AU1271999A - Process for extraction and purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plants - Google Patents
Process for extraction and purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plantsInfo
- Publication number
- AU1271999A AU1271999A AU12719/99A AU1271999A AU1271999A AU 1271999 A AU1271999 A AU 1271999A AU 12719/99 A AU12719/99 A AU 12719/99A AU 1271999 A AU1271999 A AU 1271999A AU 1271999 A AU1271999 A AU 1271999A
- Authority
- AU
- Australia
- Prior art keywords
- zeaxanthin
- lutein
- plants
- purification
- extraction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Abandoned
Links
- KBPHJBAIARWVSC-XQIHNALSSA-N trans-lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C KBPHJBAIARWVSC-XQIHNALSSA-N 0.000 title 2
- JKQXZKUSFCKOGQ-JLGXGRJMSA-N (3R,3'R)-beta,beta-carotene-3,3'-diol Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC1=C(C)C[C@@H](O)CC1(C)C JKQXZKUSFCKOGQ-JLGXGRJMSA-N 0.000 title 1
- 235000005881 Calendula officinalis Nutrition 0.000 title 1
- 241000196324 Embryophyta Species 0.000 title 1
- 240000000785 Tagetes erecta Species 0.000 title 1
- JKQXZKUSFCKOGQ-LQFQNGICSA-N Z-zeaxanthin Natural products C([C@H](O)CC=1C)C(C)(C)C=1C=CC(C)=CC=CC(C)=CC=CC=C(C)C=CC=C(C)C=CC1=C(C)C[C@@H](O)CC1(C)C JKQXZKUSFCKOGQ-LQFQNGICSA-N 0.000 title 1
- QOPRSMDTRDMBNK-RNUUUQFGSA-N Zeaxanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCC(O)C1(C)C)C=CC=C(/C)C=CC2=C(C)CC(O)CC2(C)C QOPRSMDTRDMBNK-RNUUUQFGSA-N 0.000 title 1
- JKQXZKUSFCKOGQ-LOFNIBRQSA-N all-trans-Zeaxanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2=C(C)CC(O)CC2(C)C JKQXZKUSFCKOGQ-LOFNIBRQSA-N 0.000 title 1
- 235000021466 carotenoid Nutrition 0.000 title 1
- 150000001747 carotenoids Chemical class 0.000 title 1
- 238000000605 extraction Methods 0.000 title 1
- 235000012680 lutein Nutrition 0.000 title 1
- 239000001656 lutein Substances 0.000 title 1
- KBPHJBAIARWVSC-RGZFRNHPSA-N lutein Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\[C@H]1C(C)=C[C@H](O)CC1(C)C KBPHJBAIARWVSC-RGZFRNHPSA-N 0.000 title 1
- 229960005375 lutein Drugs 0.000 title 1
- ORAKUVXRZWMARG-WZLJTJAWSA-N lutein Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=CC(O)CC2(C)C)C ORAKUVXRZWMARG-WZLJTJAWSA-N 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 238000000746 purification Methods 0.000 title 1
- FJHBOVDFOQMZRV-XQIHNALSSA-N xanthophyll Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC2C=C(C)C(O)CC2(C)C FJHBOVDFOQMZRV-XQIHNALSSA-N 0.000 title 1
- 235000010930 zeaxanthin Nutrition 0.000 title 1
- 239000001775 zeaxanthin Substances 0.000 title 1
- 229940043269 zeaxanthin Drugs 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
- A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
- A23L5/44—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives using carotenoids or xanthophylls
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/095—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of esters of organic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C35/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring
- C07C35/21—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a ring other than a six-membered aromatic ring polycyclic, at least one hydroxy group bound to a non-condensed ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C403/00—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone
