[go: up one dir, main page]

BR0100068A - Processo contìnuo e dispositivo para a secagem e a formação de gel de polìmeros formadores de gel contendo solventes - Google Patents

Processo contìnuo e dispositivo para a secagem e a formação de gel de polìmeros formadores de gel contendo solventes

Info

Publication number
BR0100068A
BR0100068A BR0100068-3A BR0100068A BR0100068A BR 0100068 A BR0100068 A BR 0100068A BR 0100068 A BR0100068 A BR 0100068A BR 0100068 A BR0100068 A BR 0100068A
Authority
BR
Brazil
Prior art keywords
hpa
gel
drying
continuous process
polymers containing
Prior art date
Application number
BR0100068-3A
Other languages
English (en)
Inventor
Dietrich Gehrmann
Hartwig Kempkes
Original Assignee
Bayer Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer Ag filed Critical Bayer Ag
Publication of BR0100068A publication Critical patent/BR0100068A/pt

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B17/00Apparatus for esterification or etherification of cellulose
    • C08B17/06Apparatus for esterification or etherification of cellulose for making cellulose ethers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B11/00Machines or apparatus for drying solid materials or objects with movement which is non-progressive
    • F26B11/12Machines or apparatus for drying solid materials or objects with movement which is non-progressive in stationary drums or other mainly-closed receptacles with moving stirring devices
    • F26B11/14Machines or apparatus for drying solid materials or objects with movement which is non-progressive in stationary drums or other mainly-closed receptacles with moving stirring devices the stirring device moving in a horizontal or slightly-inclined plane
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/06Flash distillation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/90Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms 
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/75Discharge mechanisms
    • B01F35/754Discharge mechanisms characterised by the means for discharging the components from the mixer
    • B01F35/75455Discharge mechanisms characterised by the means for discharging the components from the mixer using a rotary discharge means, e.g. a screw beneath the receptacle
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08BPOLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B11/00Preparation of cellulose ethers
    • C08B11/20Post-etherification treatments of chemical or physical type, e.g. mixed etherification in two steps, including purification
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Drying Of Solid Materials (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

Patente de invenção: <B>"PROCESSO CONTìNUO E DISPOSITIVO PARA A SECAGEM E A FORMAçãO DE GEL DE POLìMEROS FORMADORES DE GEL CONTENDO SOLVENTES"<D>. é descrito um processo contínuo para a secagem e a formação de gel de polímeros formadores de gel contendo solventes, em particular, derivados de polissacarídeos, por meio de resfriamento brusco de suspensões dos polímeros, bem como, um dispositivo para a secagem de produtos contendo solventes. O processo abrange as etapas: dosagem do polímero contendo solventes com um conteúdo de substância sólida de 1 a 65% em peso, e com uma pressão ambiente especial de até 6000 hPa, com uma temperatura do polímero de 20 até 100 C, em uma zona de evaporação (1), sendo que a zona de evaporação (1) apresenta uma pressão de 0,1 hPa até 800 hPa, resfriamento do polímero, em particular, a uma temperatura de < 93 C, liberação do polímero dos solventes em torno de 2 até 5% em peso, com agitação mecânica, mistura e transporte da mistura para a extremidade inferior da zona de evaporação (1) com a formação de uma espessa camada de produto de gel, descarga do polímero com um dispositivo de descarga (7) mecânico, eventualmente, com condensação do polímero e secagem, logo em seguida, do polímero com gel em um dispositivo de secagem para um conteúdo de solvente de, no máximo, 5% em peso. O dispositivo é constituído de, pelo menos, um recipiente de evaporação (3) com uma zona de evaporácão (1), um mecanismo agitador e um dispositivo de transporte (8), com uma admissão de produto (12), uma extração de vapor (5) com produtor de vácuo conectado, com um dispositivo de descarga (7) conectado na extremidade inferior do recipiente de evaporação (3), sendo que no plano mais inferior do dispositivo de transporte (8) estão previstas uma ou mais pás de transporte (9) com aletas de pressão (10), que ultrapassam a entrada do dispositivo de descarga (7) em uma altura de, no máximo, 5 mm, em particular, de 1 a 3 mm.
BR0100068-3A 2000-01-14 2001-01-12 Processo contìnuo e dispositivo para a secagem e a formação de gel de polìmeros formadores de gel contendo solventes BR0100068A (pt)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10001256A DE10001256A1 (de) 2000-01-14 2000-01-14 Kontinuierliches Verfahren und Vorrichtung zur Trocknung und Gelbildung von lösungsmittelhaltigen gelbildenden Polymeren

