NO324840B1 - Fremgangsmate for fremstilling av baret koboltkatalysator og forloper for denne, og anvendelse av denne ved fremstilling av hydrokarboner. - Google Patents

Fremgangsmate for fremstilling av baret koboltkatalysator og forloper for denne, og anvendelse av denne ved fremstilling av hydrokarboner. Download PDF

Info

Publication number: NO324840B1
Authority: NO; Norway
Prior art keywords: catalyst; weight; range; dough; particle size
Prior art date: 2000-07-14

Application number

NO20030160A

Other languages

English (en)

Norwegian (no)

Other versions

NO20030160D0 (no

NO20030160L (no

Inventor

Gerardus Petrus Lambert Niesen

Johannes Jacobus Ma Vlaanderen

Hans Michiel Huisman

Original Assignee

Shell Int Research

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

2000-07-14

Filing date

2003-01-13

Publication date

2007-12-17

2003-01-13 Application filed by Shell Int Research filed Critical Shell Int Research

2003-01-13 Publication of NO20030160D0 publication Critical patent/NO20030160D0/no

2003-01-13 Publication of NO20030160L publication Critical patent/NO20030160L/no

2007-12-17 Publication of NO324840B1 publication Critical patent/NO324840B1/no

Links

239000003054 catalyst Substances 0.000 title claims description 81
238000000034 method Methods 0.000 title claims description 38
229910017052 cobalt Inorganic materials 0.000 title claims description 34
239000010941 cobalt Substances 0.000 title claims description 34
GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 title claims description 34
229930195733 hydrocarbon Natural products 0.000 title claims description 26
150000002430 hydrocarbons Chemical class 0.000 title claims description 26
238000004519 manufacturing process Methods 0.000 title claims description 14
239000002243 precursor Substances 0.000 title claims description 9
238000002360 preparation method Methods 0.000 title description 3
239000002245 particle Substances 0.000 claims description 59
239000002002 slurry Substances 0.000 claims description 30
GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 26
239000001257 hydrogen Substances 0.000 claims description 21
229910052739 hydrogen Inorganic materials 0.000 claims description 21
239000000203 mixture Substances 0.000 claims description 21
UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 19
239000007787 solid Substances 0.000 claims description 15
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
238000001354 calcination Methods 0.000 claims description 11
UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims description 10
229910002091 carbon monoxide Inorganic materials 0.000 claims description 10
150000001875 compounds Chemical class 0.000 claims description 4
238000001694 spray drying Methods 0.000 claims description 4
229910052751 metal Inorganic materials 0.000 description 25
239000002184 metal Substances 0.000 description 25
230000015572 biosynthetic process Effects 0.000 description 19
239000007789 gas Substances 0.000 description 18
238000003786 synthesis reaction Methods 0.000 description 18
239000007788 liquid Substances 0.000 description 11
238000006243 chemical reaction Methods 0.000 description 9
IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 7
239000000843 powder Substances 0.000 description 7
239000004215 Carbon black (E152) Substances 0.000 description 6
239000012018 catalyst precursor Substances 0.000 description 6
238000002156 mixing Methods 0.000 description 6
239000012071 phase Substances 0.000 description 6
238000001035 drying Methods 0.000 description 5
230000000694 effects Effects 0.000 description 5
230000001976 improved effect Effects 0.000 description 5
239000011572 manganese Substances 0.000 description 5
PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 4
238000004898 kneading Methods 0.000 description 4
229910052748 manganese Inorganic materials 0.000 description 4
VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 4
239000007858 starting material Substances 0.000 description 4
229910052720 vanadium Inorganic materials 0.000 description 4
GPPXJZIENCGNKB-UHFFFAOYSA-N vanadium Chemical compound [V]#[V] GPPXJZIENCGNKB-UHFFFAOYSA-N 0.000 description 4
230000005587 bubbling Effects 0.000 description 3
125000004432 carbon atom Chemical group C* 0.000 description 3
239000010419 fine particle Substances 0.000 description 3
238000011065 in-situ storage Methods 0.000 description 3
150000002739 metals Chemical class 0.000 description 3
229910052757 nitrogen Inorganic materials 0.000 description 3
239000000376 reactant Substances 0.000 description 3
