ATE536338T1 - Verfahren zur herstellung einer mischung aus acetol, propylenglykcol und ethylenglykol aus glycerin - Google Patents
Verfahren zur herstellung einer mischung aus acetol, propylenglykcol und ethylenglykol aus glycerinInfo
- Publication number
- ATE536338T1 ATE536338T1 AT06836781T AT06836781T ATE536338T1 AT E536338 T1 ATE536338 T1 AT E536338T1 AT 06836781 T AT06836781 T AT 06836781T AT 06836781 T AT06836781 T AT 06836781T AT E536338 T1 ATE536338 T1 AT E536338T1
- Authority
- AT
- Austria
- Prior art keywords
- glycerin
- propylene glycol
- acetol
- mixture
- producing
- Prior art date
Links
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 title abstract 9
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title abstract 6
- 235000011187 glycerol Nutrition 0.000 title abstract 3
- XLSMFKSTNGKWQX-UHFFFAOYSA-N hydroxyacetone Chemical compound CC(=O)CO XLSMFKSTNGKWQX-UHFFFAOYSA-N 0.000 title abstract 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title 3
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 title 1
- 150000001875 compounds Chemical class 0.000 abstract 2
- GXDVEXJTVGRLNW-UHFFFAOYSA-N [Cr].[Cu] Chemical compound [Cr].[Cu] GXDVEXJTVGRLNW-UHFFFAOYSA-N 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 230000002528 anti-freeze Effects 0.000 abstract 1
- 238000009835 boiling Methods 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
- C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
- C07C29/143—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones
- C07C29/145—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of ketones with hydrogen or hydrogen-containing gases
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/60—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by elimination of -OH groups, e.g. by dehydration
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
- C07C45/52—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition by dehydration and rearrangement involving two hydroxy groups in the same molecule
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
- C09K5/20—Antifreeze additives therefor, e.g. for radiator liquids
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C11/00—Fermentation processes for beer
- C12C11/02—Pitching yeast
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Food Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Microbiology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Mycology (AREA)
- Zoology (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Thermal Sciences (AREA)
- Materials Engineering (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US73167305P | 2005-10-31 | 2005-10-31 | |
| US11/510,992 US8017816B2 (en) | 2002-04-22 | 2006-08-28 | Method of producing lower alcohols from glycerol |
| PCT/US2006/042707 WO2007053705A2 (en) | 2005-10-31 | 2006-10-31 | Method of producing lower alcohols from glycerol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ATE536338T1 true ATE536338T1 (de) | 2011-12-15 |
Family
ID=37716027
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| AT06836781T ATE536338T1 (de) | 2005-10-31 | 2006-10-31 | Verfahren zur herstellung einer mischung aus acetol, propylenglykcol und ethylenglykol aus glycerin |
Country Status (9)
| Country | Link |
|---|---|
| US (2) | US8017816B2 (de) |
| EP (1) | EP1948582B1 (de) |
| CN (1) | CN101410361B (de) |
| AT (1) | ATE536338T1 (de) |
| BR (1) | BRPI0618120B1 (de) |
| ES (1) | ES2379622T3 (de) |
| PL (1) | PL1948582T3 (de) |
| PT (1) | PT1948582E (de) |
| WO (1) | WO2007053705A2 (de) |