Publications (1)

Publication Number Publication Date
BR0100068A true BR0100068A (pt) 2001-08-21

Family

ID=7627455

Family Applications (1)

Application Number Title Priority Date Filing Date
BR0100068-3A BR0100068A (pt) 2000-01-14 2001-01-12 Processo contìnuo e dispositivo para a secagem e a formação de gel de polìmeros formadores de gel contendo solventes

Country Status (16)

Country Link
US (2) US6381866B2 (pt)
EP (1) EP1116728B1 (pt)
JP (1) JP4632537B2 (pt)
KR (1) KR100722359B1 (pt)
CN (1) CN1203111C (pt)
AT (1) ATE315586T1 (pt)
BR (1) BR0100068A (pt)
CA (1) CA2330714A1 (pt)
DE (2) DE10001256A1 (pt)
HK (1) HK1038934B (pt)
MX (1) MXPA01000434A (pt)
NO (1) NO326512B1 (pt)
PL (1) PL345053A1 (pt)
RU (1) RU2270837C2 (pt)
TW (1) TW573113B (pt)
UA (1) UA75324C2 (pt)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT413698B (de) * 2002-09-27 2006-05-15 Suedzucker Ag Mischvorrichtung und abdeckvorrichtung, verwendung derselben sowie verfahren zur modifizierung und derivatisierung von kohlenhydraten
US8777479B2 (en) * 2008-10-13 2014-07-15 Dfine, Inc. System for use in bone cement preparation and delivery
DE102006006096A1 (de) * 2006-02-10 2007-08-16 Altenburger Maschinen Jäckering GmbH Vorrichtung und Verfahren zur Einspeisung von feuchten und/oder klebrigen Produkten, insbesondere Zellulose, in einer Luftwirbelmühle
EP2316562A1 (de) * 2009-10-29 2011-05-04 Bühler AG Vorrichtung und Verfahren zur Behandlung eines Schüttguts
US9359450B2 (en) 2011-04-06 2016-06-07 Dow Global Technologies Llc Process for reducing the amount of water-insoluble fibers in a water-soluble cellulose derivative
KR101775414B1 (ko) * 2011-07-27 2017-09-19 다우 글로벌 테크놀로지스 엘엘씨 셀룰로스 에테르로부터 알킬렌 할로게노하이드린을 제거하는 방법
FI125941B (en) * 2012-02-13 2016-04-15 Upm Kymmene Corp Method and apparatus for treating fibril pulp and a fibril pulp product
JP6013018B2 (ja) * 2012-04-25 2016-10-25 株式会社カワタ 供給装置
CN102914134A (zh) * 2012-10-15 2013-02-06 曾应祥 一种过热蒸汽干燥装置
EP2937363B1 (en) * 2014-04-22 2019-02-27 Shin-Etsu Chemical Co., Ltd Method for producing cellulose ether
DK2949218T3 (en) 2014-05-28 2018-01-02 Dmk Deutsches Milchkontor Gmbh Process for the production of bacteria-poor milk products
DK2962574T3 (da) 2014-07-02 2017-11-27 Dmk Deutsches Milchkontor Gmbh Proces til fremstillingen af lav-bakterie mælkeprodukter
CN104740888A (zh) * 2014-12-25 2015-07-01 天津北洋百川生物技术有限公司 甜菊叶浸提液的干燥方法
CN108940020A (zh) * 2018-08-15 2018-12-07 邢文涛 一种进料及输送一体化涂料搅拌装置
CN110332776A (zh) * 2019-05-14 2019-10-15 嘉兴沐栗服饰有限公司 一种甘草加工装置
CN111252724A (zh) * 2020-01-19 2020-06-09 清华-伯克利深圳学院筹备办公室 凝胶纤维连续制造装置及连续制造方法和生物打印机
CN111426169A (zh) * 2020-04-12 2020-07-17 嘉兴沃瑞科技有限公司 一种二氧化硅用旋转闪蒸干燥机
CN111916656B (zh) * 2020-07-21 2025-05-13 合肥通用机械研究院有限公司 一种用于三元材料的集成式生产系统
CN111912197A (zh) * 2020-08-03 2020-11-10 南京睿泉环保科技有限公司 一种有机固体的烘干装置
US11287185B1 (en) 2020-09-09 2022-03-29 Stay Fresh Technology, LLC Freeze drying with constant-pressure and constant-temperature phases
CN114082503B (zh) * 2022-01-24 2022-07-12 常州汉科汽车科技有限公司 一种液体合金用辅助颗粒混匀输送设备及其使用方法
CN115406205A (zh) * 2022-09-01 2022-11-29 乐山职业技术学院 一种炭气凝胶干燥装置

