AU2001254703A1 - Method for producing 2,3,4,5-tetrachlorobenzotrifluoride - Google Patents
Method for producing 2,3,4,5-tetrachlorobenzotrifluorideInfo
- Publication number
- AU2001254703A1 AU2001254703A1 AU2001254703A AU5470301A AU2001254703A1 AU 2001254703 A1 AU2001254703 A1 AU 2001254703A1 AU 2001254703 A AU2001254703 A AU 2001254703A AU 5470301 A AU5470301 A AU 5470301A AU 2001254703 A1 AU2001254703 A1 AU 2001254703A1
- Authority
- AU
- Australia
- Prior art keywords
- chloride
- iii
- tetrachlorobenzotrifluoride
- producing
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- PVRJKVZQZVDIQH-UHFFFAOYSA-N 1,2,3,4-tetrachloro-5-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=CC(Cl)=C(Cl)C(Cl)=C1Cl PVRJKVZQZVDIQH-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 abstract 4
- 229910021578 Iron(III) chloride Inorganic materials 0.000 abstract 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 abstract 2
- QULYNCCPRWKEMF-UHFFFAOYSA-N parachlorobenzotrifluoride Chemical compound FC(F)(F)C1=CC=C(Cl)C=C1 QULYNCCPRWKEMF-UHFFFAOYSA-N 0.000 abstract 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
- C07C17/12—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms in the ring of aromatic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Disclosed herein is a method for producing 2,3,4,5-tetrachlorobenzotrifluoride comprising chlorinating 4-chlorobenzotrifluoride with elemental chlorine, in the presence of from 0.1 to 2% by weight of iron(III) chloride and 0.05 to 0.75% by weight of aluminum(III) chloride, in each case based on 4-chlorobenzotrifluoride, where the weight ratio of iron(III) chloride to aluminum(III) chloride is 10:1 to 1:1.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10016192 | 2000-03-31 | ||
| DE10016192A DE10016192A1 (en) | 2000-03-31 | 2000-03-31 | Process for the preparation of 2,3,4,5-tetrachlorobenzotrifluoride |
| PCT/EP2001/003112 WO2001074746A1 (en) | 2000-03-31 | 2001-03-19 | Method for producing 2,3,4,5-tetrachlorobenzotrifluoride |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AU2001254703A1 true AU2001254703A1 (en) | 2001-10-15 |
Family
ID=7637212
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU2001254703A Abandoned AU2001254703A1 (en) | 2000-03-31 | 2001-03-19 | Method for producing 2,3,4,5-tetrachlorobenzotrifluoride |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US6706934B2 (en) |
| EP (1) | EP1272447B1 (en) |
| JP (1) | JP2003529573A (en) |
| CN (1) | CN1184178C (en) |
| AT (1) | ATE308494T1 (en) |
| AU (1) | AU2001254703A1 (en) |
| CZ (1) | CZ20023256A3 (en) |
| DE (2) | DE10016192A1 (en) |
| ES (1) | ES2250391T3 (en) |
| PL (1) | PL357998A1 (en) |
| WO (1) | WO2001074746A1 (en) |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4401623A (en) * | 1981-07-17 | 1983-08-30 | Rhone-Poulenc Agrochimie | Use of calcium chloride to minimize hydrofluoric acid corrosion to glass during the chlorination of 4-chlorobenzotrifluoride |
| DE4301247A1 (en) * | 1993-01-19 | 1994-07-21 | Bayer Ag | Process for the production of multi-halogenated benzotrichlorides and benzoyl chlorides as well as new trihalobenzotrichlorides and benzoyl chlorides |
| US5750811A (en) * | 1997-04-07 | 1998-05-12 | Occidental Chemical Corporation | Method of making m-chlorobenzotrifluoride |
-
2000
- 2000-03-31 DE DE10016192A patent/DE10016192A1/en not_active Withdrawn
-
2001
- 2001-03-19 PL PL01357998A patent/PL357998A1/en not_active IP Right Cessation
- 2001-03-19 JP JP2001572443A patent/JP2003529573A/en active Pending
- 2001-03-19 WO PCT/EP2001/003112 patent/WO2001074746A1/en not_active Ceased
- 2001-03-19 EP EP01927751A patent/EP1272447B1/en not_active Expired - Lifetime
- 2001-03-19 DE DE50107909T patent/DE50107909D1/en not_active Expired - Lifetime
- 2001-03-19 ES ES01927751T patent/ES2250391T3/en not_active Expired - Lifetime
- 2001-03-19 CN CNB018072364A patent/CN1184178C/en not_active Expired - Fee Related
- 2001-03-19 US US10/239,981 patent/US6706934B2/en not_active Expired - Fee Related
- 2001-03-19 AT AT01927751T patent/ATE308494T1/en not_active IP Right Cessation
- 2001-03-19 CZ CZ20023256A patent/CZ20023256A3/en unknown
- 2001-03-19 AU AU2001254703A patent/AU2001254703A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| EP1272447B1 (en) | 2005-11-02 |
| ATE308494T1 (en) | 2005-11-15 |
| US20030078459A1 (en) | 2003-04-24 |
| PL357998A1 (en) | 2004-08-09 |
| DE10016192A1 (en) | 2001-10-04 |
| WO2001074746A1 (en) | 2001-10-11 |
| CN1184178C (en) | 2005-01-12 |
| CZ20023256A3 (en) | 2003-02-12 |
| ES2250391T3 (en) | 2006-04-16 |
| JP2003529573A (en) | 2003-10-07 |
| US6706934B2 (en) | 2004-03-16 |
| DE50107909D1 (en) | 2005-12-08 |
| CN1419529A (en) | 2003-05-21 |
| EP1272447A1 (en) | 2003-01-08 |
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