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AU601249B2 - Gray cast iron having both increased wear resistance and toughness - Google Patents

Gray cast iron having both increased wear resistance and toughness Download PDF

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Publication number
AU601249B2
AU601249B2 AU82879/87A AU8287987A AU601249B2 AU 601249 B2 AU601249 B2 AU 601249B2 AU 82879/87 A AU82879/87 A AU 82879/87A AU 8287987 A AU8287987 A AU 8287987A AU 601249 B2 AU601249 B2 AU 601249B2
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Australia
Prior art keywords
wear resistance
cast iron
iron
product
austenite
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AU82879/87A
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AU8287987A (en
Inventor
Bela Victor Kovacs
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Ford Motor Company of Canada Ltd
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Ford Motor Company of Canada Ltd
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D5/00Heat treatments of cast-iron
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C37/00Cast-iron alloys

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Heat Treatment Of Articles (AREA)
  • Refinement Of Pig-Iron, Manufacture Of Cast Iron, And Steel Manufacture Other Than In Revolving Furnaces (AREA)

Description

L.J. DYSON Registered Patent Attorney THE COMMISSIONER OF PATENTS.
Edwd. Waters Sons.
Melbourne.
COMMONWEALTH OF AUSTRAL 0 1 4 t ^f PATENTS ACT 1952-69 COMPLETE SPECIFICATION
(ORIGINAL)
Class Int. Class Application Number: Lodged: 4* Complete Specification Lodged: Accepted: Published: Priority Related Art Related Art: 4 Name of Applicant: Address of Applicant: Actual Inventor: Address for Service: FORD MOTOR COMPANY OF CANADA, LIMITED The Canadian Road, Oakville, Ontario, Canada.
BELA VICTOR KOVACS EDWD. WATERS SONS, 50 QUEEN STREET, MELBOURNE, AUSTRALIA, 3000.
Complete Specification for the invention entitled: GRAY CAST IRON HAVING BOTH INCREASED WEAR RESISTANCE AND TOUGHNESS The following statement is a full description of this invention, including the best method of performing it known to us 1.
61h..- To: The Commissioner of Patents.
I-R 69- I GRAY CAST IRON HAVING BOTH INCREASED WEAR RESISTANCE AND TOUGHNESS Background of the Invention Technical Field The invention relates to the art of making gray cast iron and, more particularly, to the technology Description of the Prior Art "o iv Gray cast iron is the least expensive of all the 15 cast metals. This is due to the type of raw materials used: pig iron, cast iron scrap; steel scrap, limestone, coke and air, all of which are relatively inexpensive.
Most gray cast iron used commercially is used primarily in the as-cast condition. There has been some attention 0 tT to heat treatment and low alloying for gray cast irons through the years.
The general concensus of foundry operators in this country indicates that the composition of gray cast iron should be about (using weight percentages here and throughout the description): 2.0-4.0 carbon; 1.25-3.25 silicon; .75-1.25 manganese; .08-.12 sulfur; and .07-.20 phosphorus.
In the field of abrasive wear, gray cast iron is usually used where the required impact toughness in I 30 service is not severe. Such cast iron is resistant to abrasive wear because of the presence of a high amount of carbides in the matrix of the cast iron. Most gray cast irons will contain at least 10% by weight primary complex :i -2iron carbides. Unfortunately, however, these carbides are normally massive and impart a degree of brittleness to the cast iron which considerably limits its usefulness with reference to impact strength. While relegating gray cast iron to applications without the need for hig'i impact strength, the main developmental effort has been to improve machining.
One attempt to provide greater machinability while retaining excellent wear resistance and fatigue i0 resistance of gray cast irons involves heat treating the as-cast iron to reduce hardness while retaining the carbidic microstructure (see U.S. patent 4,230,506). In this patent, the cast metal was alloyed with a combination of carbide forming agents such as chromium, nickel, copper, molybdenum, and vanadium. They were used in combination to provide a composite total in an amount of 2.25-3.85%; this is a considerable amount of carbide forming agent. The improvement in machinability was achieved by heat treating to an austenitizing temperature, slowly cooling over a period of 1-1/2 hours to a temperature level of 400 0 F, and then air cooling.
Slow cooling promoted the production of pearlite and reduced the hardness of such cast iron, making it more readily machinable. After machining, the iron was quenched to transform any retained austenite to martensite.
The problem with the 4,230,506 patent is that wear resistance is retained or improved at the sacrifice of toughness and strength characteristics, making it unsuitable for applications that require a high level for both of these characteristics.
Similarly, in U.S. patent 3,384,515, the solution to the problem of machinability was to control heat treating to permit the promotion of complex iron carbides while providing for incipient spheroidization of
A
r 3 :;ii~ 3 pearlite, thereby avoiding martensite and reducing the hardness of the material. The same problem with respect to lack of enhancement of toughness and strength characteristics in such a carbidic cast iron remains.
In U.S. patent 2,885,284, an attempt was made to provide for an increase in both the abrasive wear as well as the impact properties of the gray cast iron. The Icontribution of this patent is to incorporate high r amounts of alloying ingredients in the form of aluminum and manganese to promote contrary characteristics.
Aluminum is added in amounts greater than 1% to promote graphitization and manganese is added in amounts greater than 1.5% to promote carbide stabilization. There is no attempt to modify or introduce any unusual heat treating parameters; there is simply a reliance upon conventional processing and heat treating steps. The disclosure i admits, in column 2, lines 27-33, that the amount of t aluminum or manganese that is incorporated will depend c upon which characteristic is desired in the final t t product, namely, to increase toughness the carbon must be predominantly in the form graphite promoted by the use of aluminum,-and to provide for increased hardness the carbon must be predominantly in the form of carbides, which is promoted by the incorporation of manganese.
