NO20032335D0 - Process for Preparation of Alkoxylated Carbonyl Compounds by Enanionic Oxidation Method Using Cathodic Coupler Reaction for Organic Synthesis - Google Patents
Process for Preparation of Alkoxylated Carbonyl Compounds by Enanionic Oxidation Method Using Cathodic Coupler Reaction for Organic SynthesisInfo
- Publication number
- NO20032335D0 NO20032335D0 NO20032335A NO20032335A NO20032335D0 NO 20032335 D0 NO20032335 D0 NO 20032335D0 NO 20032335 A NO20032335 A NO 20032335A NO 20032335 A NO20032335 A NO 20032335A NO 20032335 D0 NO20032335 D0 NO 20032335D0
- Authority
- NO
- Norway
- Prior art keywords
- alkyl
- compounds
- cathodic
- enanionic
- preparation
- Prior art date
Links
- 230000003647 oxidation Effects 0.000 title abstract 3
- 238000007254 oxidation reaction Methods 0.000 title abstract 3
- 150000001728 carbonyl compounds Chemical class 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 2
- 238000006243 chemical reaction Methods 0.000 title 1
- 238000002360 preparation method Methods 0.000 title 1
- 238000003786 synthesis reaction Methods 0.000 title 1
- 125000004169 (C1-C6) alkyl group Chemical group 0.000 abstract 6
- 150000001875 compounds Chemical class 0.000 abstract 5
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- FKLJPTJMIBLJAV-UHFFFAOYSA-N Compound IV Chemical compound O1N=C(C)C=C1CCCCCCCOC1=CC=C(C=2OCCN=2)C=C1 FKLJPTJMIBLJAV-UHFFFAOYSA-N 0.000 abstract 1
- 239000003792 electrolyte Substances 0.000 abstract 1
- 238000006056 electrooxidation reaction Methods 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B3/00—Electrolytic production of organic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A method for producing alcoxylated carbonyl compounds of general formula (I) (compounds I): R<1>aR<2>C(OR<3>)b wherein R<1>, R<2 >represent hydrogen or C1-C6-alkyl, R<3 >independently means C1-C6-alkyl, a is 0 or 1, b 2 or 3 with the proviso that the sum of a and b is 3, by means of anodic oxidation of germinal dialcoxy compounds of general formula (II) (compounds II) wherein R<4>, R<5>, R<6>, R<7 >represent hydrogen or C1-C6-alkyl, R<5>, R<6 >represent C1-C6-alkyl or C1-C6-alcoxy, in the presence of a C1-C6-alkyl alcohol (compounds III). A usual compound (compound IV) is used as a cathodic depolarizer suitable for electrochemical oxidation. The anodic oxidation and cathodic reduction is carried out in an undivided electrolyte cell in the presence of C1-C6-alkyl alcohols.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10058304A DE10058304A1 (en) | 2000-11-24 | 2000-11-24 | Process for the preparation of alkoxylated carbonyl compounds by an anodic oxidation process using the cathodic coupling reaction for organic synthesis |
| PCT/EP2001/013587 WO2002042524A2 (en) | 2000-11-24 | 2001-11-22 | Method for producing alcoxylated carbonyl compounds by an anodic oxidation method using a cathodic coupled reaction for organic synthesis |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| NO20032335D0 true NO20032335D0 (en) | 2003-05-23 |
| NO20032335L NO20032335L (en) | 2003-07-14 |
Family
ID=7664478
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20032335A NO20032335L (en) | 2000-11-24 | 2003-05-23 | Process for Preparation of Alkoxylated Carbonyl Compounds by Enanionic Oxidation Method Using Catonic Coupler Reaction for Organic Synthesis |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US6822124B2 (en) |
| EP (1) | EP1348043B1 (en) |
| JP (1) | JP3906153B2 (en) |
| CN (1) | CN1329556C (en) |
| AT (1) | ATE290616T1 (en) |
| AU (1) | AU2002224874A1 (en) |
| CA (1) | CA2429450A1 (en) |
| DE (2) | DE10058304A1 (en) |
| ES (1) | ES2238501T3 (en) |
| NO (1) | NO20032335L (en) |
| WO (1) | WO2002042524A2 (en) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10146566A1 (en) | 2001-09-21 | 2003-07-17 | Basf Ag | Process for the preparation of orthocarboxylic acid trialkyl esters |
| DE10355087A1 (en) * | 2003-11-24 | 2005-06-09 | Basf Ag | Process for the electrochemical preparation of a crystalline porous organometallic framework |
| FR2910784B1 (en) | 2006-12-27 | 2009-02-20 | Arkema France | USE OF COMPOUNDS FOR PRESERVATION OF THE HUMAN OR ANIMAL BODY AND COMPOSITIONS COMPRISING SAME |