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2331864A (en) * 1942-03-20 1943-10-12 Dow Chemical Co Method of preparing powdered cellulose ethers quickly soluble in cold water
DE952264C (de) * 1952-04-06 1956-11-15 Henkel & Cie Gmbh Verfahren zur UEberfuehrung feuchter, faseriger Methylcellulosen in Pulver von hoherLoesungsgeschwindigkeit
DE1964949C3 (de) * 1969-12-24 1980-09-25 Bayer Ag, 5090 Leverkusen Vorrichtung zum Konzentrieren einer Lösung oder Suspension
SU392072A1 (ru) * 1970-12-21 1973-07-27 Способ отбелки органорастворимых
JPS5440479Y2 (pt) * 1975-05-12 1979-11-28
JPS51143781A (en) * 1975-06-02 1976-12-10 Toho Rayon Kk Unexpansible unwoven fabrics
US4127945A (en) * 1976-06-01 1978-12-05 Bayer Aktiengesellschaft Process and a dryer for drying polychloroprene sheets
US4575950A (en) * 1983-11-08 1986-03-18 Phillips Petroleum Company Method for removal of residual solvent from particulate crumb made by solution polymerization
BR9107026A (pt) * 1991-05-08 1994-04-19 Tom Ao Zakrytogo N Proizv Processo de secagem de um revestimento de polimero protetor em uma superficie de um artigo, a partir de uma solucao e dispositivo para preparacao do mesmo
GB2262527A (en) * 1992-07-02 1993-06-23 Dow Deutschland Inc Process for grinding cellulose compounds
US5394622A (en) * 1993-06-15 1995-03-07 Xerox Corporation Method and apparatus for a mechanical dryer for drying thick polymer layers on a substrate
US6058623A (en) * 1993-09-24 2000-05-09 The Chemithon Corporation Apparatus and process for removing volatile components from a composition
US5662840A (en) * 1994-06-10 1997-09-02 Fmc Corporation Process for making gel microbeads
WO1996030410A1 (de) * 1995-03-31 1996-10-03 Akzo Nobel N.V. Verfahren zur herstellung von celluloselösungen in wasserhaltigen tertiären amin-n-oxiden
US5849862A (en) * 1995-06-07 1998-12-15 Cytec Technology Corp. Processes of spray drying polymer-containing dispersions, water-in-oil emulsions and water-in-oil microemulsions
US5659972A (en) * 1995-10-06 1997-08-26 Avery Dennison Corporation Apparatus and method for drying or curing web materials and coatings
DE19602227A1 (de) 1996-01-23 1997-07-24 Bayer Ag Vorratsbehälter mit Austragsvorrichtung
US5647142A (en) * 1996-05-13 1997-07-15 Niro A/S Apparatus and process for drying a moist material dispersed or dispersible in a stream of drying gas
BR9807498A (pt) * 1997-01-21 2000-03-21 Wolff Walsrode Ag Processo para a preparação de derivados de polissacarìdeos divididos finamente
US5893950A (en) * 1997-07-31 1999-04-13 The Dexter Corporation Method and apparatus for applying a water-based coating composition to a substrate
CN1166444C (zh) * 1998-03-20 2004-09-15 埃克森美孚化学专利公司 浆液聚合中的挥发性物质的连续除去
US6253463B1 (en) * 1999-04-26 2001-07-03 Niro A/S Method of spray drying
US6223455B1 (en) * 1999-05-03 2001-05-01 Acusphere, Inc. Spray drying apparatus and methods of use

