BR9307589A - Processo para a preparação de substncias celulósicas de viscose - Google Patents
Processo para a preparação de substncias celulósicas de viscoseInfo
- Publication number
- BR9307589A BR9307589A BR9307589-8A BR9307589A BR9307589A BR 9307589 A BR9307589 A BR 9307589A BR 9307589 A BR9307589 A BR 9307589A BR 9307589 A BR9307589 A BR 9307589A
- Authority
- BR
- Brazil
- Prior art keywords
- liquor
- boiler
- preparation
- substance
- viscose
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 6
- 239000000126 substance Substances 0.000 title abstract 6
- 229920000297 Rayon Polymers 0.000 title abstract 3
- 229920002678 cellulose Polymers 0.000 abstract 3
- 239000001913 cellulose Substances 0.000 abstract 3
- 238000010411 cooking Methods 0.000 abstract 2
- 238000006386 neutralization reaction Methods 0.000 abstract 2
- 229920002488 Hemicellulose Polymers 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 239000007857 degradation product Substances 0.000 abstract 1
- 238000006073 displacement reaction Methods 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 229920005610 lignin Polymers 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- 239000002023 wood Substances 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/02—Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes
- D21C3/022—Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes in presence of S-containing compounds
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C1/00—Pretreatment of the finely-divided materials before digesting
- D21C1/02—Pretreatment of the finely-divided materials before digesting with water or steam
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Paper (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Patente de Invenção: <B>"PROCESSO PARA A PREPARAçãO DE SUBSTNCIAS CELULóSICAS DE VISCOSE"<D>. A presente invenção refere-se a um processo para a preparação de substância celulósica de viscose de lignoceluloses como madeiras de matos folhados, árvores coníferas ou plantas de um ano, em cujo processo a lignocelulose é tratada em um fervedouro inicialmente com vapor saturado para a pré-hidrólise de hemiceluloses e em seguida sem distensão com lixívia preta (HSL) de um cozimento de substância celulósica de sulfato precedente, bem como eventualmente sob adição de lixívia branca fresca (WL) para a neutralização dos produtos de reação ácidos originados, pelo que no fervedouro se origina lixívia de neutralização (NL). Após a adição da quantidade de álcali necessária na forma de lixívia branca fresca (WL), eventualmente ligada com um deslocamento da lixívia de neutralização (NL) e ajuste de temperatura, efetua-se o cozimento logo a seguir com ou sem gradiente de temperatura. Ao alcançar o grau de desintegração desejado, o cozimento é terminado pelo deslocamento da lixívia preta quente (HSL), simultaneamente a substância celulósica é liberta de produtos de degradação da lignina ainda aderentes e a substância celulósica assim obtida é evacuada em uma temperatura inferior a 100C do fervedouro.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AT0238292A AT398588B (de) | 1992-12-02 | 1992-12-02 | Verfahren zur herstellung von viskosezellstoffen |