Families Citing this family (41)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8017816B2 (en) | 2002-04-22 | 2011-09-13 | The Curators Of The University Of Missouri | Method of producing lower alcohols from glycerol |
| US8252961B2 (en) | 2002-04-22 | 2012-08-28 | The Curators Of The University Of Missouri | Method of producing lower alcohols from glycerol |
| US7663004B2 (en) | 2002-04-22 | 2010-02-16 | The Curators Of The University Of Missouri | Method of producing lower alcohols from glycerol |
| EP1968887A2 (de) | 2005-12-21 | 2008-09-17 | Virent Energy Systems Inc. | Katalysatoren und verfahren zur neuformung von sauerstoff angereichterten verbindungen |
| EP2016037B1 (de) | 2006-05-08 | 2015-10-28 | Virent, Inc. | Verfahren und systeme zur erzeugung von polyolen |
| KR20090101260A (ko) | 2006-12-20 | 2009-09-24 | 바이렌트 에너지 시스템 인코포레이션 | 기체 생성물을 제조하기 위한 반응기 시스템 |
| ES2817876T3 (es) | 2007-03-08 | 2021-04-08 | Virent Inc | Síntesis de combustibles líquidos a partir de hidrocarburos oxigenados |
| DK2162416T3 (en) * | 2007-05-18 | 2019-02-11 | Biofuel Solution I Malmoe Ab | GAS PHASE PROCEDURE FOR PREPARING MONOAL ALCOHOL FROM GLYCEROL |
| US8293951B2 (en) | 2007-08-31 | 2012-10-23 | Basf Se | Method for producing 1,2-propandiol by hydrogenation in at least three successive reactors |
| US8252962B2 (en) | 2007-08-31 | 2012-08-28 | Basf Se | Method for producing 1,2-propandiol by hydrogenating glycerine in a two-step reactor cascade |
| GB0724232D0 (en) * | 2007-12-12 | 2008-01-23 | Davy Process Techn Ltd | Process |
| EP2240429B1 (de) * | 2007-12-19 | 2018-05-09 | The Curators Of The University Of Missouri | Verfahren zur herstellung niederer alkohole aus glycerol |
| JP5305669B2 (ja) * | 2008-01-21 | 2013-10-02 | 花王株式会社 | 多価アルコールの水素化分解物の製造方法 |
| AR072446A1 (es) * | 2008-03-02 | 2010-09-01 | Dow Global Technologies Inc | Proceso de hidrogenacion mejorado |
| US20090246430A1 (en) | 2008-03-28 | 2009-10-01 | The Coca-Cola Company | Bio-based polyethylene terephthalate polymer and method of making same |
| SG191646A1 (en) * | 2008-06-05 | 2013-07-31 | Huntsman Petrochemical Llc | Process for the production and purification of propylene glycol |
| WO2009151021A1 (ja) * | 2008-06-13 | 2009-12-17 | 三井化学株式会社 | プロピレングリコールの製造方法 |
| US8137527B1 (en) | 2008-07-28 | 2012-03-20 | Primafuel, Inc. | Carbon dioxide isolation and generation |
| KR20110059731A (ko) | 2008-08-27 | 2011-06-03 | 바이렌트 에너지 시스템 인코포레이션 | 바이오매스로부터 액체 연료의 합성방법 |
| WO2010094769A1 (de) * | 2009-02-20 | 2010-08-26 | Basf Se | Verfahren zur herstellung von 1,2-propandiol |
| EP2403894B1 (de) | 2009-03-03 | 2016-06-01 | The Coca-Cola Company | Polyethylenterephthalatverpackung auf biologischer basis und herstellungsverfahren dafür |
| WO2011009936A2 (en) * | 2009-07-24 | 2011-01-27 | Basf Se | Process for the preparation of 1,2-propanediol from glycerol |
| EP2488807B1 (de) * | 2009-10-13 | 2020-04-08 | Sonoco Development, Inc. | Wärmegesteuerte verpackungsvorrichtung und herstellungsverfahren dafür |
| US8383864B2 (en) * | 2009-12-08 | 2013-02-26 | Iowa State University Research Foundation, Inc. | Method for the conversion of cellulose and related carbohydrate materials to low-molecular-weight compounds |
| US8686192B2 (en) | 2009-12-08 | 2014-04-01 | Iowa State University Research Foundation, Inc. | Method for the conversion of cellulose and related carbohydrate materials to low-molecular-weight compounds |
| US8937202B2 (en) * | 2010-02-23 | 2015-01-20 | Battelle Memorial Institute | Processes and systems for the production of propylene glycol from glycerol |