This disclosure is an "either/or" teaching in that the there is no suggestion that both of such characteristics can be achieved at a high level at the same time.
It is an object of this invention to provide a gray cast iron having both increased wear resistance and i 30 toughness which can be achieved by modification both in the chemistry and the heat treating techniques for gray cast iron.
In addition, it is an object of this invention to provide the above type of gray cast iron which additionally has high tensile strength, high damping
I
rmu*sr~ 4 capacity, high heat conductivity, and more ductility than conventional cast irons.
Summary of the Invention The above objects have been achieved by development of chemistry and process controls which disperse a predetermined mixture of eutectic carbide particles and flake graphite throughout a matrix of high carbon austenite and ferrite.
i 10 The invention specifically is a method comprising: solidifying a hypoeutectic gray iron melt to which has been added a carbide forming agent in an I amount of by weight, selected from the group consisting of Ti, V, Cr, and Mo and, advantageously, a high carbon austenite-ferrite forming agent in an amount of by weight, selected from the group consisting of nickel and copper and (ii) at a solidification rate to form a matrix with a mixture of flake graphite and Seutectic carbide suspended in the matrix; and heat treating the solid by heating to a temperature and I for a period of time to fully austenitize the solid and (ii) quenching the solid to a temperature level and for a period of time to decompose austenite to form a high carbon austenite and ferrite matrix, I ar c-oo\\' The hypoeutectic gray iron contains less than 4.35% carbon equivalent and preferably comprises, by weight, 2.5-3.0% carbon, 2.0-2.5% silicon, .5-.90% manganese, and the remainder iron.
Preferably, the heat treating comprises heating to a temperature level of 1560-1590 0 F for a period of time of 1.5-2.5 hours; and the quenching step comprises quenching to a temperature level of 450-800°F for a period of time of 1.5-2.5 hours. The rate at which such quenching is carried out is preferably in the range of 300-375F per minute.
1
I
Ir a S 4 It S t S 54 5 The resultant cast iron will comprise a microstructure preferably having the suspended mixture comprised of 40-60% flake graphite and the remainder of the mixture eutectic carbide. Such mixture is controlled by the selection of the solidification rate and by the selection of chemistry for the gray cast iron melt. The casting will preferably have a tensile strength of 45-55 ksi, an impact strength of 30-35 ft. lb, and an elongation of about The wear resistance of such casting is 2-3 times greater than conventional gray cast irons and when measured by a standard sleeve test is .0028-.0019 inch per 1000 hours. The casting also is characterized by resistance to scuffing whereby the ratio of horsepower to produce scuffing divided by the normal horsepower is greater than 1.5. These wear resistance parameters are achieved through attainment of a type A graphite flake in the casting.
Summary of the Drawings Figure 1 is a photo-micrograph of the structure of the casting produced by the method of this invention, the microstructure being shown at an enlargement of 500X. Areas of flake graphite, eutectic carbide, and austenite ferrite are indicated.
:1 :1 r S At 954* Detailed Description and Best Mode The preferred method for making a gray cast iron having both increased wear resistance and impact toughness comprises: solidifying a hypoeutectic gray iron melt to which has been added a carbide forming first agent in an amount of by weight, selected from the group consisting of titanium, vanadium, chromium, and molybdenum, and a second agent to facilitate the formation of high carbon austenite-ferrite, said second agent being present in an c~ ~~ia 6 amount of by weight, selected from the group consisting of nickel and copper and (ii) at a solidification rate to form a matrix with a mixture of flake graphite and eutectic carbide suspended in the matrix; and heat treating the solid by heating to a temperature and for a predetermined period of time to fully austenitize the solid (ii) quenching the solid to a temperature level and for a period of time to decompose austenite to form a high carbon austenite-ferrite matrix and (iii) air cooling the solid.
,Chemistry A conventional wear resistant gray iron usually contains 3.0-4.0% carbon, 1.5-3.0% silicon, and .5-.9 manganese. This method lowers the carbon content and o ^adds both a carbide forming agent and an agent to S, facilitate the formation of high carbon austenite-ferrite o during heat treatment. The carbide forming agent is made o in addition to the normal carbide forming tendencies of manganese which is a normal part of gray cast iron.
Aluminum is specifically absent from the present .I chemistry because it is a graphitizer which works against carbide formation and encourages pin hole defects. The addition .of a graphitizing agent is conspicuously absent from the present invention because graphitization can be controlled through process parameters with a given lower amount of ca-bon.
Specifically, the chemistry comprises, preferably, 2.5-3.0% by weight carbon (a hypoeutectic iron-carbon alloy would comprise less than 35% carbon equivalent). If the carbon content were to be below it would be difficult to provide the desired amount of carbide/graphite ratio (40:60 to 60:40) that is necessary for the wear resistance of this invention. If the carbon content were in excess of processing 7 parameters would tend to form an excessive amount of graphite. It is desirable for the starting melt for this invention that it have a carbon equivalent in the range of 3.2-4.35 because below 3.2 too much carbide is formed, and above 4.35 too much graphite is formed, making it difficult to control the graphite/carbide ratio. Silicon is present in an amount of 2.0-2.5% and manganese remains at If the silicon and manganese contents were to be below the designated amounts of 2.0 and i°o. 10 respectively, there would be insufficient volumes of graphite or carbide formation; if the upper limit of manganese was exceeded, Mn segregation will occur and a nonuniform matrix structure will result. If the.upper limit of silicon is exceeded, excessive carbide and/or graphite formation will occur.
