BR0203040A - Processo para preparação de um ácido silìcico de precipitação hidrófobo com elevado grau de brancura e absorção de umidade extremamente baixa - Google Patents
Processo para preparação de um ácido silìcico de precipitação hidrófobo com elevado grau de brancura e absorção de umidade extremamente baixaInfo
- Publication number
- BR0203040A BR0203040A BR0203040-3A BR0203040A BR0203040A BR 0203040 A BR0203040 A BR 0203040A BR 0203040 A BR0203040 A BR 0203040A BR 0203040 A BR0203040 A BR 0203040A
- Authority
- BR
- Brazil
- Prior art keywords
- bed
- preparation
- extremely low
- moisture absorption
- low moisture
- Prior art date
Links
- 238000001556 precipitation Methods 0.000 title abstract 3
- 235000012239 silicon dioxide Nutrition 0.000 title abstract 3
- 238000010521 absorption reaction Methods 0.000 title abstract 2
- 230000002209 hydrophobic effect Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 title abstract 2
- 239000012530 fluid Substances 0.000 abstract 2
- 230000001590 oxidative effect Effects 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 230000003750 conditioning effect Effects 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 125000005375 organosiloxane group Chemical group 0.000 abstract 1
- 238000010791 quenching Methods 0.000 abstract 1
- 230000000171 quenching effect Effects 0.000 abstract 1
- 125000005624 silicic acid group Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3009—Physical treatment, e.g. grinding; treatment with ultrasonic vibrations
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3045—Treatment with inorganic compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3081—Treatment with organo-silicon compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/309—Combinations of treatments provided for in groups C09C1/3009 - C09C1/3081
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/10—Solid density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/11—Powder tap density
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/19—Oil-absorption capacity, e.g. DBP values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
- C01P2006/82—Compositional purity water content
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/90—Other properties not specified above
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
"PROCESSO PARA PREPARAçãO DE UM áCIDO SILìCICO DE PRECIPITAçãO HIDRóFOBO COM ELEVADO GRAU DE BRANCURA, E ABSORçãO DE UMIDADE EXTREMAMENTE BAIXA". A invenção refere-se a um processo para preparação de ácidos silícicos de precipitação hidrófobos, caracterizado pelo fato de que a) é preparada uma mistura de um derivado de organossiloxano e um ácido silícico de precipitação, b) é realizado um condicionamento a 10 até 150<198>C por um tempo de 0,5 até 72 horas e C) é realizada uma têmpera oxidativa sob condições líquidas acima de 300<198>C com um gás oxidante. As condições fluidas são ajustadas de preferência em um leito em suspensão, leito fixo, leito turbilhonado, leito fluido e/ou leito em ebulição.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10138491A DE10138491A1 (de) | 2001-08-04 | 2001-08-04 | Verfahren zur Herstellung einer hydrophoben Fällungskieselsäure mit hohem Weißgrad und extrem niedriger Feuchtigkeitsaufnahme |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| BR0203040A true BR0203040A (pt) | 2003-05-27 |
Family
ID=7694515
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| BR0203040-3A BR0203040A (pt) | 2001-08-04 | 2002-07-31 | Processo para preparação de um ácido silìcico de precipitação hidrófobo com elevado grau de brancura e absorção de umidade extremamente baixa |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US7074457B2 (pt) |
| EP (1) | EP1281734A1 (pt) |
| JP (1) | JP2003137532A (pt) |
| KR (1) | KR20030022685A (pt) |
| CN (1) | CN1210354C (pt) |
| BR (1) | BR0203040A (pt) |
| DE (1) | DE10138491A1 (pt) |
| TW (1) | TW585839B (pt) |
