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AU2001291689A1 - Method for producing tertiary c4-c8-alkyl esters of (meth)acryl acid and a falling film evaporator involved therein - Google Patents

Method for producing tertiary c4-c8-alkyl esters of (meth)acryl acid and a falling film evaporator involved therein

Info

Publication number
AU2001291689A1
AU2001291689A1 AU2001291689A AU9168901A AU2001291689A1 AU 2001291689 A1 AU2001291689 A1 AU 2001291689A1 AU 2001291689 A AU2001291689 A AU 2001291689A AU 9168901 A AU9168901 A AU 9168901A AU 2001291689 A1 AU2001291689 A1 AU 2001291689A1
Authority
AU
Australia
Prior art keywords
meth
alkyl esters
film evaporator
falling film
acryl acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001291689A
Inventor
Ruprecht Kroker
Gerhard Nestler
Werner Schmitt
Winfried Schumm
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of AU2001291689A1 publication Critical patent/AU2001291689A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/04—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides onto unsaturated carbon-to-carbon bonds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/06—Evaporators with vertical tubes
    • B01D1/065—Evaporators with vertical tubes by film evaporating
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/09—Plural feed

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
AU2001291689A 2000-07-28 2001-07-27 Method for producing tertiary c4-c8-alkyl esters of (meth)acryl acid and a falling film evaporator involved therein Abandoned AU2001291689A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE10036958A DE10036958A1 (en) 2000-07-28 2000-07-28 Process for the preparation of tert-C4-C8-alkyl esters of (meth) acrylic acid
DE10036958.8 2000-07-28
PCT/EP2001/008713 WO2002010110A2 (en) 2000-07-28 2001-07-27 Method for producing tertiary c4-c8-alkyl esters of (meth)acryl acid and a falling film evaporator involved therein

Publications (1)

Publication Number Publication Date
AU2001291689A1 true AU2001291689A1 (en) 2002-02-13

Family

ID=7650632

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001291689A Abandoned AU2001291689A1 (en) 2000-07-28 2001-07-27 Method for producing tertiary c4-c8-alkyl esters of (meth)acryl acid and a falling film evaporator involved therein

Country Status (6)

Country Link
US (1) US6998026B2 (en)
EP (1) EP1305276B1 (en)
JP (1) JP4970700B2 (en)
AU (1) AU2001291689A1 (en)
DE (2) DE10036958A1 (en)
WO (1) WO2002010110A2 (en)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4278058B2 (en) 2004-11-29 2009-06-10 ボッシュ株式会社 Hydraulic fluid reservoir and hydraulic pressure control unit
DE102006062258A1 (en) * 2006-12-22 2008-06-26 Basf Se Transferring heat to a liquid mixture comprising (meth)acrylic monomer comprises introducing the liquid mixture simultaneously into the primary side of the heat exchanger by a liquid heat carrier and secondary side of the heat exchanger
EP2017255A1 (en) * 2007-07-19 2009-01-21 Basf Se Method for manufacturing tertiary alkyl esters of (meth) acrylic acid with at least 4 carbon atoms in the alkyl
DE102015205752A1 (en) 2015-03-31 2016-10-20 Basf Se Preparation of tert-butyl esters of aliphatic carboxylic acids
MY185499A (en) 2015-12-15 2021-05-19 Basf Se Production of tert-butyl esters of ethylenically unsaturated carboxylic acids
DE202016006882U1 (en) 2016-11-10 2016-11-23 Basf Se Filmable dispersions with tert-butyl (meth) acrylate
FR3060000B1 (en) * 2016-12-08 2020-05-01 Arkema France PROCESS FOR AVOIDING DEPOSITION OF POLYMERS IN A PROCESS FOR THE PURIFICATION OF (METH) ACRYLIC ACID.
CN110114335A (en) * 2016-12-21 2019-08-09 巴斯夫欧洲公司 The method of pure (methyl) tert-butyl acrylate is separated by distillation out from thick (methyl) tert-butyl acrylate
JP7452997B2 (en) * 2016-12-21 2024-03-19 ビーエーエスエフ ソシエタス・ヨーロピア A process in which pure butyl acrylate is obtained by distillation from crude butyl acrylate, where the butyl is n-butyl or isobutyl.
CN115089986B (en) * 2022-07-28 2025-07-22 河南能化技研有限公司 Low temperature centrifugal film-forming evaporator with small temperature difference
CN120359198A (en) 2022-12-15 2025-07-22 巴斯夫欧洲公司 Process for the continuous production of tert-butyl (meth) acrylate

Family Cites Families (31)