The additional carbide forming agent, which is o Sadded to the gray iron melt herein, comprises molybdenum, titanium, chromium, or vanadium. Any one or all of these ingredients may be added as long as they are present in the alloy melt in an amount in the range of as combined. If less than is employed, the carbide volume will be too low; if greater than is employed, then too much carbide will be present.
In order to promote the decomposition of austenite into high carbon austenite and ferrite, without the formation of pearlite or martensite, during the heat treatment and cooling sequence, it is desirable to add either nickel and/or copper in an amount of which functions as a pearlite suppressor and thus an austenite-ferrite former. If the amount of these elements, singly or combined, were to be below then pearlite formation in larger castings will occur, and if exceeding the alloying agent would be wated and is uneconomical.
The above melt is fully solidified at a rate I t rrt 8 over a period of 4-16 minutes to ensure the formation of a carbon mixture in the form of 40-60% by volume graphite and the remainder eutectic carbide.
Processing The solidification of the melt as indicated above is then subjected to a heat treatment sequence which comprises heating to an austenitizing temperature in the range of 1560-1590'F (848.9-865.6 0 C) and held at 10 such temperature for a period of 1.5-2.5 hours, during which time the casting will be fully austenitized. The casting is then quenched to a temperature level of 450-800°F and held for a period of 1.5-2.5 hours. The quench rate should be in the range of 300-375 0 F per minute. If the quench rate were to be slower than 300°F per minute, the opportunity for formation of pearlite would be increased. If the quench rate were to exceed 375 0 F per minute, the tendency for forming quenching cracks (due to high thermal stresses) would be experienced. The quench rate is important because it attempts, by way of processing, to determine the desirable matrix of austenite and ferrite. By observing the quench rate and the required chemistry, such heat treatment sequence will result in a cast iron matrix of austenite-ferrite having a suspended carbon mixture in the form of 40-60% flake graphite and the remainder in the form of eutectic carbide particles. This pro ortioned mixture is one of the key aspects of providing for simultaneous enhancement of wear resistance and impact resistance.
Following the decomposition of austenite to high carbon austenite and ferrite, the casting or solidification is then cooled to room temperature by air cooling.
1~ o ar o o, Do 0 00 0 0) 00 0 9 Microstructure The resulting casting will have a microstructure which consists of a high carbon au.tenite and ferrite matrix with a suspended mixture of flake graphite and eutectic carbide particles. There is a conspicuous absence of martensite or pearlite in the microstructure. The suspended mixture particles constitute about 20% by volume of the microstructure. The graphite particles will be in the form of type A flake graphite because of good inoculation using ferro-silicone. Such type A graphite will influence the damping capacity, thermal conductivity, and machinability of the gray cast iron.
The physical characteristics of such gray cast iron S will have a wear resistance which is at least 2-3 times 15 greater than that of conventional gray cast irons, and with the limited samples that have been tested to date the wear resistance shows .0028-.0019 inch per 1000 hours of a S conventional sleeve test, such test being outlined in the Metals Handbook.
In addition, the wear resistance is characterized by resistance to scuffing wherein the ratio of horsepower to produce scuffing divided by the normal horsepower is greater than 1.5. Gray cast iron, having a type A graphite in a S martensitic matrix, normally exhibits a resistance to scuffing in the range of 1.39-1.45.
C-s' a. C-VN LsE).
The impact resistance was Eested to be in the range of 25-35 ft.lbf, where a conventional gray cast iron has a charpy notch impact value normally in the range of 1-2 ft.lbf. The v-notch used for the test had a 450 included angle, a 0.079 depth, and a 0.010 radius at the bottom of the notch.
The tensile strength of such resultant cast iron is 45-55 ksi, which is in the high range for gray cast iron, and elongation of The hardness for such material is the range of 160-248 BHN.
eaC 0006 *aad a 4 10 Examples Several examples were prepared by melting a gray iron starting material which consisted of silicon in an amount of manganese with phosphorus being and sulphur being The carbon content of the gray iron was varied according to that sh-,/n in Table I along with variations in the added carbide forming agent, and variations in the addition of nickel as an agent to 4 encourage the decomposition of austenite to high 0 austenite and ferrite. Heat Treatment was employed as indicated (such treatment being to heat the casting to 1570 0 F for two hours, quench to 600 0 F, and hold for two 4 hours, then air cool). The wear resistance and impact resistance were recorded for each such example.
While various enx-a h -we £-tae.
been illustrated and described, it will be o-a us to those skilled in the art that vario anges and modifications may be made -iout departing from the invention, and jb'-intended to cover in the appended claims- such changes and equivalents as fall within -true sp rint -and scope of the inetion.
j -4 4 ,*Q a tea S S S S I S C C C 14*5 4 4 TABLE I: C arbo n Content Sample Carbide Former Additive None Austenite! Ferrite Promoter None Heat Treatment Applied No Wear Resistance Poor Impact Resistance (ft. lbE) 2 Mo. .5 Yes Moderate to Good NiI2. 0 Good V. 5 MoI. 5 Ti/. 1 Mo! .1 tv Very Good Good Poor Poor 32 1 (damping very low) 3 None