| PCT/AT1993/000183 WO1994012719A1 (de) | 1992-12-02 | 1993-12-02 | Verfahren zur herstellung von viskosezellstoffen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR9307589A true BR9307589A (pt) | 1999-08-31 |
Family
ID=3533355
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR9307589-8A BR9307589A (pt) | 1992-12-02 | 1993-12-02 | Processo para a preparação de substncias celulósicas de viscose |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US5676795A (pt) |
| EP (1) | EP0672207B1 (pt) |
| JP (1) | JPH08503744A (pt) |
| CN (1) | CN1041645C (pt) |
| AT (1) | AT398588B (pt) |
| BR (1) | BR9307589A (pt) |
| CA (1) | CA2150381C (pt) |
| DE (1) | DE59304443D1 (pt) |
| ES (1) | ES2097021T3 (pt) |
| FI (1) | FI952509A7 (pt) |
| RU (1) | RU2122055C1 (pt) |
| WO (1) | WO1994012719A1 (pt) |
Families Citing this family (50)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI103898B (fi) * | 1994-01-24 | 1999-10-15 | Sunds Defibrator Pori Oy | Menetelmä prehydrolysoidun sellun ja/tai sellumassan tuottamiseksi |
| US6210801B1 (en) | 1996-08-23 | 2001-04-03 | Weyerhaeuser Company | Lyocell fibers, and compositions for making same |
| US6235392B1 (en) * | 1996-08-23 | 2001-05-22 | Weyerhaeuser Company | Lyocell fibers and process for their preparation |
| US6221487B1 (en) | 1996-08-23 | 2001-04-24 | The Weyerhauser Company | Lyocell fibers having enhanced CV properties |
| US6471727B2 (en) | 1996-08-23 | 2002-10-29 | Weyerhaeuser Company | Lyocell fibers, and compositions for making the same |
| US6306334B1 (en) | 1996-08-23 | 2001-10-23 | The Weyerhaeuser Company | Process for melt blowing continuous lyocell fibers |
| US6331354B1 (en) | 1996-08-23 | 2001-12-18 | Weyerhaeuser Company | Alkaline pulp having low average degree of polymerization values and method of producing the same |
| US6773648B2 (en) | 1998-11-03 | 2004-08-10 | Weyerhaeuser Company | Meltblown process with mechanical attenuation |
| BR9916641A (pt) | 1998-12-30 | 2001-09-25 | Kimberly Clark Co | Processo de reciclagem por explosão a vapor de fibras e tecidos fabricados a partir das fibras recicladas |
| US6413362B1 (en) | 1999-11-24 | 2002-07-02 | Kimberly-Clark Worldwide, Inc. | Method of steam treating low yield papermaking fibers to produce a permanent curl |
| RU2198973C2 (ru) * | 2001-01-22 | 2003-02-20 | Кооператив "Техпрогресс" | Способ получения целлюлозы |
| WO2005045108A1 (ja) * | 2003-10-31 | 2005-05-19 | Toray Industries, Inc. | 繊維糸およびそれを用いた布帛 |
| US8317975B2 (en) | 2004-04-20 | 2012-11-27 | The Research Foundation Of The State University Of New York | Product and processes from an integrated forest biorefinery |
| US7520958B2 (en) * | 2005-05-24 | 2009-04-21 | International Paper Company | Modified kraft fibers |
| EP3002365A1 (en) * | 2005-05-24 | 2016-04-06 | International Paper Company | Modified kraft fibers |
| FI20065105A0 (fi) * | 2006-02-10 | 2006-02-10 | Metso Paper Inc | Menetelmä hydrolyysituotteiden talteenottamiseksi |
| FI123036B (fi) | 2006-02-10 | 2012-10-15 | Metso Paper Inc | Menetelmä hydrolyysituotteiden talteenottamiseksi |
| AT503610B1 (de) * | 2006-05-10 | 2012-03-15 | Chemiefaser Lenzing Ag | Verfahren zur herstellung eines zellstoffes |