239000011949 solid catalyst Substances 0.000 description 3
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 2
VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
238000001311 chemical methods and process Methods 0.000 description 2
229910001873 dinitrogen Inorganic materials 0.000 description 2
238000000227 grinding Methods 0.000 description 2
238000010438 heat treatment Methods 0.000 description 2
150000002431 hydrogen Chemical class 0.000 description 2
239000000463 material Substances 0.000 description 2
238000009740 moulding (composite fabrication) Methods 0.000 description 2
239000000047 product Substances 0.000 description 2
229910052707 ruthenium Inorganic materials 0.000 description 2
QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
238000004438 BET method Methods 0.000 description 1
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
229910021503 Cobalt(II) hydroxide Inorganic materials 0.000 description 1
241000403354 Microplus Species 0.000 description 1
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 1
150000001242 acetic acid derivatives Chemical class 0.000 description 1
230000003213 activating effect Effects 0.000 description 1
230000002730 additional effect Effects 0.000 description 1
238000013019 agitation Methods 0.000 description 1
PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
239000006227 byproduct Substances 0.000 description 1
238000004364 calculation method Methods 0.000 description 1
229910002092 carbon dioxide Inorganic materials 0.000 description 1
239000001569 carbon dioxide Substances 0.000 description 1
150000004649 carbonic acid derivatives Chemical class 0.000 description 1
230000003197 catalytic effect Effects 0.000 description 1
230000000052 comparative effect Effects 0.000 description 1
239000003085 diluting agent Substances 0.000 description 1
239000011363 dried mixture Substances 0.000 description 1
238000001914 filtration Methods 0.000 description 1
239000008240 homogeneous mixture Substances 0.000 description 1
238000005984 hydrogenation reaction Methods 0.000 description 1
230000007062 hydrolysis Effects 0.000 description 1
238000006460 hydrolysis reaction Methods 0.000 description 1
150000004679 hydroxides Chemical class 0.000 description 1
239000011261 inert gas Substances 0.000 description 1
239000004615 ingredient Substances 0.000 description 1
229910052742 iron Inorganic materials 0.000 description 1
239000007791 liquid phase Substances 0.000 description 1
WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
229910052759 nickel Inorganic materials 0.000 description 1
150000002823 nitrates Chemical class 0.000 description 1
QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
230000003287 optical effect Effects 0.000 description 1
229910052760 oxygen Inorganic materials 0.000 description 1
239000001301 oxygen Substances 0.000 description 1
230000000737 periodic effect Effects 0.000 description 1
229910052702 rhenium Inorganic materials 0.000 description 1
WUAPFZMCVAUBPE-UHFFFAOYSA-N rhenium atom Chemical compound [Re] WUAPFZMCVAUBPE-UHFFFAOYSA-N 0.000 description 1
150000003839 salts Chemical class 0.000 description 1
229910052706 scandium Inorganic materials 0.000 description 1
SIXSYDAISGFNSX-UHFFFAOYSA-N scandium atom Chemical compound [Sc] SIXSYDAISGFNSX-UHFFFAOYSA-N 0.000 description 1
238000007493 shaping process Methods 0.000 description 1
239000000377 silicon dioxide Substances 0.000 description 1
239000011343 solid material Substances 0.000 description 1
239000007921 spray Substances 0.000 description 1
238000005507 spraying Methods 0.000 description 1
229910052717 sulfur Inorganic materials 0.000 description 1
239000011593 sulfur Substances 0.000 description 1
XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 1
229910052726 zirconium Inorganic materials 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
- C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
- C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
- C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
- C10G2/331—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals
- C10G2/332—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals of the iron-group
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/74—Iron group metals
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J23/889—Manganese, technetium or rhenium
- B01J23/8892—Manganese
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
- B01J37/0027—Powdering
- B01J37/0045—Drying a slurry, e.g. spray drying
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying

