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AU8310987A - Process for removal of basic materials - Google Patents

Process for removal of basic materials

Info

Publication number
AU8310987A
AU8310987A AU83109/87A AU8310987A AU8310987A AU 8310987 A AU8310987 A AU 8310987A AU 83109/87 A AU83109/87 A AU 83109/87A AU 8310987 A AU8310987 A AU 8310987A AU 8310987 A AU8310987 A AU 8310987A
Authority
AU
Australia
Prior art keywords
tobacco
nicotine
solvent
components
conditions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
AU83109/87A
Other versions
AU612128B2 (en
Inventor
Harvey Joseph Grubbs
Tony M. Howell
Ravi Prasad
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
PHILIP MORRIS PRODUCTS Inc
Original Assignee
Philip Morris USA Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=25485521&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=AU8310987(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Philip Morris USA Inc filed Critical Philip Morris USA Inc
Publication of AU8310987A publication Critical patent/AU8310987A/en
Application granted granted Critical
Publication of AU612128B2 publication Critical patent/AU612128B2/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Fertilizers (AREA)
  • Fire-Extinguishing Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Laminated Bodies (AREA)
  • Protection Of Pipes Against Damage, Friction, And Corrosion (AREA)
  • Control Of El Displays (AREA)
  • Superconductors And Manufacturing Methods Therefor (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

A process is provided for the selective removal of basic materials from plant products, in particular, for removing nicotine from tobacco without materially affecting the content of the other components of the tobacco. Tobacco is traversed with a solvent in the supercritical state or in the liquid state wherein nicotine and the other components dissolve in the solvent. The solvent is then passed through an acid-containing trap where the solvent is essentially freed of nicotine. The solvent, depleted of nicotine and enriched in the other components, is then recycled to the tobacco to reextract nicotine. In addition, the tobacco may be pretreated with a chemical base which does not substantially react withe the tobacco components under ambient conditions but rather is activated under the conditions of the extraction process. Pretreatment of the tobacco with a chemical base neutralizes nicotine salts and permits the extraction process to be carried out under milder conditions.
AU83109/87A 1986-12-29 1987-12-29 Process for removal of basic materials Ceased AU612128B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US94710286A 1986-12-29 1986-12-29
US947102 1986-12-29

Publications (2)

Publication Number Publication Date
AU8310987A true AU8310987A (en) 1988-06-30
AU612128B2 AU612128B2 (en) 1991-07-04

Family

ID=25485521

Family Applications (1)

Application Number Title Priority Date Filing Date
AU83109/87A Ceased AU612128B2 (en) 1986-12-29 1987-12-29 Process for removal of basic materials

Country Status (9)

Country Link
EP (1) EP0280817B1 (en)
JP (1) JP2694253B2 (en)
AT (1) ATE102446T1 (en)
AU (1) AU612128B2 (en)
BR (1) BR8707110A (en)
CA (1) CA1317961C (en)
DE (1) DE3789300D1 (en)
FI (1) FI88453C (en)
ZA (1) ZA879384B (en)