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Publication number Priority date Publication date Assignee Title
US3172905A (en) 1965-03-09 Catalytic preparation of esters from tertiary olefins and carboxylic acids
US995776A (en) * 1910-07-18 1911-06-20 Joseph E Dunn Evaporating and concentrating apparatus.
US1028792A (en) * 1910-12-28 1912-06-04 Sanborn Evaporator Company Evaporating apparatus.
CH225352A (en) 1941-05-18 1943-01-31 Rosenblads Patenter Ab Tube evaporator for sprinkling operation with device for distributing the liquid.
US2392255A (en) * 1943-10-20 1946-01-01 John J Mcandrews Evaporator
BE590370A (en) 1959-04-29 1900-01-01
DE1128428B (en) 1959-08-08 1962-04-26 Hoechst Ag Process for the preparation of tertiary alkyl carboxylic acid esters and for the separation and / or recovery of tertiary olefins from hydrocarbon mixtures containing them
DE1135897B (en) 1959-12-28 1962-09-06 Basf Ag Process for the preparation of tertiary butyl esters of acrylic acid or of acrylic acid substituted in the ª ‡ position by chlorine or alkyl radicals
US3087962A (en) 1960-01-21 1963-04-30 Rohm & Haas Process of making esters of acrylic and methacrylic acids
US3082246A (en) 1960-02-17 1963-03-19 Texaco Inc Preparation of tertiary esters
US3031495A (en) 1960-05-13 1962-04-24 Sinclair Refining Co Preparation of tertiary alkyl formate and acetate
DE1249857B (en) 1961-03-29 1967-09-14 Badische Anilin &. Soda-Fabnk Aktiengesellschaft, Ludwigshaf en/Rhem PROCESS FOR THE CONTINUOUS PRODUCTION OF CARBONIC ACID ESTERS OF TERTIARY ALCOHOLS
US3088969A (en) 1961-04-21 1963-05-07 Standard Oil Co Manufacture of t-butyl esters of unsaturated acids
US3620283A (en) * 1969-02-04 1971-11-16 Artisan Ind Falling film evaporator stripper
JPS4924898B1 (en) 1970-12-26 1974-06-26
DE2121123C3 (en) 1971-04-29 1980-06-12 Basf Ag, 6700 Ludwigshafen Process for separating water from aqueous solutions of acrylic acid by azeotropic distillation
DE2212816C3 (en) * 1972-03-16 1974-12-12 Wiegand Karlsruhe Gmbh, 7505 Ettlingen Device for evenly distributing the liquid to be evaporated in a falling film evaporator
US4094734A (en) * 1973-10-15 1978-06-13 Henderson Industrial Corporation Evaporator and treatment of viscous brines
CH586567A5 (en) * 1974-10-09 1977-04-15 Luwa Ag
DE2931553A1 (en) 1979-08-03 1981-02-26 Basf Ag METHOD FOR STABILIZING MONOMERIC ACRYLIC ACID ESTERS AGAINST EARLY POLYMERIZATION
JPS5772939A (en) * 1980-10-24 1982-05-07 Celanese Corp Improved manufacture of ethyl acrylate
DE3105399A1 (en) 1981-02-14 1982-10-21 EC Erdölchemie GmbH, 5000 Köln Process for the preparation of carboxylic acid esters
JPS60130546A (en) 1983-12-20 1985-07-12 Mitsubishi Petrochem Co Ltd Purification of 1,2-unsaturated carboxylic acid
JPH07116103B2 (en) 1986-11-27 1995-12-13 三菱レイヨン株式会社 Method for producing t-butyl methacrylate
DE3709652A1 (en) * 1987-03-24 1988-10-06 Thermo Consulting Heidelberg DEVICE FOR EVAPORATING LIQUIDS OR ABSORBING OR DEGASSING TWO- OR MULTIPLE-MATERIAL SOLUTIONS IN DOWNTUBE CASE FILM DESIGN
US5246541A (en) * 1991-05-14 1993-09-21 A. Ahlstrom Corporation Evaporator for liquid solutions
FI93427B (en) * 1993-04-01 1994-12-30 Tampella Power Oy Falling membrane evaporator
FI101644B (en) * 1994-02-25 1998-07-31 Ahlstrom Machinery Oy Heat transfer elements and process for making it
DE19602640A1 (en) * 1996-01-25 1997-07-31 Basf Ag Process and evaporator for evaporating compounds sensitive to oxidation
JP2001131116A (en) * 1999-11-08 2001-05-15 Nippon Shokubai Co Ltd Method of distillation for liquid including material liable to polymerize
DE19957458A1 (en) * 1999-11-29 2001-05-31 Bayer Ag String evaporator used for removing volatile components has a product distributor formed as a pipe distributor having parallel nozzle pipes with openings in the pipe wall

Also Published As

Publication number Publication date
JP4970700B2 (en) 2012-07-11
US20030127315A1 (en) 2003-07-10
WO2002010110A2 (en) 2002-02-07
JP2004505102A (en) 2004-02-19
EP1305276A2 (en) 2003-05-02
DE50102341D1 (en) 2004-06-24
EP1305276B1 (en) 2004-05-19
DE10036958A1 (en) 2002-02-07
WO2002010110A3 (en) 2002-09-19
US6998026B2 (en) 2006-02-14

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