| US9090915B2 (en) * | 2008-04-22 | 2015-07-28 | Wisconsin Alumni Research Foundation | Sulfite pretreatment for biorefining biomass |
| FI20085425L (fi) * | 2008-05-08 | 2009-11-09 | Metso Paper Inc | Sulfaattiesihydrolyysikeittomenetelmä |
| FI121237B (fi) | 2008-10-21 | 2010-08-31 | Danisco | Menetelmä ksyloosin ja liukosellun tuottamiseksi |
| WO2010104458A1 (en) * | 2009-03-09 | 2010-09-16 | Kiram Ab | A shaped cellulose manufacturing process combined with a pulp mill recovery system |
| RU2523973C1 (ru) * | 2010-05-04 | 2014-07-27 | Байа Спешалти Сельюлоз Са | Способ переработки целлюлозной массы холоднощелочной экстракцией с повторным использованием щелочного фильтрата и система для его осуществления |
| KR20110123184A (ko) | 2010-05-06 | 2011-11-14 | 바히아 스페셜티 셀룰로스 에스에이 | 높은 알파 용해 펄프 제조를 위한 방법 및 시스템 |
| AT509899A2 (de) | 2010-06-02 | 2011-12-15 | Chemiefaser Lenzing Ag | Verfahren zur verbesserten verarbeitbarkeit von hydrothermolysaten von lignozellulosischem material |
| US8980050B2 (en) | 2012-08-20 | 2015-03-17 | Celanese International Corporation | Methods for removing hemicellulose |
| US8815561B2 (en) | 2010-08-23 | 2014-08-26 | Wisconsin Alumni Research Foundation | Metal compounds to eliminate nonproductive enzyme adsorption and enhance enzymatic saccharification of lignocellulose |
| US8916023B2 (en) | 2011-03-18 | 2014-12-23 | Andritz, Inc. | Vapor phase hydrolysis vessel and methods related thereto |
| US8951388B2 (en) * | 2011-04-08 | 2015-02-10 | Pec-Tech Engineering And Construction Pte Ltd | Method and system for efficient production of dissolving pulp in a kraft mill producing paper grade pulp with a continuous type digester |
| JP5712754B2 (ja) * | 2011-04-13 | 2015-05-07 | 王子ホールディングス株式会社 | 溶解パルプの製造方法 |
| WO2012158075A1 (en) * | 2011-05-13 | 2012-11-22 | Metso Paper Sweden Ab | Compact process for producing prehydrolyzed pulp |
| CN102251423B (zh) * | 2011-07-28 | 2013-04-24 | 曲传武 | 溶解浆连续置换蒸煮工艺 |
| BR112014029701B8 (pt) * | 2012-05-28 | 2022-02-08 | Chemiefaser Lenzing Ag | Processo para fabricação de polpa de dissolução, licor, e, polpa |
| US20140048221A1 (en) * | 2012-08-20 | 2014-02-20 | Celanese International Corporation | Methods for extracting hemicellulose from a cellulosic material |
| WO2015037647A1 (ja) * | 2013-09-11 | 2015-03-19 | 日本製紙株式会社 | 溶解クラフトパルプの製造方法 |
| SE539706C2 (en) | 2014-11-07 | 2017-11-07 | Valmet Oy | Method for recovering hydrolyzate |
| SE538454C2 (en) | 2014-11-27 | 2016-07-12 | Valmet Oy | Method for displacement in batch digesters |
| KR102053562B1 (ko) * | 2016-01-26 | 2019-12-06 | 후지필름 가부시키가이샤 | 나노 파이버 및 부직포 |
| DE102016225827B4 (de) * | 2016-12-21 | 2019-04-11 | Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. | Zweistufiges Aufschlussverfahren zur chemischen Fraktionierung von Lignocellulose |
| SE541646C2 (en) * | 2017-07-04 | 2019-11-19 | Valmet Oy | Method for operating a continuous vertical reactor comprising a prehydrolysis zone and the reactor design as such |
| WO2019039982A1 (en) * | 2017-08-25 | 2019-02-28 | Valmet Ab | IMPROVED COMPACT PROCESS FOR THE PRODUCTION OF A PREHYDROLYZED PASTE |
| EP3536833A1 (de) | 2018-03-06 | 2019-09-11 | Lenzing Aktiengesellschaft | Lyocell-fasern ohne mannan |