| BRPI1000430A2 (pt) | 2010-02-24 | 2011-10-25 | Petroleo Brasileiro Sa | produção de propilenoglicol a partir de glicerina |
| WO2011138643A2 (en) * | 2010-02-26 | 2011-11-10 | Council Of Scientific & Industrial Research (An Indian Registered Body Incorporated Under The Registration Of Societies Act (Act Xxxi Of 1860) | A process for preparation of hydroxyacetone or propylene glycol |
| IS8889A (is) * | 2010-03-18 | 2011-09-19 | Efnaferli Ehf | Vetnismeðhöndlun glýseríns við lágan þrýsting til að framleiða blandaðar afurðir |
| JP5861024B2 (ja) | 2011-01-13 | 2016-02-16 | Jnc株式会社 | 多価アルコールからのグリコールの製造方法 |
| US8969634B2 (en) | 2011-09-26 | 2015-03-03 | Honeywell International Inc. | Combination reactor system |
| CN102399131A (zh) * | 2011-09-30 | 2012-04-04 | 西南化工研究设计院 | 一种由生物甘油低温低压加氢制备1,2-丙二醇的工艺 |
| US8975453B2 (en) | 2012-03-13 | 2015-03-10 | University Of Idaho | Catalytic conversion of glycerol or acetol to alcohols |
| WO2014034956A1 (ja) * | 2012-09-03 | 2014-03-06 | 住友化学株式会社 | 4-(メチルチオ)ブタン-1,2-ジオールの製造方法 |
| CN105873886B (zh) * | 2013-12-23 | 2019-06-18 | 阿彻丹尼尔斯米德兰德公司 | 用于生产丙二醇的改进的方法 |
| KR101648341B1 (ko) * | 2014-04-30 | 2016-08-16 | 한국화학연구원 | 글리세롤의 수소첨가반응에 의한 프로필렌 글리콜 제조 방법 및 이에 사용되는 촉매 |
| US10235176B2 (en) | 2015-12-17 | 2019-03-19 | The Charles Stark Draper Laboratory, Inc. | Techniques for metadata processing |
| US20190367436A1 (en) * | 2017-01-13 | 2019-12-05 | Archer Daniels Midland Company | Improved process of making bioderived propylene glycol |
| US20250243138A1 (en) * | 2022-04-08 | 2025-07-31 | Ayas Renewables, Inc. | Improved methods of producing lower alcohols from glycerol |
| CN116751117B (zh) * | 2023-05-15 | 2025-07-01 | 大连理工大学 | 一种甘油光催化转化制备丙酮醇和合成气的方法 |
| WO2025078586A1 (en) | 2023-10-13 | 2025-04-17 | Basf Se | Process for preparing a product mixture comprising hydroxyacetone |
Family Cites Families (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE524101C (de) | 1926-01-13 | 1931-05-11 | I G Farbenindustrie Akt Ges | Verfahren zur UEberfuehrung von hoeherwertigen Alkoholen in niedrigerwertige |
| GB490211A (en) | 1936-02-07 | 1938-08-05 | Ass Of American Soap And Glyce | Method of converting aliphatic polyhydric alcohols to alcohols of lower molecular weight |
| BE793928A (fr) * | 1972-01-13 | 1973-05-02 | Deggendorfer Werft Eisenbau | Appareil pour la mise en oeuvre de processus chimiques exothermiques et endothermiques |
| US4451677A (en) * | 1981-08-20 | 1984-05-29 | Davy Mckee (London) Limited | Multistage aldehyde hydrogenation |
| US4516632A (en) * | 1982-08-31 | 1985-05-14 | The United States Of America As Represented By The United States Deparment Of Energy | Microchannel crossflow fluid heat exchanger and method for its fabrication |
| US4642394A (en) * | 1985-07-16 | 1987-02-10 | Celanese Corporation | Production of propanediols |
| US4626604A (en) * | 1985-09-11 | 1986-12-02 | Davy Mckee (London) Limited | Hydrogenation process |
| GB8917862D0 (en) * | 1989-08-04 | 1989-09-20 | Davy Mckee London | Process |
| IT1249955B (it) | 1991-07-10 | 1995-03-30 | Menon S R L | Procedimento di idrogenazione della glicerina |
| IT1249956B (it) * | 1991-07-10 | 1995-03-30 | Menon S R L | Procedimento di idrogenazione catalitica della glicerina |
| DE4128692A1 (de) | 1991-08-29 | 1993-03-04 | Henkel Kgaa | Verfahren zum herstellen von acetol |
| DE4138792A1 (de) | 1991-11-26 | 1993-05-27 | Basf Ag | Verfahren zur herstellung von 1,2-propylenglykol |
| US5266181A (en) * | 1991-11-27 | 1993-11-30 | C. Uyemura & Co., Ltd. | Controlled composite deposition method |
