AR091998A1 - CELLULOSE PREPARATION PROCEDURE WITH LIGNIN LOW CONCENTRATION - Google Patents
CELLULOSE PREPARATION PROCEDURE WITH LIGNIN LOW CONCENTRATIONInfo
- Publication number
- AR091998A1 AR091998A1 ARP130101261A ARP130101261A AR091998A1 AR 091998 A1 AR091998 A1 AR 091998A1 AR P130101261 A ARP130101261 A AR P130101261A AR P130101261 A ARP130101261 A AR P130101261A AR 091998 A1 AR091998 A1 AR 091998A1
- Authority
- AR
- Argentina
- Prior art keywords
- cellulose
- lignin
- low concentration
- hemicellulose
- preparation procedure
- Prior art date
Links
- 229920002678 cellulose Polymers 0.000 title abstract 6
- 239000001913 cellulose Substances 0.000 title abstract 6
- 229920005610 lignin Polymers 0.000 title abstract 5
- 229920002488 Hemicellulose Polymers 0.000 abstract 4
- 239000000463 material Substances 0.000 abstract 3
- 239000007864 aqueous solution Substances 0.000 abstract 2
- PQUCIEFHOVEZAU-UHFFFAOYSA-N Diammonium sulfite Chemical compound [NH4+].[NH4+].[O-]S([O-])=O PQUCIEFHOVEZAU-UHFFFAOYSA-N 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 239000012670 alkaline solution Substances 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 239000012978 lignocellulosic material Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/66—Salts, e.g. alums
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/02—Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/02—Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes
- D21C3/026—Pulping cellulose-containing materials with inorganic bases or alkaline reacting compounds, e.g. sulfate processes in presence of O2, e.g. air
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/04—Pulping cellulose-containing materials with acids, acid salts or acid anhydrides
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/20—Pulping cellulose-containing materials with organic solvents or in solvent environment
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C5/00—Other processes for obtaining cellulose, e.g. cooking cotton linters ; Processes characterised by the choice of cellulose-containing starting materials
- D21C5/005—Treatment of cellulose-containing material with microorganisms or enzymes
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Paper (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Compounds Of Unknown Constitution (AREA)
Abstract
Procedimiento para la preparación de celulosa con baja concentración de lignina, caracterizado por una combinación de etapas, en que a) un material lignocelulósico es tratado con una solución acuosa que contiene un alcohol C₁₋₆ y tiene pH 10 a 14, a una temperatura inferior a 100ºC y la solución acuosa en la cual la lignina separada de la lignocelulosa esta disuelta, se separa de los sólidos que consisten en un material enriquecido en celulosa y hemicelulosa, b) la hemicelulosa es separada del material enriquecido con celulosa y hemicelulosa obtenida en la etapa a), c) el material obtenido en la etapa b) con menor concentración de hemicelulosa, es tratado en solución alcalina con un sulfito alcalino, alcalinotérreo o sulfito de amonio, tal como Na₂SO₃ y/o con oxígeno con lo cual se disuelve la lignina y se obtiene celulosa con baja concentración de lignina; y celulosa obtenida por el procedimiento.Process for the preparation of cellulose with a low concentration of lignin, characterized by a combination of stages, in which a) a lignocellulosic material is treated with an aqueous solution containing a C₁₋₆ alcohol and has pH 10 to 14, at a lower temperature at 100 ° C and the aqueous solution in which the lignin separated from the lignocellulose is dissolved, is separated from the solids consisting of a material enriched in cellulose and hemicellulose, b) the hemicellulose is separated from the material enriched with cellulose and hemicellulose obtained in the stage a), c) the material obtained in stage b) with a lower concentration of hemicellulose, is treated in alkaline solution with an alkaline, alkaline earth sulphite or ammonium sulphite, such as Na₃SO₃ and / or with oxygen whereby the lignin and cellulose with low concentration of lignin is obtained; and cellulose obtained by the process.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12166676 | 2012-05-03 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR091998A1 true AR091998A1 (en) | 2015-03-18 |