| DE102007008668A1 (en) * | 2007-02-20 | 2008-08-21 | Tesa Ag | Method of marking or marking surfaces |
| ES2719585T3 (en) * | 2010-02-12 | 2019-07-11 | Basf Se | Procedure for the preparation of 4-isopropylcyclohexylmethanol |
| US8889920B2 (en) * | 2010-02-12 | 2014-11-18 | Basf Se | Process for preparing 4-isopropylcyclohexylmethanol |
| KR20150023709A (en) | 2012-06-15 | 2015-03-05 | 바스프 에스이 | Anodic oxidation of organic substrates in the presence of nucleophiles |
| CN107473945B (en) * | 2016-06-08 | 2020-09-01 | 中国科学院大连化学物理研究所 | Method for preparing tetramethoxymethane by catalyzing direct oxidation esterification of methanol |
| CN106591877A (en) * | 2016-11-14 | 2017-04-26 | 江苏科技大学 | Coupling agent with convertible central atoms and preparing method of coupling agent |
| CN109983162A (en) * | 2016-11-24 | 2019-07-05 | 阿凡田知识中心有限公司 | Process for processing furan-2,5-dicarboxylic acid compositions |
| DE102017113141A1 (en) * | 2017-06-14 | 2018-12-20 | Westfälische Wilhelms-Universität Münster | Electrolyte for lithium-ion batteries |
| DE102017012021A1 (en) | 2017-12-22 | 2019-06-27 | Friedrich-Schiller-Universität Jena | Acetal electrolyte |
| JP7105418B2 (en) * | 2018-02-08 | 2022-07-25 | Eneos株式会社 | Apparatus and method for producing cis-disubstituted non-aromatic compound |
| CN108677210B (en) * | 2018-04-17 | 2019-10-29 | 大连理工大学 | A kind of method of ketone and carboxylic acid step hydrogenation and esterification in electrochemical hydrogen pump reactor |
| CN112195481B (en) * | 2020-11-02 | 2021-12-10 | 上海漫关越水处理有限公司 | Method for synthesizing tetramethoxyethane by membrane electrolysis |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3000243A1 (en) | 1980-01-05 | 1981-07-09 | Hoechst Ag, 6230 Frankfurt | Electrochemical alkoxylation of aliphatic ether(s) - using vitreous carbon or platinum anode(s) |
| US4450055A (en) * | 1983-03-30 | 1984-05-22 | Celanese Corporation | Electrogenerative partial oxidation of organic compounds |
| US4648948A (en) * | 1985-05-23 | 1987-03-10 | Meshbesher Thomas M | Electrogenerative oxidation of lower alcohols to useful products |
| US5223102A (en) * | 1992-03-03 | 1993-06-29 | E. I. Du Pont De Nemours And Company | Process for the electrooxidation of methanol to formaldehyde and methylal |
| DE19618854A1 (en) * | 1996-05-10 | 1997-11-13 | Basf Ag | Process for the production of phthalides |
| DE19741423A1 (en) * | 1997-09-19 | 1999-03-25 | Basf Ag | Pure phthalide or derivative preparation in high yield |
-
2000
- 2000-11-24 DE DE10058304A patent/DE10058304A1/en active Pending
-
2001
- 2001-11-22 EP EP01994702A patent/EP1348043B1/en not_active Expired - Lifetime
- 2001-11-22 CN CNB018194397A patent/CN1329556C/en not_active Expired - Fee Related
- 2001-11-22 DE DE50105570T patent/DE50105570D1/en not_active Expired - Fee Related
- 2001-11-22 CA CA002429450A patent/CA2429450A1/en not_active Abandoned
- 2001-11-22 AT AT01994702T patent/ATE290616T1/en not_active IP Right Cessation
- 2001-11-22 US US10/432,249 patent/US6822124B2/en not_active Expired - Fee Related
- 2001-11-22 ES ES01994702T patent/ES2238501T3/en not_active Expired - Lifetime
- 2001-11-22 JP JP2002545221A patent/JP3906153B2/en not_active Expired - Fee Related
- 2001-11-22 AU AU2002224874A patent/AU2002224874A1/en not_active Abandoned
- 2001-11-22 WO PCT/EP2001/013587 patent/WO2002042524A2/en not_active Ceased
-
2003
- 2003-05-23 NO NO20032335A patent/NO20032335L/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| NO20032335L (en) | 2003-07-14 |
| JP3906153B2 (en) | 2007-04-18 |
| EP1348043B1 (en) | 2005-03-09 |
| EP1348043A2 (en) | 2003-10-01 |
| US6822124B2 (en) | 2004-11-23 |
| CN1329556C (en) | 2007-08-01 |
| AU2002224874A1 (en) | 2002-06-03 |
| CA2429450A1 (en) | 2002-05-30 |
| WO2002042524A2 (en) | 2002-05-30 |
| ES2238501T3 (en) | 2005-09-01 |
| DE50105570D1 (en) | 2005-04-14 |
| WO2002042524A3 (en) | 2003-03-13 |
| US20040026263A1 (en) | 2004-02-12 |
| JP2004514791A (en) | 2004-05-20 |
| CN1476491A (en) | 2004-02-18 |
| DE10058304A1 (en) | 2002-05-29 |
| ATE290616T1 (en) | 2005-03-15 |
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