Families Citing this family (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10138490A1 (de) * | 2001-08-04 | 2003-02-13 | Degussa | Hydrophobe Fällungskieselsäure mit hohem Weißgrad und extrem niedriger Feuchtigkeitsaufnahme |
| JP4209608B2 (ja) * | 2001-11-14 | 2009-01-14 | 信越化学工業株式会社 | 室温硬化性シリコーンゴム組成物 |
| ATE315537T1 (de) * | 2002-06-14 | 2006-02-15 | Degussa | Aluminium-haltige fällungskieselsäure mit einstellbarem bet/ctab-verhältnis |
| BRPI0406904A (pt) * | 2003-01-22 | 2005-12-13 | Degussa | ácidos silìcicos especialmente precipitados para aplicações em borrachas |
| WO2004065299A1 (de) | 2003-01-22 | 2004-08-05 | Degussa Ag | Höchstdispergierbare silicas für gummianwendungen |
| KR101104088B1 (ko) * | 2003-05-14 | 2012-01-12 | 에보닉 데구사 게엠베하 | 표면 개질된 침강 실리카 |
| DE102004005411A1 (de) | 2004-02-03 | 2005-08-18 | Degussa Ag | Hydrophobe Fällungskieselsäure für Entschäumerformulierungen |
| DE102004005409A1 (de) * | 2004-02-03 | 2005-08-18 | Degussa Ag | Hydrophile Fällungskieselsäure für Entschäumerformulierungen |
| DE102004010755A1 (de) * | 2004-03-05 | 2005-09-22 | Degussa Ag | Silikonkautschuk |
| DE102004029069A1 (de) | 2004-06-16 | 2005-12-29 | Degussa Ag | Oberflächenmodifizierte Silicagele |
| DE102005012409A1 (de) * | 2005-03-17 | 2006-09-21 | Wacker Chemie Ag | Wäßrige Dispersionen teilhydrophober Kieselsäuren |
| JP4905652B2 (ja) * | 2005-05-13 | 2012-03-28 | 信越化学工業株式会社 | 室温硬化性オルガノポリシロキサン組成物 |
| US7276156B2 (en) * | 2005-05-26 | 2007-10-02 | Tony Mason Lockerman | Storm drain filter |
| DE102005043202A1 (de) * | 2005-09-09 | 2007-03-15 | Degussa Ag | Fällungskieselsäuren mit besonderer Porengrößenverteilung |
| DE102005043201A1 (de) * | 2005-09-09 | 2007-03-15 | Degussa Ag | Fällungskieselsäuren mit einer besonderen Porengrößenverteilung |
| DE102006048850A1 (de) * | 2006-10-16 | 2008-04-17 | Evonik Degussa Gmbh | Amorphe submicron Partikel |
| US7767180B2 (en) | 2006-05-26 | 2010-08-03 | Degussa Gmbh | Precipitated silicas having special surface properties |
| DE102006024590A1 (de) * | 2006-05-26 | 2007-11-29 | Degussa Gmbh | Hydrophile Kieselsäure für Dichtungsmassen |
| DE102007025685A1 (de) * | 2007-06-01 | 2008-12-04 | Evonik Degussa Gmbh | RTV-Zweikomponenten-Silikonkautschuk |
| WO2009057821A1 (en) * | 2007-10-31 | 2009-05-07 | Dow Corning Toray Co., Ltd. | Microparticle of metal or metal oxide having silicon-containing organic group, and method for producing the same |
| DE102007052269A1 (de) * | 2007-11-02 | 2009-05-07 | Evonik Degussa Gmbh | Fällungskieselsäuren für lagerstabile RTV-1 Siliconkautschukformulierungen ohne Stabilisator |
| US7985292B2 (en) | 2007-11-26 | 2011-07-26 | Evonik Degussa Corporation | Precipitated silica for thickening and creating thixotropic behavior in liquid systems |
| DE102007061455A1 (de) | 2007-12-20 | 2009-06-25 | Evonik Degussa Gmbh | Entschäumerformulierung |
| US9322542B2 (en) * | 2009-08-12 | 2016-04-26 | Edward Bryant Stoneham | Versatile sealed LED lamp |
| CN103911022B (zh) * | 2014-04-10 | 2016-01-20 | 福建省馨和纳米硅业有限公司 | 一种粒径可控的纳米二氧化硅及其制备方法 |
| EP3161043A4 (en) * | 2014-06-30 | 2018-02-14 | Cooper Tire & Rubber Company | Modified fillers for rubber compounding and masterbatches derived therefrom |
| EP3813972A4 (en) | 2018-06-15 | 2022-03-23 | W. R. Grace & Co.-Conn | Defoamer active, manufacturing method thereof, and defoaming formulation |
| DE102020208510A1 (de) | 2020-07-07 | 2022-01-13 | Evonik Operations Gmbh | Modifizierte Kieselsäuren, Verfahren zur deren Herstellung und deren Verwendung |
| EP3954743A1 (de) | 2020-08-12 | 2022-02-16 | Evonik Operations GmbH | Verwendung von siliziumdioxid zur verbesserung der leitfähigkeit von beschichtungen |
| KR20240089012A (ko) * | 2021-11-01 | 2024-06-20 | 미쯔비시 가스 케미칼 컴파니, 인코포레이티드 | 탈산소제 조성물 및 그의 제조 방법, 및 해당 탈산소제 조성물을 구비하는 탈산소제 포장체 및 그의 제조 방법 |
| CN115504762A (zh) * | 2022-09-09 | 2022-12-23 | 南通福美新材料有限公司 | 一种高性能二氧化硅真空绝热板芯材 |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB813453A (en) | 1954-12-14 | 1959-05-13 | Columbia Southern Chem Corp | Silica pigments |