Claims (6)

1. A method of making a more wear resistant gray cast iron with high wear resistance and impact strength, comprising: solidifying a hypoeutectic gray iron melt to which has been added a carbide forming first agent in an amount of by weight, selected from the group consisting of titanium, vanadi.um, and molybdenum, said solidification being at a rate to form a matrix with a 10 mixture of flake graphite and eutectic carbide suspended in said matrix; and heat treating said solid by heating to a temperature and for a period of time to fully aus-.enitize the solid, (ii) quenching said solid to a 15 predetermined temperature level and holding at said level for a period of time to decompose austenite to form a high carbon austenite and ferrite matrix, (iii) air cooling the solid to room temperature.
2. The method as in claim 1, in which said solidifying step additionally comprises adding a high carbon austenite-ferrite forming agent in an amount of selected from the group consisting of nickel and copper.
3. The method as in claim 1, in which said hypoeuctectic iron contains less than 4.35% carbon equivalent.
4. The method as in claim 1, in which said hypoeutectic gray iron melt comprises, by weight, 2.5-3.0% carbon, 2.0-2.5% silicon, manganese, and the remainder iron. The method as in claim 1, in which said step comprises heating to 1560-1590 0 F for 1.5-2.5 hours.
6. The method as in claim 1, in which step comprises quenching to a temperature level of
450-800OF for 1.5-2.5 hours. 7. is 3 8. comp mixt 9. meth stre ft. 1 char than 11. resi test Art Ar A AIII r a. *r a a atr At A A Al W~OI b *i 4. 4.4 L V 12. resi scuf 13. for WATE The 1 1wt. AUST LJD/j 13 7. The method as in claim 6, in which said quench rate is 300-3750F/minute. 8. The method as in claim 1, in which said mixture is comprised of 40-60% flake graphite and the remainder of said mixture being eutectic carbide particles. 9. The product resulting from the practice of the method of claim 1, which is characterized by a tensile strength of 40-50 ksi, and an impact strength of 30-35 ft.lbf. The product as in claim 9, which is further S*characterized by wear resistance which is 2-3 times greater than that of conventional gray cast iron. t S, 11. The product as in claim 10, in which said wear resistance is .0019-.0028 inch per 1000 hours of sleeve I test. 12. The product as in claim 10, in which said wear resistance is further characterized by a resistance to scuffing ratio greater than 13. The product as in claim 9, in which the graphite for said product is in the type A form. DATED this 14th day of March, 1990 FORD MOTOR COMPANY OF CANADA, LIMITED WATERMARK PATENT TRADEMARK ATTORNEYS, "The Atrium", 290 Burwood Road Hawthorn, Victoria, 3122 AUSTRALIA LJD/AGB:JJC (3/20)
AU82879/87A 1986-12-22 1987-12-21 Gray cast iron having both increased wear resistance and toughness Ceased AU601249B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US945145 1978-09-22
US94514586A 1986-12-22 1986-12-22