| TW201938591A (zh) | 2018-03-06 | 2019-10-01 | 奧地利商蘭仁股份有限公司 | 溶解性木漿 |
| CN109505178B (zh) * | 2018-11-21 | 2021-08-17 | 湖南骏泰新材料科技有限责任公司 | 一种农林三剩物制备纤维素的蒸煮方法 |
| WO2020132120A1 (en) * | 2018-12-18 | 2020-06-25 | North Carolina State University | Fast disintegrating paper products and methods of making |
| SE1950402A1 (en) * | 2019-04-01 | 2020-10-02 | Valmet Oy | Method for extracting hemicellulose from lignocellulosic material |
| SE543924C2 (en) * | 2019-04-02 | 2021-09-28 | Valmet Oy | A method for extracting hydrolysate in a batch pulp production process |
| SE1950606A1 (en) * | 2019-05-22 | 2020-10-13 | Valmet Oy | A method for extracting hydrolyzate, a batch cooking system and a hydrolyzate extracting arrangement |
| CN112321726B (zh) * | 2020-11-23 | 2022-11-25 | 北方化学工业股份有限公司 | 低粘度高硝化度含能b棉的煮洗工艺 |
| CN112726252B (zh) * | 2020-11-30 | 2022-11-25 | 山东华泰纸业股份有限公司 | 一种造纸厂废渣的综合利用方法 |
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| DE399876C (de) * | 1924-07-31 | Maschf Augsburg Nuernberg Ag | Verfahren und Vorrichtung zum Betrieb von Kochanlagen, insbesondere zur Herstellung von Zellstoff | |
| CA605742A (en) * | 1960-09-27 | N. Rogers Linwood | Purified cellulose fiber and process for producing | |
| DE366701C (de) * | 1919-08-16 | 1923-01-10 | Erik Ludvig Rinman Dr | Verfahren zur Vorbehandlung des zellulosehaltigen Rohstoffes bei der Herstellung vonZellulose |
| US1742218A (en) * | 1925-04-28 | 1930-01-07 | Brown Co | Process for the production of high alpha cellulose fiber |
| US1831435A (en) * | 1926-02-12 | 1931-11-10 | Eastern Mfg Company | Method for the preparation of alpha cellulose pulp |
| US1839773A (en) * | 1927-01-21 | 1932-01-05 | Brown Co | Rayon manufacture |
| US1851008A (en) * | 1927-04-28 | 1932-03-29 | Eastern Mfg Company | Preparation of alpha cellulose pulp by attrition |
| US1780347A (en) * | 1929-05-08 | 1930-11-04 | Lauri I L Durchman | Process of manufacturing alpha cellulose |
| US1852466A (en) * | 1930-07-11 | 1932-04-05 | Permutit Co | Purification of viscose |
| US2301314A (en) * | 1935-02-16 | 1942-11-10 | Univ Minnesota Board Of Regent | Process of making alpha cellulose |
| USRE23868E (en) * | 1946-09-10 | 1954-09-14 | Method of removing hemicellulose | |
| US2694631A (en) * | 1949-08-31 | 1954-11-16 | Eastman Kodak Co | Process of preparing wood pulp |
| AT181173B (de) * | 1951-01-11 | 1955-02-25 | Karlstad Mekaniska Ab | Verfahren zur Verarbeitung von Holz zu Zellstoff |
| CH291830A (de) * | 1951-01-18 | 1953-07-15 | Aktiebolag Wikmanshytte Bruks | Verfahren zur Vorbehandlung von Holzschnitzeln zwecks Herstellung von Zellstoff. |
| US3413189A (en) * | 1964-01-29 | 1968-11-26 | Kamyr Ab | Method of performing hydrolysis and alkalic digestion of cellulosic fiber material with prevention of lignin precipitation |
| US3532597A (en) * | 1969-03-11 | 1970-10-06 | Uddeholms Ab | Preparation of dissolving pulps from wood by hydrolysis and alkaline sulfite digestion |
| US3544422A (en) * | 1969-06-10 | 1970-12-01 | Buckeye Cellulose Corp | Prehydrolysis treatment for chemical cellulose production |