Landscapes

Chemical & Material Sciences (AREA)
Engineering & Computer Science (AREA)
Organic Chemistry (AREA)
Chemical Kinetics & Catalysis (AREA)
Materials Engineering (AREA)
Oil, Petroleum & Natural Gas (AREA)
General Chemical & Material Sciences (AREA)
Catalysts (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

NO20030160A 2000-07-14 2003-01-13 Fremgangsmate for fremstilling av baret koboltkatalysator og forloper for denne, og anvendelse av denne ved fremstilling av hydrokarboner. NO324840B1 (no)

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
EP00305993		2000-07-14
PCT/EP2001/007938 WO2002005958A1 (en)	2000-07-14	2001-07-10	A catalyst support, a supported group viii metal catalyst and a precursor thereof, processes for their preparation, and a use of the supported group viii metal catalyst

Publications (3)

Publication Number	Publication Date
NO20030160D0 NO20030160D0 (no)	2003-01-13
NO20030160L NO20030160L (no)	2003-01-13
NO324840B1 true NO324840B1 (no)	2007-12-17

Family

ID=8173122

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NO20030160A NO324840B1 (no)	2000-07-14	2003-01-13	Fremgangsmate for fremstilling av baret koboltkatalysator og forloper for denne, og anvendelse av denne ved fremstilling av hydrokarboner.

Country Status (16)

Country	Link
US (1)	US7282467B2 (es)
EP (1)	EP1301278B1 (es)
AR (1)	AR029708A1 (es)
AT (1)	ATE342129T1 (es)
AU (2)	AU8582301A (es)
CA (1)	CA2415638A1 (es)
DE (1)	DE60123791T2 (es)
DZ (1)	DZ3374A1 (es)
ES (1)	ES2272530T3 (es)
MX (1)	MXPA03000320A (es)
MY (1)	MY138918A (es)
NO (1)	NO324840B1 (es)
NZ (1)	NZ523611A (es)
RU (1)	RU2282500C2 (es)
WO (1)	WO2002005958A1 (es)
ZA (1)	ZA200300367B (es)

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CA2415638A1 (en)	2000-07-14	2002-01-24	Shell Internationale Research Maatschappij B.V.	A catalyst support, a supported group viii metal catalyst and a precursor thereof, processes for their preparation, and a use of the supported group viii metal catalyst
US7045670B2 (en) *	2003-09-03	2006-05-16	Synfuels International, Inc.	Process for liquid phase hydrogenation
WO2007068731A1 (en) *	2005-12-16	2007-06-21	Shell Internationale Research Maatschappij B.V.	Process for preparing a hydrocarbon synthesis catalyst
US8394864B2 (en) *	2008-04-15	2013-03-12	Sasol Technology (Proprietary) Limited	Catalysts
MY171504A (en) *	2013-07-24	2019-10-16	Shell Int Research	Process for preparing a chlorine comprising catalyst, the prepared catalyst, and its use
US12000333B2 (en)	2021-05-14	2024-06-04	AMOGY, Inc.	Systems and methods for processing ammonia
US11724245B2 (en)	2021-08-13	2023-08-15	Amogy Inc.	Integrated heat exchanger reactors for renewable fuel delivery systems
AU2022290866A1 (en)	2021-06-11	2023-12-21	Amogy Inc.	Systems and methods for processing ammonia
US11539063B1 (en)	2021-08-17	2022-12-27	Amogy Inc.	Systems and methods for processing hydrogen
US11840447B1 (en)	2022-10-06	2023-12-12	Amogy Inc.	Systems and methods of processing ammonia
US11866328B1 (en)	2022-10-21	2024-01-09	Amogy Inc.	Systems and methods for processing ammonia
US11795055B1 (en)	2022-10-21	2023-10-24	Amogy Inc.	Systems and methods for processing ammonia
WO2025006628A2 (en)	2023-06-26	2025-01-02	Amogy Inc.	Compositions and methods for treating porous materials