| FR1234245A (fr) | 1959-05-13 | 1960-10-14 | Rhone Poulenc Sa | Procédé de traitement de charges minérales par des dérivés organosiliciques |
| US3334062A (en) | 1965-03-01 | 1967-08-01 | Dow Corning | Process for rendering inorganic powders hydrophobic |
| US3920865A (en) * | 1969-03-29 | 1975-11-18 | Degussa | Process of hydrophorizing highly dispersed metal or metalloid oxides |
| US3830738A (en) | 1970-02-16 | 1974-08-20 | Ici Ltd | Surface treatment of particulate solids |
| DE2435860B2 (de) * | 1974-07-25 | 1977-10-20 | Deutsche Gold- U. Silber-Scheideanstalt, Vorm. Roessler, 6000 Frankfurt | Verfahren zur herstellung von feinteiligen hydrophoben kieselsaeuren oder silicaten |
| DE2513608C2 (de) | 1975-03-27 | 1982-08-05 | Degussa Ag, 6000 Frankfurt | Verfahren zur Hydrophobierung von Kieselsäuren und Silikaten mit Organosilanen |
| DE2628975A1 (de) * | 1976-06-28 | 1977-12-29 | Degussa | Faellungskieselsaeure |
| US4344858A (en) | 1977-03-23 | 1982-08-17 | Kalcor Coatings Company, Inc. | Anti-foaming compositions |
| DE2729244A1 (de) | 1977-06-29 | 1979-01-04 | Degussa | Faellungskieselsaeure |
| US4377493A (en) | 1981-06-26 | 1983-03-22 | Drew Chemical Corporation | Defoamer composition and use thereof |
| JPS636062A (ja) * | 1986-06-25 | 1988-01-12 | Toray Silicone Co Ltd | シリカ微粉末の表面改質方法 |
| FR2630722B1 (fr) | 1988-04-28 | 1990-09-07 | Rhone Poulenc Chimie | Silice de precipitation hydrophobe a proprietes ameliorees |
| DE3815670A1 (de) * | 1988-05-07 | 1990-01-25 | Degussa | Feinteilige faellungskieselsaeure mit hoher struktur, verfahren zu seiner herstellung und verwendung |
| DE3835592A1 (de) | 1988-10-19 | 1990-04-26 | Degussa | Insektizide |
| WO1995005880A1 (en) | 1993-08-20 | 1995-03-02 | Henkel Corporation | Defoamer |
| IN188702B (pt) * | 1995-06-01 | 2002-10-26 | Degussa | |
| US6191122B1 (en) * | 1996-03-29 | 2001-02-20 | DEGUSSA HüLS AKTIENGESELLSCHAFT | Partially hydrophobic precipitated silicas |
| US5959005A (en) * | 1996-04-26 | 1999-09-28 | Degussa-Huls Aktiengesellschaft | Silanized silica |
| DE19616781A1 (de) * | 1996-04-26 | 1997-11-06 | Degussa | Silanisierte Kieselsäure |
| US6020395A (en) * | 1998-01-06 | 2000-02-01 | Kerr Corporation | Homogeneous microfilled dental composite material and method of preparation |
| DE19828364A1 (de) | 1998-06-25 | 1999-12-30 | Degussa | Hydrophobe Fällungskieselsäure |
| US6239243B1 (en) * | 1999-06-10 | 2001-05-29 | Dow Corning Corporation | Method for preparing hydrophilic silica gels with high pore volume |
| WO2001012731A1 (en) | 1999-08-19 | 2001-02-22 | Ppg Industries Ohio, Inc. | Hydrophobic particulate inorganic oxides and polymeric compositions containing same |
-
2001
- 2001-08-04 DE DE10138491A patent/DE10138491A1/de not_active Withdrawn
-
2002
- 2002-05-03 TW TW091109224A patent/TW585839B/zh not_active IP Right Cessation
- 2002-06-11 EP EP02012875A patent/EP1281734A1/de not_active Withdrawn
- 2002-07-31 BR BR0203040-3A patent/BR0203040A/pt not_active IP Right Cessation
- 2002-08-01 JP JP2002225135A patent/JP2003137532A/ja not_active Withdrawn
- 2002-08-02 KR KR1020020045759A patent/KR20030022685A/ko not_active Withdrawn
- 2002-08-02 CN CN02127464.9A patent/CN1210354C/zh not_active Expired - Fee Related
- 2002-08-05 US US10/211,267 patent/US7074457B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| KR20030022685A (ko) | 2003-03-17 |
| US20030130379A1 (en) | 2003-07-10 |
| DE10138491A1 (de) | 2003-02-13 |
| TW585839B (en) | 2004-05-01 |
| JP2003137532A (ja) | 2003-05-14 |
| CN1405239A (zh) | 2003-03-26 |
| US7074457B2 (en) | 2006-07-11 |
| CN1210354C (zh) | 2005-07-13 |
| EP1281734A1 (de) | 2003-02-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 5A E 6A ANUIDADES. |
|
| B08K | Patent lapsed as no evidence of payment of the annual fee has been furnished to inpi [chapter 8.11 patent gazette] |
Free format text: REFERENTE AO DESPACHO PUBLICADO NA RPI 1980 DE 16/12/2008. |