AR021215A1 - A METHOD FOR PREPARING AND PURIFYING A LOW MOLECULAR WEIGHT POLYETHYLENE GLYCOLBOBOXYL ACID - Google Patents
A METHOD FOR PREPARING AND PURIFYING A LOW MOLECULAR WEIGHT POLYETHYLENE GLYCOLBOBOXYL ACIDInfo
- Publication number
- AR021215A1 AR021215A1 ARP990104408A AR021215A1 AR 021215 A1 AR021215 A1 AR 021215A1 AR P990104408 A ARP990104408 A AR P990104408A AR 021215 A1 AR021215 A1 AR 021215A1
- Authority
- AR
- Argentina
- Prior art keywords
- molecular weight
- low molecular
- weight polyethylene
- preparing
- glycolboboxyl
- Prior art date
Links
- 239000002253 acid Substances 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- -1 POLYETHYLENE Polymers 0.000 title 1
- 239000004698 Polyethylene Substances 0.000 title 1
- 229920000573 polyethylene Polymers 0.000 title 1
- 229920001223 polyethylene glycol Polymers 0.000 abstract 4
- 239000002202 Polyethylene glycol Substances 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 150000001735 carboxylic acids Chemical class 0.000 abstract 3
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000000502 dialysis Methods 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 238000002523 gelfiltration Methods 0.000 abstract 1
- 229910052736 halogen Inorganic materials 0.000 abstract 1
- 150000002367 halogens Chemical class 0.000 abstract 1
- 239000000543 intermediate Substances 0.000 abstract 1
- 239000012074 organic phase Substances 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/09—Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid esters or lactones
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
- C07C67/31—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by introduction of functional groups containing oxygen only in singly bound form
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Polyethers (AREA)
- Paper (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Un método para preparar ácidos polietilenglicolcarboxílico de bajo peso molecular que comprende hacer reaccionar polietilenglicoles de bajo peso molecularcon ésteres de ácidos alifáticos monosustituidos con un halogeno en una base, y saponificar luego los productos intermediarios resultantes. Luego, los ácidospolietilenglicolcarboxílico son extraidos con una fase orgánica que contiene tolueno para separar compuestos sin reaccionar y productos secundarios. Luego, losácidos polietilenglicolcarboxílicos extraidos son acidificados y purificados por diálisis, filtracion por gel, o precipitacion.A method for preparing low molecular weight polyethylene glycol carboxylic acids comprising reacting low molecular weight polyethylene glycols with monosubstituted aliphatic acid esters with a halogen in a base, and then saponifying the resulting intermediates. Then, polyethylene glycol carboxylic acids are extracted with an organic phase containing toluene to separate unreacted compounds and by-products. Then, the polyethylene glycol carboxylic acids extracted are acidified and purified by dialysis, gel filtration, or precipitation.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US9880298P | 1998-09-02 | 1998-09-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR021215A1 true AR021215A1 (en) | 2002-07-03 |
Family
ID=22270969
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP990104408 AR021215A1 (en) | 1998-09-02 | 1999-09-02 | A METHOD FOR PREPARING AND PURIFYING A LOW MOLECULAR WEIGHT POLYETHYLENE GLYCOLBOBOXYL ACID |
Country Status (4)
| Country | Link |
|---|---|
| AR (1) | AR021215A1 (en) |
| AU (1) | AU6134699A (en) |
| TW (1) | TW474912B (en) |
| WO (1) | WO2000012458A1 (en) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8026289B2 (en) | 2008-10-21 | 2011-09-27 | E.I. Du Pont De Nemours And Company | Fluorinated polyoxyalkylene glycol diamide surfactants |
| WO2014157117A1 (en) * | 2013-03-27 | 2014-10-02 | 日油株式会社 | Purification method for polyethylene glycol having a single amino group |
| JP6935059B2 (en) * | 2017-03-30 | 2021-09-15 | 日油株式会社 | A method for purifying polyethylene glycol having one carboxyl group |
| US10745606B2 (en) | 2017-08-15 | 2020-08-18 | Saudi Arabian Oil Company | Oil-based drilling fluid compositions which include layered double hydroxides as rheology modifiers |
| US10793762B2 (en) | 2017-08-15 | 2020-10-06 | Saudi Arabian Oil Company | Layered double hydroxides for oil-based drilling fluids |
| US10988659B2 (en) | 2017-08-15 | 2021-04-27 | Saudi Arabian Oil Company | Layered double hydroxides for oil-based drilling fluids |
| CN111032818A (en) | 2017-08-15 | 2020-04-17 | 沙特阿拉伯石油公司 | Thermally stable surfactants for oil-based drilling fluids |
| US10876039B2 (en) | 2017-08-15 | 2020-12-29 | Saudi Arabian Oil Company | Thermally stable surfactants for oil based drilling fluids |
| US10640696B2 (en) | 2017-08-15 | 2020-05-05 | Saudi Arabian Oil Company | Oil-based drilling fluids for high pressure and high temperature drilling operations |
| US10647903B2 (en) | 2017-08-15 | 2020-05-12 | Saudi Arabian Oil Company | Oil-based drilling fluid compositions which include layered double hydroxides as rheology modifiers and amino amides as emulsifiers |
| US10676658B2 (en) | 2017-08-15 | 2020-06-09 | Saudi Arabian Oil Company | Oil-based drilling fluids for high pressure and high temperature drilling operations |
| JP7376850B2 (en) | 2019-03-29 | 2023-11-09 | 日油株式会社 | Method for producing terminal carboxyl group-containing polyethylene glycol and method for producing activated polyethylene glycol |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2623900A (en) * | 1948-09-01 | 1952-12-30 | Sandoz Ag | Method for the preparation of polyether acetic acids |
| FR2268006B1 (en) * | 1974-04-17 | 1980-08-14 | Huels Chemische Werke Ag |
-
1999
- 1999-09-02 AU AU61346/99A patent/AU6134699A/en not_active Abandoned
- 1999-09-02 AR ARP990104408 patent/AR021215A1/en unknown
- 1999-09-02 WO PCT/US1999/020135 patent/WO2000012458A1/en not_active Ceased
-
2000
- 2000-03-01 TW TW88115070A patent/TW474912B/en not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| TW474912B (en) | 2002-02-01 |
| AU6134699A (en) | 2000-03-21 |
| WO2000012458A1 (en) | 2000-03-09 |
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