- C07C403/24—Derivatives of cyclohexane or of a cyclohexene or of cyclohexadiene, having a side-chain containing an acyclic unsaturated part of at least four carbon atoms, this part being directly attached to the cyclohexane or cyclohexene or cyclohexadiene rings, e.g. vitamin A, beta-carotene, beta-ionone having side-chains substituted by six-membered non-aromatic rings, e.g. beta-carotene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/09—Geometrical isomers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/16—Systems containing only non-condensed rings with a six-membered ring the ring being unsaturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US6257297P | 1997-10-21 | 1997-10-21 | |
| US60062572 | 1997-10-21 | ||
| US7836098P | 1998-03-18 | 1998-03-18 | |
| US60078360 | 1998-03-18 | ||
| PCT/US1998/022229 WO1999020587A1 (en) | 1997-10-21 | 1998-10-21 | Process for extraction and purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plants |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AU1271999A true AU1271999A (en) | 1999-05-10 |
Family
ID=26742423
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AU12719/99A Abandoned AU1271999A (en) | 1997-10-21 | 1998-10-21 | Process for extraction and purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plants |
Country Status (2)
| Country | Link |
|---|---|
| AU (1) | AU1271999A (en) |
| WO (1) | WO1999020587A1 (en) |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6191293B1 (en) | 1998-04-20 | 2001-02-20 | Inexa, Industria Extractora C.A. | Trans-xanthophyll ester concentrates of enhanced purity and methods of making same |
| UA74177C2 (en) | 2000-01-27 | 2005-11-15 | Дсм Іп Ассетс Б.В. | A process for the preparation of crystalline carotenoid compound |
| US6818798B1 (en) | 2000-05-03 | 2004-11-16 | University Of Maryland, College Park | Process for making a (3R,3′R)-zeaxanthin precursor |
| US6329557B1 (en) | 2000-06-09 | 2001-12-11 | Prodemex, S.A. De C.V. | Purification of xanthophylls from marigold extracts that contain high levels of chlorophylls |
| WO2002004415A2 (en) * | 2000-07-12 | 2002-01-17 | University Of Maryland, College Park | Process for purification and crystallization of palm oil carotenoids |
| PT1303484E (en) | 2000-07-27 | 2005-06-30 | Univ Maryland | METHOD FOR PRODUCING RARE CAROTENOIDS ROUGH FROM COMMERCIALLY AVAILABLE LUTEIN |
| JP2002218994A (en) * | 2001-01-26 | 2002-08-06 | Fuji Chem Ind Co Ltd | Purification of crude xanthophylls |
| JP4227409B2 (en) * | 2001-01-30 | 2009-02-18 | サビンサ コーポレーション | Process for obtaining stable compositions of lutein and lutein derivatives |
| US6784351B2 (en) * | 2001-06-29 | 2004-08-31 | Ball Horticultural Company | Targetes erecta marigolds with altered carotenoid compositions and ratios |
| US7575766B2 (en) * | 2001-06-29 | 2009-08-18 | Ball Horticultural Company | Tagetes erecta with altered carotenoid compositions and ratios |
| WO2003048284A1 (en) | 2001-11-29 | 2003-06-12 | University Of Maryland | Process for extraction and purification of lutein, zeaxanthin and rare carotenoids from marigold flowers and plants |
| JP4834290B2 (en) | 2002-02-06 | 2011-12-14 | ユニバーシティ オブ メリーランド カレッジ パーク | Process for producing β-cryptoxanthin and α-cryptoxanthin from commercially available lutein |
| US6737535B2 (en) | 2002-06-05 | 2004-05-18 | Kancor Flavours And Extracts Limited | Trans-lutein enriched xanthophyll ester concentrate and a process for its preparation |
| EP1371641A1 (en) * | 2002-06-10 | 2003-12-17 | Adisseo France S.A.S. | Process for the formation and isolation of carotenoid crystals |
| US6743953B2 (en) * | 2002-08-26 | 2004-06-01 | Kancor Flavours & Extracts Ltd. | Process for the preparation of xanthophyll crystals |