Family
ID=48446264
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP130101261A AR091998A1 (en) | 2012-05-03 | 2013-04-17 | CELLULOSE PREPARATION PROCEDURE WITH LIGNIN LOW CONCENTRATION |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US20150122429A1 (en) |
| EP (1) | EP2844796B1 (en) |
| AR (1) | AR091998A1 (en) |
| WO (1) | WO2013164234A1 (en) |
Families Citing this family (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8317975B2 (en) * | 2004-04-20 | 2012-11-27 | The Research Foundation Of The State University Of New York | Product and processes from an integrated forest biorefinery |
| US10077283B2 (en) * | 2013-11-20 | 2018-09-18 | Annikki Gmbh | Process for fractionating lignocellulosics |
| CA2944905C (en) | 2014-05-01 | 2022-05-10 | Renmatix, Inc. | Upgrading lignin from lignin-containing residues through reactive extraction |
| HUE066391T2 (en) | 2015-04-10 | 2024-07-28 | Comet Biorefining Inc | Methods and compositions for the treatment of cellulosic biomass and products produced thereby |
| CN105297510B (en) * | 2015-10-22 | 2017-06-23 | 岳阳市天成植物制浆技术研发有限公司 | A kind of Chinese traditional medicine biology agent of cold pulping |
| US11033867B2 (en) * | 2017-09-27 | 2021-06-15 | Sustainable Fiber Technologies, LLC | Aqueous lignin and hemicellulose dispersion |
| US11066588B2 (en) | 2017-11-21 | 2021-07-20 | Sustainable Fiber Technologies, LLC | Deicing composition comprising lignocellulosic byproducts |
| US11091697B2 (en) | 2017-11-29 | 2021-08-17 | Sustainable Fiber Technologies, LLC | Dust suppressant and soil stabilization composition comprising lignocellulosic byproducts |
| MX2020011986A (en) | 2018-05-10 | 2021-01-29 | Comet Biorefining Inc | Compositions comprising glucose and hemicellulose and their use. |
| CN111218490A (en) * | 2018-11-27 | 2020-06-02 | 南京理工大学 | Method for pretreatment of lignocellulose with ammonia and additives |
| EP3722501A1 (en) * | 2019-04-12 | 2020-10-14 | Lenzing Aktiengesellschaft | Method for the recovery of alkaline solution and method for producing regenerated cellulose moulded parts comprising such a method |
| CN114072012B (en) | 2019-05-10 | 2025-03-18 | 彗星生物炼制公司 | Materials and methods for producing arabinoxylan compositions |
| CN112538503A (en) * | 2019-09-20 | 2021-03-23 | 中国科学院过程工程研究所 | Novel pretreatment method for steam explosion-ammonium sulfite combined pretreatment of high-efficiency clean non-enzymatic hydrolysis fermentation inhibitor |
| US20230160141A1 (en) * | 2020-04-21 | 2023-05-25 | University Of Maryland, College Park | Extraction of delignified, cellulose-based fibers from natural plant material, and materials incorporating such fibers |
| US11572474B2 (en) | 2020-05-22 | 2023-02-07 | Sustainable Fiber Technologies, LLC | Compositions comprising lignocellulosic byproducts for tire ballasts and associated methods |
| CN114907860B (en) * | 2022-06-01 | 2023-12-01 | 中国标准化研究院 | Soil treatment agent and preparation method thereof |
| CN116676799B (en) * | 2023-06-29 | 2024-09-24 | 广东食品药品职业学院 | Preparation method and application of apocynum cellulose |
Family Cites Families (31)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US296935A (en) | 1884-04-15 | Gael febdinand dahl | ||
| US3630832A (en) | 1969-11-10 | 1971-12-28 | Int Paper Canada | Controlled alkaline sulfite pulping |
| US3954553A (en) | 1972-05-15 | 1976-05-04 | Owens-Illinois, Inc. | Non-sulfur pulping process for corrugating medium using sodium carbonate and sodium hydroxide |
| US4004967A (en) | 1972-06-22 | 1977-01-25 | Billeruds Aktiebolag | Bleaching cellulose pulp with oxygen in the presence of formaldehyde |
| WO1982001568A1 (en) | 1980-10-29 | 1982-05-13 | Renata Marton | Use of ethanol in alkaline pulping |