Also Published As

Publication number Publication date
NO326512B1 (no) 2008-12-22
NO20010214L (no) 2001-07-16
EP1116728B1 (de) 2006-01-11
CA2330714A1 (en) 2001-07-14
CN1306028A (zh) 2001-08-01
DE10001256A1 (de) 2001-07-19
EP1116728A1 (de) 2001-07-18
US20020112361A1 (en) 2002-08-22
RU2270837C2 (ru) 2006-02-27
US20010008048A1 (en) 2001-07-19
KR100722359B1 (ko) 2007-05-29
HK1038934A1 (en) 2002-04-04
MXPA01000434A (es) 2002-08-06
ATE315586T1 (de) 2006-02-15
JP4632537B2 (ja) 2011-02-16
PL345053A1 (en) 2001-07-16
US6487788B2 (en) 2002-12-03
TW573113B (en) 2004-01-21
CN1203111C (zh) 2005-05-25
NO20010214D0 (no) 2001-01-12
US6381866B2 (en) 2002-05-07
HK1038934B (zh) 2006-01-13
UA75324C2 (en) 2006-04-17
DE50108644D1 (de) 2006-04-06
KR20010086333A (ko) 2001-09-10
JP2001233961A (ja) 2001-08-28

Similar Documents

Publication Publication Date Title
BR0100068A (pt) Processo contìnuo e dispositivo para a secagem e a formação de gel de polìmeros formadores de gel contendo solventes
ROOS et al. Phase transitions of amorphous sucrose and frozen sucrose solutions
BR9710300A (pt) Método para a desvolatização de uma solução de polìmero-solvente e de um polìmero e sistema de descarga para uso com um secador térmico.
EP0801081A3 (en) Method of drying solid polymer and drying apparatus
RU2001100672A (ru) Непрерывный способ и устройство для сушки и гелеобразования гелеобразных полимеров, содержащих растворитель
JPH11285700A (ja) スラッジの機械的及び熱的な脱水方法及び装置
AU781513B2 (en) Method for drying paste-like materials
KR20010034912A (ko) 용액으로부터의 중합체 단리 방법
EP0362706A3 (en) Process for preparing dry IB type crystals of alpha-L-aspartyl-L-phenylalanine methyl ester having improved solubility
KR910011323A (ko) 증기 회수 시스템
WO2015156679A1 (en) Improved process and reactor for drying a mixture containing solid or semi-solids
TW521064B (en) Process for the preparation of anhydrous sodium sulfide
WO2011122935A1 (en) Method and system for drying biomass
BR9916174A (pt) Produtos precursores de medicamentos fluidos prontos para prensagem em comprimidos, péletes e comprimidos revestidos com açúcar, e processos para a preparação dos mesmos
JP2001353719A (ja) 含水原料の脱水乾燥方法およびその装置
US6946571B2 (en) Drying of adipic acid
BG104479A (en) Method for producing phenols, aldehydes, esters and/or ketones from lignin and/or ligninsulphonic acid
IT1255247B (it) Procedimento per l&#39;allontanamento dei componenti volatili da soluzioni contenenti polifenileneteri
NL1003950C2 (nl) Werkwijze voor het continu-drogen van slib en inrichting daarvoor.
US5327660A (en) Drum drying of acrylonitrile production wastes
SU771423A1 (ru) Вакуум-сублимационна сушилка непрерывного действи дл термочувствительных материалов
SU151294A1 (ru) Способ выпаривани водных растворов мочевины
RU2340845C1 (ru) Способ удаления влаги в вакууме
RU2040297C1 (ru) Устройство для очистки сублимирующихся веществ
Goddard Large-scale vacuum dehydration

Legal Events

Date Code Title Description
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: INDEFIRO O PRESENTE PEDIDO DE PATENTE COMO INVENCAO - DE ACORDO COM O ART. 8O DA LPI.

B09B Patent application refused [chapter 9.2 patent gazette]

Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL.