume delivery
US5804538A (en) * 1996-06-20 1998-09-08 The Procter & Gamble Company Perfume delivery systems in liquid personal cleansing compositions
US5843875A (en) * 1996-06-20 1998-12-01 The Procter & Gamble Company Perfume delivery systems in liquid personal cleansing
US5858959A (en) * 1997-02-28 1999-01-12 Procter & Gamble Company Delivery systems comprising zeolites and a starch hydrolysate glass

Also Published As

Publication number Publication date
US6245732B1 (en) 2001-06-12
EP0888431B1 (en) 2004-02-11
JPH11506164A (ja) 1999-06-02
ATE259410T1 (de) 2004-02-15
EP0888431A1 (en) 1999-01-07
ZA972143B (en) 1997-09-17
CN1219957A (zh) 1999-06-16
DE69727557T2 (de) 2004-12-23
CN1130451C (zh) 2003-12-10
WO1997034981A1 (en) 1997-09-25
DE69727557D1 (de) 2004-03-18
JP3378014B2 (ja) 2003-02-17
AR006348A1 (es) 1999-08-25
ES2216129T3 (es) 2004-10-16
CA2249291A1 (en) 1997-09-25
AU2063697A (en) 1997-10-10

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Legal Events

Date Code Title Description
B06A Patent application procedure suspended [chapter 6.1 patent gazette]
B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 05/03/1997, OBSERVADAS AS CONDICOES LEGAIS.

B24C Patent annual fee: request for for restoration

Free format text: REFERENTE A 11A E 12A ANUIDADES.

B21F Lapse acc. art. 78, item iv - on non-payment of the annual fees in time

Free format text: REFERENTE AO DESPACHO 24.3 PUBLICADO NA RPI 2002 DE 19/05/2009.