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NZ504988A (en) *	1997-12-30	2001-08-31	Shell Int Research	Cobalt and titania based fisher-tropsch catalyst
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GC0000360A (en) *	2000-05-04	2007-03-31	Shell Int Research	A catalyst support and a supported metal catalyst, a process for their preparation, and the use of the catalyst
CA2415638A1 (en)	2000-07-14	2002-01-24	Shell Internationale Research Maatschappij B.V.	A catalyst support, a supported group viii metal catalyst and a precursor thereof, processes for their preparation, and a use of the supported group viii metal catalyst

2001
- 2001-07-10 CA CA002415638A patent/CA2415638A1/en not_active Abandoned
- 2001-07-10 WO PCT/EP2001/007938 patent/WO2002005958A1/en not_active Ceased
- 2001-07-10 AU AU8582301A patent/AU8582301A/xx active Pending
- 2001-07-10 RU RU2003104353/04A patent/RU2282500C2/ru not_active IP Right Cessation
- 2001-07-10 US US10/332,094 patent/US7282467B2/en not_active Expired - Fee Related
- 2001-07-10 MX MXPA03000320A patent/MXPA03000320A/es active IP Right Grant
- 2001-07-10 NZ NZ523611A patent/NZ523611A/en unknown
- 2001-07-10 ES ES01965104T patent/ES2272530T3/es not_active Expired - Lifetime
- 2001-07-10 AU AU2001285823A patent/AU2001285823B2/en not_active Ceased
- 2001-07-10 AT AT01965104T patent/ATE342129T1/de not_active IP Right Cessation
- 2001-07-10 DZ DZ013374A patent/DZ3374A1/xx active
- 2001-07-10 DE DE60123791T patent/DE60123791T2/de not_active Expired - Lifetime
- 2001-07-10 EP EP01965104A patent/EP1301278B1/en not_active Expired - Lifetime
- 2001-07-12 MY MYPI20013323A patent/MY138918A/en unknown
- 2001-07-12 AR ARP010103308A patent/AR029708A1/es active IP Right Grant
2003
- 2003-01-13 NO NO20030160A patent/NO324840B1/no not_active IP Right Cessation
- 2003-01-14 ZA ZA200300367A patent/ZA200300367B/en unknown

Also Published As

Publication number	Publication date
EP1301278B1 (en)	2006-10-11
NZ523611A (en)	2004-09-24
DE60123791T2 (de)	2007-08-23
US7282467B2 (en)	2007-10-16
ZA200300367B (en)	2004-04-02
ES2272530T3 (es)	2007-05-01
AU8582301A (en)	2002-01-30
US20030158271A1 (en)	2003-08-21
RU2282500C2 (ru)	2006-08-27
MY138918A (en)	2009-08-28
AU2001285823B2 (en)	2004-09-23
EP1301278A1 (en)	2003-04-16
NO20030160D0 (no)	2003-01-13
AR029708A1 (es)	2003-07-10
MXPA03000320A (es)	2004-04-05
DE60123791D1 (de)	2006-11-23
ATE342129T1 (de)	2006-11-15
NO20030160L (no)	2003-01-13
DZ3374A1 (fr)	2002-01-24
CA2415638A1 (en)	2002-01-24
WO2002005958A1 (en)	2002-01-24

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JP2000104078A (ja)	2000-04-11	炭素ガスを含む低級炭化水素ガスから液体炭化水素油を製造する方法
CN101801525A (zh)	2010-08-11	费-托催化剂的稳定方法
EP2076331A1 (en)	2009-07-08	Process and catalyst for hydrocarbon conversion
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