| US3832278A (en) * | 1971-06-01 | 1974-08-27 | Process Evaluation Devel | Prehydrolysis and digestion of bagasse fibers |
| US3832279A (en) * | 1972-08-07 | 1974-08-27 | Texaco Inc | Integrated kraft pulping process,including hydrogen sulfide pretreatment of wood chips and sulfur dioxide treatment of black liquor to lower ph thereof prior to coking |
| US4123318A (en) * | 1976-06-29 | 1978-10-31 | Kamyr, Inc. | Three-vessel treatment system |
| US4574032A (en) * | 1979-10-15 | 1986-03-04 | Westvaco Corporation | Process for delignification of lignocellulosic material in the presence of anthraquinone in solution with white and black liquors |
| SU1331924A1 (ru) * | 1985-12-16 | 1987-08-23 | Всесоюзное научно-производственное объединение целлюлозно-бумажной промышленности | Способ получени целлюлозы дл химической переработки |
| SU1490198A1 (ru) * | 1987-09-14 | 1989-06-30 | Всесоюзное научно-производственное объединение целлюлозно-бумажной промышленности | Способ получени целлюлозы дл химической переработки |
| US5053108A (en) * | 1989-06-28 | 1991-10-01 | Kamyr Ab | High sulfidity cook for paper pulp using black liquor sulfonization of steamed chips |
| US5183535B1 (en) * | 1990-02-09 | 1996-02-06 | Sunds Defibrator Rauma Oy | Process for preparing kraft pulp using black liquor pretreatment reaction |
| US5213662A (en) * | 1991-08-14 | 1993-05-25 | Kamyr, Inc. | Treatment of chips with high temperature black liquor to reduce black liquor viscosity |
-
1992
- 1992-12-02 AT AT0238292A patent/AT398588B/de not_active IP Right Cessation
-
1993
- 1993-12-02 RU RU95113599A patent/RU2122055C1/ru active
- 1993-12-02 ES ES94900624T patent/ES2097021T3/es not_active Expired - Lifetime
- 1993-12-02 BR BR9307589-8A patent/BR9307589A/pt not_active IP Right Cessation
- 1993-12-02 WO PCT/AT1993/000183 patent/WO1994012719A1/de not_active Ceased
- 1993-12-02 US US08/446,819 patent/US5676795A/en not_active Expired - Lifetime
- 1993-12-02 EP EP94900624A patent/EP0672207B1/de not_active Expired - Lifetime
- 1993-12-02 FI FI952509A patent/FI952509A7/fi unknown
- 1993-12-02 CA CA002150381A patent/CA2150381C/en not_active Expired - Lifetime
- 1993-12-02 JP JP6512567A patent/JPH08503744A/ja active Pending
- 1993-12-02 DE DE59304443T patent/DE59304443D1/de not_active Expired - Fee Related
- 1993-12-02 CN CN93121600A patent/CN1041645C/zh not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| ES2097021T3 (es) | 1997-03-16 |
| CN1041645C (zh) | 1999-01-13 |
| EP0672207B1 (de) | 1996-11-06 |
| FI952509A0 (fi) | 1995-05-23 |
| JPH08503744A (ja) | 1996-04-23 |
| FI952509A7 (fi) | 1995-05-23 |
| EP0672207A1 (de) | 1995-09-20 |
| RU2122055C1 (ru) | 1998-11-20 |
| ATA238292A (de) | 1994-05-15 |
| DE59304443D1 (de) | 1996-12-12 |
| AT398588B (de) | 1994-12-27 |
| CN1094108A (zh) | 1994-10-26 |
| WO1994012719A1 (de) | 1994-06-09 |
| CA2150381A1 (en) | 1994-06-09 |
| RU95113599A (ru) | 1997-05-27 |
| US5676795A (en) | 1997-10-14 |
| CA2150381C (en) | 2004-11-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FF | Decision: intention to grant | ||
| FG9A | Patent or certificate of addition granted | ||
| B21A | Patent or certificate of addition expired [chapter 21.1 patent gazette] |
Free format text: PATENTE EXTINTA EM 02/12/2013 |