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AR086710A1 - PROCEDURE TO DEHYDATE A COMPOSITION CONTAINING CARBON HYDRATS - Google Patents

PROCEDURE TO DEHYDATE A COMPOSITION CONTAINING CARBON HYDRATS

Info

Publication number
AR086710A1
AR086710A1 ARP120102227A AR086710A1 AR 086710 A1 AR086710 A1 AR 086710A1 AR P120102227 A ARP120102227 A AR P120102227A AR 086710 A1 AR086710 A1 AR 086710A1
Authority
AR
Argentina
Prior art keywords
composition containing
composition
dehydate
hydrats
procedure
Prior art date
Application number
Other languages
Spanish (es)
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of AR086710A1 publication Critical patent/AR086710A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48Furfural
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48Furfural
    • C07D307/50Preparation from natural products

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Saccharide Compounds (AREA)
  • Furan Compounds (AREA)

Abstract

Un procedimiento para deshidratar una composición que contiene hidratos de carbono.Reivindicación 1: Procedimiento continuo para deshidratar una composición que contiene hidratos de carbono, caracterizado porque: i) se proporciona una composición que contiene por lo menos un material de partida que contiene hidratos de carbono, por lo menos un líquido iónico (IL), y por lo menos un solvente (LM) que, bajo presión normal (1013 mbaros), presenta un punto de ebullición de a lo sumo 120ºC, ii) la composición del paso i) se introduce en un evaporador y se la somete a una transformación y evaporación, a una temperatura que oscila entre 100 y 300ºC y a una presión de a lo sumo 500 mbaros, iii) se saca del evaporador una descarga gaseosa que contiene el producto de deshidratación, y una descarga líquida que contiene por lo menos un líquido iónico, iv) se condensa una descarga gaseosa y se la somete a una disociación, con la que se obtiene el producto de deshidratación.A method for dehydrating a composition containing carbohydrates. Claim 1: Continuous process for dehydrating a composition containing carbohydrates, characterized in that: i) a composition is provided containing at least one starting material containing carbohydrates , at least one ionic liquid (IL), and at least one solvent (LM) which, under normal pressure (1013 mbaros), has a boiling point of at most 120 ° C, ii) the composition of step i) is introduced into an evaporator and subjected to transformation and evaporation, at a temperature ranging from 100 to 300 ° C and at a pressure of at most 500 mbaros, iii) a gaseous discharge containing the dehydration product is removed from the evaporator, and a liquid discharge containing at least one ionic liquid, iv) a gaseous discharge is condensed and subjected to a dissociation, with which the dehydration product is obtained.

ARP120102227 2011-06-22 2012-06-21 PROCEDURE TO DEHYDATE A COMPOSITION CONTAINING CARBON HYDRATS AR086710A1 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
EP11170998 2011-06-22

Publications (1)

Publication Number Publication Date
AR086710A1 true AR086710A1 (en) 2014-01-15

Family

ID=46321029

Family Applications (1)

Application Number Title Priority Date Filing Date
ARP120102227 AR086710A1 (en) 2011-06-22 2012-06-21 PROCEDURE TO DEHYDATE A COMPOSITION CONTAINING CARBON HYDRATS

Country Status (10)

Country Link
EP (1) EP2723726A1 (en)
JP (1) JP2014517052A (en)
CN (1) CN103619827B (en)
AR (1) AR086710A1 (en)
BR (1) BR112013032556A2 (en)
CA (1) CA2837782A1 (en)
RU (1) RU2608609C2 (en)
TW (1) TWI548644B (en)
UY (1) UY34159A (en)
WO (1) WO2012175584A1 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9156802B2 (en) 2011-12-13 2015-10-13 Basf Se Separating off 5-hydroxymethylfurfural (HMF) from reaction solutions by steam distillation
WO2016207025A1 (en) 2015-06-24 2016-12-29 Basf Se Method for synthesizing and separating hmf
US9321744B1 (en) 2015-06-26 2016-04-26 Industrial Technology Research Institute Method for preparing 2,5-furan dicarboxylic acid
WO2019143802A1 (en) * 2018-01-17 2019-07-25 Texas Tech University System Dissolution of cellulose in ionic liquids
KR102380678B1 (en) * 2020-10-29 2022-04-01 씨제이제일제당 주식회사 Manufacturing method for solid state amino acids mixture and manufacturing system for solid state amino acids mixture