| NO152907C (en) | 1983-06-29 | 1985-12-11 | Peterson & Son As M | PROCEDURE FOR DELIGNIFICATION OF CHEMICAL MASS. |
| ZA877379B (en) * | 1986-10-02 | 1989-04-26 | James Fullerton Terry | Manufacture of pulp |
| FI93866B (en) | 1990-02-09 | 1995-02-28 | Sunds Defibrator Rauma Oy | Process for the preparation of sulphate pulp |
| BR9102464A (en) | 1991-06-14 | 1993-01-12 | White Martins Sa | IMPROVEMENT IN THE DESIGNIFICATION PROCESS WITH LIGNOCELLULOSIC PULP OXYGEN |
| DE69503238D1 (en) | 1994-04-28 | 1998-08-06 | Mac Millan Bloedel Ltd | BLEACHING OF CELLULAR WITH OXYGEN |
| JP2001515136A (en) | 1997-08-14 | 2001-09-18 | 隆司 渡邊 | Chemical method for lignin depolymerization |
| SE9703365D0 (en) | 1997-09-18 | 1997-09-18 | Kvaerner Pulping Tech | Method in connection with impregnation and digestion of lignocelulosic material |
| US6613192B1 (en) | 1998-03-13 | 2003-09-02 | Biopulping International, Inc. | Process for producing biokraft pulp from eucalyptus chips |
| CA2282238C (en) | 1998-10-09 | 2003-04-29 | Pulp And Paper Research Institute Of Canada | Pulping process |
| CA2318027C (en) | 1999-09-13 | 2008-07-08 | Andritz-Ahlstrom Inc. | Treating pulp with yield or strength-enhancing additive |
| EP1375734A1 (en) | 2002-06-17 | 2004-01-02 | SCA Hygiene Products GmbH | Bleached, strong sulfite chemical pulp, a process for the production thereof and products derived therefrom |
| SE0202711D0 (en) | 2002-09-12 | 2002-09-12 | Kiram Ab | Alkaline process for the manufacture of pulp using alkali metaborate as buffering alkali |
| US6923887B2 (en) | 2003-02-21 | 2005-08-02 | Alberta Research Council Inc. | Method for hydrogen peroxide bleaching of pulp using an organic solvent in the bleaching medium |
| DE10323376A1 (en) | 2003-05-21 | 2004-12-16 | Voith Paper Fiber Systems Gmbh & Co. Kg | Delignification procedure |
| AT413820B (en) | 2004-06-02 | 2006-06-15 | Chemiefaser Lenzing Ag | METHOD FOR THE PRODUCTION OF CELLULOSIC FORM BODIES |
| US7520958B2 (en) | 2005-05-24 | 2009-04-21 | International Paper Company | Modified kraft fibers |
| AT503624B1 (en) | 2006-05-10 | 2008-08-15 | Chemiefaser Lenzing Ag | PROCESS FOR THE PREPARATION OF XYLOOLIGOSACCHARIDES |
| US7824521B2 (en) | 2006-12-18 | 2010-11-02 | University Of Maine System Board Of Trustees | Process of treating a lignocellulosic material with hemicellulose pre-extraction and hemicellulose adsorption |
| US7828930B2 (en) | 2007-11-20 | 2010-11-09 | International Paper Company | Use of polysulfide in modified cooking |
| US8268125B2 (en) | 2008-03-24 | 2012-09-18 | Api Intellectual Property Holdings, Llc | Method for vapor phase pulping with alcohol and sulfur dioxide |
| TW201114906A (en) | 2009-04-30 | 2011-05-01 | Annikki Gmbh | Process for the production of carbohydrate cleavage products from a lignocellulosic material |
| TW201114907A (en) | 2009-08-06 | 2011-05-01 | Annikki Gmbh | Process for the production of carbohydrate cleavage products from a lignocellulosic material |
| US20110073264A1 (en) | 2009-08-13 | 2011-03-31 | The Research Foundation Of State University Of New York | Kraft-Pulping of Hot Water Extracted Woodchips |
| US8246779B2 (en) | 2009-09-24 | 2012-08-21 | Noram Engineering And Constructors Ltd. | Maintenance of sulfur concentration in Kraft pulp processes |
| RU2523973C1 (en) * | 2010-05-04 | 2014-07-27 | Байа Спешалти Сельюлоз Са | Method and system for pulp processing using cold caustic extraction with alkaline filtrate reuse |
| AT510346A1 (en) | 2010-09-02 | 2012-03-15 | Annikki Gmbh | lignin |
-
2013
- 2013-04-17 AR ARP130101261A patent/AR091998A1/en unknown
- 2013-04-24 EP EP13723025.6A patent/EP2844796B1/en not_active Not-in-force
- 2013-04-24 US US14/397,919 patent/US20150122429A1/en not_active Abandoned
- 2013-04-24 WO PCT/EP2013/058535 patent/WO2013164234A1/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| WO2013164234A1 (en) | 2013-11-07 |
| EP2844796A1 (en) | 2015-03-11 |
| US20150122429A1 (en) | 2015-05-07 |
| EP2844796B1 (en) | 2017-02-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FB | Suspension of granting procedure |