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5497792A (en) * 1987-11-19 1996-03-12 Philip Morris Incorporated Process and apparatus for the semicontinuous extraction of nicotine from tobacco
US5435325A (en) * 1988-04-21 1995-07-25 R. J. Reynolds Tobacco Company Process for providing tobacco extracts using a solvent in a supercritical state
US4967771A (en) * 1988-12-07 1990-11-06 R. J. Reynolds Tobacco Company Process for extracting tobacco
US5031644A (en) * 1989-12-29 1991-07-16 R. J. Reynolds Tobacco Company Tobacco expansion process and product
US5076293A (en) * 1989-06-19 1991-12-31 R. J. Reynolds Tobacco Company Process and apparatus for the treatment of tobacco material
US5025812A (en) * 1989-08-10 1991-06-25 R. J. Reynolds Tobacco Company Tobacco processing
DE4002784C1 (en) * 1990-01-31 1991-04-18 B.A.T. Cigarettenfabriken Gmbh, 2000 Hamburg, De
US5065775A (en) * 1990-02-23 1991-11-19 R. J. Reynolds Tobacco Company Tobacco processing
US5131414A (en) * 1990-02-23 1992-07-21 R. J. Reynolds Tobacco Company Tobacco processing
US5234008A (en) * 1990-02-23 1993-08-10 R. J. Reynolds Tobacco Company Tobacco processing
US5095923A (en) * 1991-04-11 1992-03-17 R. J. Reynolds Tobacco Company Tobacco expansion process using 1,1,1,2-tetrafluoroethane
DE19654945C2 (en) * 1996-07-29 1998-05-20 Mueller Extract Co Gmbh Essentially nicotine-free tobacco flavor oil and process for its production
DE19630619C2 (en) * 1996-07-29 1998-07-09 Mueller Extract Co Gmbh Essentially nicotine-free tobacco flavor oil and process for its production
EP1542555B1 (en) 2002-07-18 2011-11-16 Phasex Corporation Reduction of constituents in tobacco
RU2349363C1 (en) * 2004-10-28 2009-03-20 Джапан Тобакко Инк. Method for extraction of component from material and device for its realisation
RU2332915C1 (en) * 2007-02-27 2008-09-10 Олег Иванович Квасенков Plant for producing blend of light kretek
GB201003887D0 (en) 2010-03-09 2010-05-12 British American Tobacco Co Methods for extracting and isolating constituents of cellulosic material
EP4218404A3 (en) 2015-06-26 2023-09-06 Altria Client Services LLC Compositions and methods for producing tobacco plants and products having altered alkaloid levels
GB201707767D0 (en) 2017-05-15 2017-06-28 British American Tobacco Investments Ltd Method of making a tobacco extract
GB201707758D0 (en) 2017-05-15 2017-06-28 British American Tobacco Investments Ltd Ground tobacco composition
GB201707761D0 (en) 2017-05-15 2017-06-28 British American Tobacco Investments Ltd Method of making a tobacco extract
WO2019229704A1 (en) * 2018-05-31 2019-12-05 Radient Technologies Inc. Process for reducing nicotine in tobacco biomass and tobacco composition
CN113115976B (en) * 2021-03-11 2022-07-19 浙江中烟工业有限责任公司 Batch preparation method of nicotine salt and application of nicotine salt in electronic cigarette
CN114868763B (en) * 2022-05-13 2024-06-11 湖南省烟草公司郴州市公司 Tobacco alkali-reducing agent and preparation method and application thereof

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR397021A (en) * 1907-12-11 1909-04-27 Tabacs Desintoxiques En Failli Method and installation for the denicotinization of tobacco
US2227863A (en) * 1938-02-14 1941-01-07 Kinetic Chemicals Inc Extraction of tobacco with fluorochlorohydrocarbons
DE1517273B2 (en) * 1965-04-15 1976-06-24 Eresta Warenhandelsgesellschaft mbH, 6052 Mühlheim PROCESS FOR CONTINUOUS EXTRACTION OF NICOTINE FROM TOBACCO AND FOR THE OBTAINING PRE-CONCENTRATED NICOTINE SALT SOLUTIONS
US4153063A (en) * 1970-09-02 1979-05-08 Studiengesellschaft Kohle Mbh Process for the extraction of nicotine from tobacco
US4215706A (en) * 1978-10-13 1980-08-05 Loew's Theatres, Inc. Nicotine transfer process
US5497792A (en) * 1987-11-19 1996-03-12 Philip Morris Incorporated Process and apparatus for the semicontinuous extraction of nicotine from tobacco

Also Published As

Publication number Publication date
FI875673A0 (en) 1987-12-22
FI875673L (en) 1988-06-30
FI88453B (en) 1993-02-15
JPS63229102A (en) 1988-09-26
EP0280817A2 (en) 1988-09-07
EP0280817A3 (en) 1990-05-16
JP2694253B2 (en) 1997-12-24
CA1317961C (en) 1993-05-18
AU612128B2 (en) 1991-07-04
ATE102446T1 (en) 1994-03-15
DE3789300D1 (en) 1994-04-14
BR8707110A (en) 1988-08-02
FI88453C (en) 1993-05-25
EP0280817B1 (en) 1994-03-09
ZA879384B (en) 1988-09-28

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Legal Events

Date Code Title Description
MK14 Patent ceased section 143(a) (annual fees not paid) or expired