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2462433A1 (en) * 1979-08-03 1981-02-13 Bertin & Cie IMPROVEMENTS IN PROCESSES AND EQUIPMENT FOR OBTAINING FURFURAL FROM PLANT MATERIALS
DE19917178A1 (en) * 1999-04-16 2000-10-19 Karl Zeitsch Production of furfural from sulfite waste liquor involves heating by direct injection of steam, reaction by boiling under pressure, using easily separated ancillary, and complete vaporization by cooling and depressurization
DE10202838A1 (en) 2002-01-24 2003-08-07 Basf Ag Separation of acids from reaction mixtures by means of an auxiliary base that forms a liquid salt with the acid to result in two non-miscible phases with the product or solution of the product in a suitable solvent
US7393963B2 (en) * 2004-12-10 2008-07-01 Archer-Daniels-Midland Company Conversion of 2,5-(hydroxymethyl)furaldehyde to industrial derivatives, purification of the derivatives, and industrial uses therefor
US7939681B2 (en) * 2006-08-07 2011-05-10 Battelle Memorial Institute Methods for conversion of carbohydrates in ionic liquids to value-added chemicals
CN101589153A (en) 2007-01-23 2009-11-25 巴斯夫欧洲公司 Method for producing glucose by enzymatic hydrolysis of cellulose that can be pretreated with an ionic liquid containing a polyatomic anion
AU2008208870B2 (en) 2007-01-23 2013-05-02 Basf Se Method for producing glucose by enzymatic hydrolysis of cellulose that is obtained from material containing ligno-cellulose using an ionic liquid that comprises a polyatomic anion
PT103684A (en) * 2007-03-09 2008-09-09 Pedro Manuel Brito Da Silva Correia LIQUID BIOFUELS CONSTITUTED BY DIHYDROXYMETHYLFURAN, PROPANOL AND ITS PRODUCTION PROCESS FROM POLYOLES OF AGRICULTURAL ORIGIN
UA97690C2 (en) * 2007-09-07 2012-03-12 Фураникс Технолоджиз Б.В. Method for the manufacture of a mixture of 5-hydroxymethylfurfural ethers and a fuel or fuel composition comprising the ether mixture
DE102008009933A1 (en) * 2008-02-18 2009-08-20 Friedrich-Schiller-Universität Jena Preparing 5-hydroxymethylfurfural, useful e.g. to manufacture pharmaceutical products such as fungicides, comprises thermally reacting carbohydrates in ionic liquid and discharging formed 5-hydroxymethylfurfural using extracting agent
US8110667B2 (en) * 2008-04-28 2012-02-07 Battelle Memorial Institute Method for conversion of carbohydrate polymers to value-added chemical products
WO2009154566A1 (en) * 2008-06-18 2009-12-23 Agency For Science, Technology And Research Production of hydroxymethylfurfural
EP2145872A1 (en) * 2008-07-19 2010-01-20 Cognis IP Management GmbH Method for dehydrating alcohols
CN101333200B (en) * 2008-08-06 2012-05-09 安徽瑞赛生化科技有限公司 Synthetic method of 5-hydroxymethylfurfural
US9505985B2 (en) * 2009-07-01 2016-11-29 Circa Group Pty Ltd Method for converting lignocellulosic materials into useful chemicals
JP2011184420A (en) * 2010-03-11 2011-09-22 Univ Of Tokyo Method for producing monosaccharide
CN101811066A (en) * 2010-05-14 2010-08-25 天津大学 Catalyst for synthesizing 5-hydroxymethylfurfural by hexose dehydration and method for synthesizing 5-hydroxymethylfurfural

Also Published As

Publication number Publication date
CN103619827B (en) 2016-08-24
CN103619827A (en) 2014-03-05
WO2012175584A1 (en) 2012-12-27
CA2837782A1 (en) 2012-12-27
TWI548644B (en) 2016-09-11
BR112013032556A2 (en) 2016-08-16
UY34159A (en) 2013-01-03
RU2014101649A (en) 2015-07-27
RU2608609C2 (en) 2017-01-23
TW201307377A (en) 2013-02-16
EP2723726A1 (en) 2014-04-30
JP2014517052A (en) 2014-07-17

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