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AU601249B2 true AU601249B2 (en) 1990-09-06

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EP (1) EP0272788B1 (en)
JP (1) JPS63166929A (en)
AU (1) AU601249B2 (en)
CA (1) CA1311993C (en)
DE (1) DE3780138T2 (en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0272788B1 (en) * 1986-12-22 1992-07-01 Ford Motor Company Limited A method of making wear resistant gray cast iron
US5242510A (en) * 1992-09-25 1993-09-07 Detroit Diesel Corporation Alloyed grey iron having high thermal fatigue resistance and good machinability
GB9718982D0 (en) * 1997-09-09 1997-11-12 T & N Technology Ltd Disc brake rotor
US6395107B1 (en) * 2000-01-28 2002-05-28 Sundaresa V. Subramanian Cast iron for use in high speed machining with cubic boron nitride and silicon nitride tools
DE10064248A1 (en) 2000-12-22 2002-07-04 Zf Sachs Ag Cast iron alloy for a friction element of a friction clutch and friction element for a friction clutch
CN102211178B (en) * 2011-04-14 2013-09-18 河北坤腾泵业有限公司 Composite suspending agent for producing roller sleeve and disc lining of vertical mill
ITUB20152456A1 (en) * 2015-07-24 2017-01-24 Zanardi Fond S P A PROCEDURE FOR THE PRODUCTION OF MECHANICAL COMPONENTS IN LAMELLAR IRON OR VERMICULAR.
CN109609737B (en) * 2018-12-13 2020-09-25 苏州东海玻璃模具有限公司 Method for eliminating stress of vermicular graphite cast iron glass mold
CN113337686B (en) * 2021-05-31 2022-02-18 东风商用车有限公司 Engine cylinder cover and preparation method thereof

Citations (3)

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Publication number Priority date Publication date Assignee Title
EP0018703A2 (en) * 1979-05-06 1980-11-12 Textron Inc. Camshaft manufacturing process
AU8287987A (en) * 1986-12-22 1988-06-23 Ford Motor Company Of Canada Limited Gray cast iron having both increased wear resistance and toughness
AU577616B2 (en) * 1984-09-04 1988-09-29 Ford Motor Company Of Canada Limited Cg cast iron

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Publication number Priority date Publication date Assignee Title
FR89010E (en) * 1967-07-19
GB545102A (en) * 1940-05-30 1942-05-11 Mond Nickel Co Ltd Improvements relating to cast iron
GB840490A (en) * 1957-06-06 1960-07-06 Goetzewerke Improvements relating to the manufacture of piston rings
US3384515A (en) * 1965-06-21 1968-05-21 Gen Motors Corp Process of preparing improved cast iron articles
JPS55128563A (en) * 1979-03-28 1980-10-04 Nissan Motor Co Ltd Cast iron excellent in wear and seizure resistance
JPS6052515A (en) * 1983-09-01 1985-03-25 Hitachi Metals Ltd Manufacture of tough and hard gray cast iron
JPS6119759A (en) * 1984-07-05 1986-01-28 Toyota Motor Corp Abrasion resistant cast iron

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0018703A2 (en) * 1979-05-06 1980-11-12 Textron Inc. Camshaft manufacturing process
AU577616B2 (en) * 1984-09-04 1988-09-29 Ford Motor Company Of Canada Limited Cg cast iron
AU8287987A (en) * 1986-12-22 1988-06-23 Ford Motor Company Of Canada Limited Gray cast iron having both increased wear resistance and toughness

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CA1311993C (en) 1992-12-29
EP0272788B1 (en) 1992-07-01
DE3780138D1 (en) 1992-08-06
EP0272788A1 (en) 1988-06-29
AU8287987A (en) 1988-06-23
DE3780138T2 (en) 1993-02-11
JPS63166929A (en) 1988-07-11

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