| US7351424B2 (en) | 2004-07-22 | 2008-04-01 | Bio Lut S.A. De C.V. | Enhanced purity trans-lutein-ester compositions and methods of making same |
| EP2096177A3 (en) | 2004-12-17 | 2010-01-13 | Metanomics GmbH | Process for the production of lutein |
| US7622599B2 (en) * | 2005-04-25 | 2009-11-24 | Katra Phytochem Private Limited | Isolation and purification of carotenoids from marigold flowers |
| CN100368395C (en) * | 2006-05-17 | 2008-02-13 | 浙江医药股份有限公司新昌制药厂 | Method for separating and purifying high-content lutein fatty acid ester from marigold oleoresin |
| CN101402597A (en) * | 2008-10-31 | 2009-04-08 | 南京泛成生物化工有限公司 | Xanthophyll extraction process |
| CN102174005A (en) * | 2011-01-25 | 2011-09-07 | 石河子大学医学院第一附属医院 | Method for extracting lutein from marigold dried flowers |
| TWI466709B (en) * | 2011-07-20 | 2015-01-01 | Nat Univ Chung Hsing | From the original berry Wolfberry a liquid - liquid freezing method for separation of high purity theaflavins palmitate Maize |
| CN102558008A (en) * | 2011-09-08 | 2012-07-11 | 黑龙江省嘉宝生物技术开发有限公司 | Preparation method for lutein |
| CN103091446B (en) * | 2013-01-31 | 2015-12-23 | 甘肃省农垦农业研究院 | Lutein ester saponification degree rapid assay methods |
| CN103275088A (en) * | 2013-05-30 | 2013-09-04 | 湖南炎帝生物工程有限公司 | Method for separating chlorophyll a and carotinoid from nostoc |
| CN104803901A (en) * | 2014-01-27 | 2015-07-29 | 中国科学院大连化学物理研究所 | Method for preparing zeaxanthin through in situ enrichment |
| CN103992256B (en) * | 2014-05-17 | 2016-09-07 | 昆明涞章医药科技有限公司 | A kind of method preparing high-purity lutein ester from pot marigold |
| CN105503681A (en) * | 2014-09-25 | 2016-04-20 | 赵军 | Preparation method of high purity Chinese wolfberry zeaxanthin palmitate |
| CN104447467A (en) * | 2014-10-30 | 2015-03-25 | 蒋小春 | Method for extracting carotenoid from lycium chinense |
| CN105017116A (en) * | 2015-07-31 | 2015-11-04 | 江西恩泉油脂有限公司 | Saponifying technique of lutein extract |
| CN107082756B (en) * | 2017-03-17 | 2018-11-23 | 晨光生物科技集团股份有限公司 | A kind of industrial production process of lutein crystal |
| EP4003567A1 (en) * | 2019-07-26 | 2022-06-01 | Universita' Degli Studi Di Cagliari | Isolation of chromoplastid carotenoids from fruits |
| CN110563625B (en) * | 2019-09-29 | 2020-07-31 | 山东天音生物科技有限公司 | Method for separating and purifying zeaxanthin from marigold oleoresin |
| CN110835315A (en) * | 2019-10-28 | 2020-02-25 | 百瑞源枸杞股份有限公司 | Preparation method of lycium ruthenicum red pigment |
| KR102161387B1 (en) * | 2019-12-09 | 2020-09-29 | 대한켐텍 주식회사 | A composition comprising lutein for improving skin condition and a fuctional food comprising the composition |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4048203A (en) * | 1976-12-06 | 1977-09-13 | Thomas Philip | Purification of lutein-fatty acid esters from plant materials |
| US5382714A (en) * | 1994-03-17 | 1995-01-17 | The Catholic University Of America | Process for isolation, purification, and recrystallization of lutein from saponified marigold oleoresin and uses thereof |
| US5648564A (en) * | 1995-12-21 | 1997-07-15 | Kemin Industries, Inc. | Process for the formation, isolation and purification of comestible xanthophyll crystals from plants |
-
1998
- 1998-10-21 WO PCT/US1998/022229 patent/WO1999020587A1/en not_active Ceased
- 1998-10-21 AU AU12719/99A patent/AU1271999A/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| WO1999020587A8 (en) | 1999-08-26 |
| WO1999020587A1 (en) | 1999-04-29 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK6 | Application lapsed section 142(2)(f)/reg. 8.3(3) - pct applic. not entering national phase |