| DE4238492C2 (de) * | 1992-11-14 | 1995-06-14 | Degussa | Verfahren zur Herstellung von 1,2- und 1,3-Propandiol |
| DE4302464A1 (de) | 1993-01-29 | 1994-08-04 | Henkel Kgaa | Herstellung von 1,2-Propandiol aus Glycerin |
| DE4442124A1 (de) | 1994-11-26 | 1996-05-30 | Basf Ag | Verfahren zur Herstellung von Propandiol-1,2 |
| US5811597A (en) * | 1996-08-26 | 1998-09-22 | Huntsman Specialty Chemicals Corp. | Method for the manufacture of methyl tertiary butyl ether from tertiary butyl alcohol and methanol |
| JP3493266B2 (ja) | 1996-08-27 | 2004-02-03 | 高砂香料工業株式会社 | 新規な光学活性ジホスフィン化合物、該化合物を製造す る方法、該化合物を配位子とする遷移金属錯体並びに該 錯体を用いた光学活性体の製造方法 |
| DE19716310A1 (de) * | 1997-04-18 | 1998-10-22 | Metallgesellschaft Ag | Verfahren zum Regenerieren einer beladenen Waschflüssigkeit, die aus einer Anlage zur Entschwefelung eines Wasserstoff und Kohlenoxide enthaltenden Gasgemisches kommt |
| TW476746B (en) * | 1997-07-23 | 2002-02-21 | Shell Int Research | Hydrogenolysis of glycerol |
| US6410804B1 (en) | 1999-12-21 | 2002-06-25 | Exxon Mobil Oil Corporation | Production of phenol using reactive distillation |
| US6291725B1 (en) | 2000-03-03 | 2001-09-18 | Board Of Trustees Operating Michigan State University | Catalysts and process for hydrogenolysis of sugar alcohols to polyols |
| US6518465B2 (en) * | 2000-10-16 | 2003-02-11 | Eastman Chemical Company | Reactive distillation process for hydrolysis of esters |
| JP2002265986A (ja) | 2001-03-15 | 2002-09-18 | Akio Kobayashi | 脂肪酸アルキルエステル及びグリセリンの製造方法 |
| AU2003239799A1 (en) | 2002-04-18 | 2003-10-27 | Dsm Ip Assets B.V. | Continuous process for the manufacture of 3-hydroxy propionitrile |
| US7663004B2 (en) * | 2002-04-22 | 2010-02-16 | The Curators Of The University Of Missouri | Method of producing lower alcohols from glycerol |
| US8017816B2 (en) | 2002-04-22 | 2011-09-13 | The Curators Of The University Of Missouri | Method of producing lower alcohols from glycerol |
| WO2005095536A2 (en) | 2004-03-25 | 2005-10-13 | Suppes Galen J | Method of producing lower alcohols from glycerol |
| US7619118B2 (en) * | 2006-06-07 | 2009-11-17 | The Procter & Gamble Company | Process for the conversion of glycerol to propylene glycol and amino alcohols |
-
2006
- 2006-08-28 US US11/510,992 patent/US8017816B2/en not_active Expired - Fee Related
- 2006-10-31 ES ES06836781T patent/ES2379622T3/es active Active
- 2006-10-31 EP EP06836781A patent/EP1948582B1/de active Active
- 2006-10-31 PT PT06836781T patent/PT1948582E/pt unknown
- 2006-10-31 CN CN2006800501776A patent/CN101410361B/zh active Active
- 2006-10-31 PL PL06836781T patent/PL1948582T3/pl unknown
- 2006-10-31 WO PCT/US2006/042707 patent/WO2007053705A2/en not_active Ceased
- 2006-10-31 AT AT06836781T patent/ATE536338T1/de active
- 2006-10-31 US US12/278,634 patent/US20100019192A1/en not_active Abandoned
- 2006-10-31 BR BRPI0618120A patent/BRPI0618120B1/pt active IP Right Grant
Also Published As
| Publication number | Publication date |
|---|---|
| BRPI0618120B1 (pt) | 2016-07-05 |
| BRPI0618120A2 (pt) | 2011-08-16 |
| EP1948582B1 (de) | 2011-12-07 |
| US8017816B2 (en) | 2011-09-13 |
| US20080315151A1 (en) | 2008-12-25 |
| US20100019192A1 (en) | 2010-01-28 |
| PL1948582T3 (pl) | 2012-05-31 |
| WO2007053705A3 (en) | 2007-08-23 |
| PT1948582E (pt) | 2012-03-09 |
| WO2007053705A2 (en) | 2007-05-10 |
| EP1948582A2 (de) | 2008-07-30 |
| CN101410361A (zh) | 2009-04-15 |
| CN101410361B (zh) | 2013-05-08 |
| ES2379622T3 (es) | 2012-04-30 |
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