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NO20032335D0 - Process for Preparation of Alkoxylated Carbonyl Compounds by Enanionic Oxidation Method Using Cathodic Coupler Reaction for Organic Synthesis - Google Patents

Process for Preparation of Alkoxylated Carbonyl Compounds by Enanionic Oxidation Method Using Cathodic Coupler Reaction for Organic Synthesis

Info

Publication number
NO20032335D0
NO20032335D0 NO20032335A NO20032335A NO20032335D0 NO 20032335 D0 NO20032335 D0 NO 20032335D0 NO 20032335 A NO20032335 A NO 20032335A NO 20032335 A NO20032335 A NO 20032335A NO 20032335 D0 NO20032335 D0 NO 20032335D0
Authority
NO
Norway
Prior art keywords
alkyl
compounds
cathodic
enanionic
preparation
Prior art date
Application number
NO20032335A
Other languages
Norwegian (no)
Other versions
NO20032335L (en
Inventor
Hermann Puetter
Andreas Fischer
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of NO20032335D0 publication Critical patent/NO20032335D0/en
Publication of NO20032335L publication Critical patent/NO20032335L/en

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Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00Electrolytic production of organic compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

A method for producing alcoxylated carbonyl compounds of general formula (I) (compounds I): R<1>aR<2>C(OR<3>)b wherein R<1>, R<2 >represent hydrogen or C1-C6-alkyl, R<3 >independently means C1-C6-alkyl, a is 0 or 1, b 2 or 3 with the proviso that the sum of a and b is 3, by means of anodic oxidation of germinal dialcoxy compounds of general formula (II) (compounds II) wherein R<4>, R<5>, R<6>, R<7 >represent hydrogen or C1-C6-alkyl, R<5>, R<6 >represent C1-C6-alkyl or C1-C6-alcoxy, in the presence of a C1-C6-alkyl alcohol (compounds III). A usual compound (compound IV) is used as a cathodic depolarizer suitable for electrochemical oxidation. The anodic oxidation and cathodic reduction is carried out in an undivided electrolyte cell in the presence of C1-C6-alkyl alcohols.
NO20032335A 2000-11-24 2003-05-23 Process for Preparation of Alkoxylated Carbonyl Compounds by Enanionic Oxidation Method Using Catonic Coupler Reaction for Organic Synthesis NO20032335L (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10058304A DE10058304A1 (en) 2000-11-24 2000-11-24 Process for the preparation of alkoxylated carbonyl compounds by an anodic oxidation process using the cathodic coupling reaction for organic synthesis
PCT/EP2001/013587 WO2002042524A2 (en) 2000-11-24 2001-11-22 Method for producing alcoxylated carbonyl compounds by an anodic oxidation method using a cathodic coupled reaction for organic synthesis

Publications (2)

Publication Number Publication Date
NO20032335D0 true NO20032335D0 (en) 2003-05-23
NO20032335L NO20032335L (en) 2003-07-14

Family

ID=7664478

Family Applications (1)

Application Number Title Priority Date Filing Date
NO20032335A NO20032335L (en) 2000-11-24 2003-05-23 Process for Preparation of Alkoxylated Carbonyl Compounds by Enanionic Oxidation Method Using Catonic Coupler Reaction for Organic Synthesis

Country Status (11)

Country Link
US (1) US6822124B2 (en)
EP (1) EP1348043B1 (en)
JP (1) JP3906153B2 (en)
CN (1) CN1329556C (en)
AT (1) ATE290616T1 (en)
AU (1) AU2002224874A1 (en)
CA (1) CA2429450A1 (en)
DE (2) DE10058304A1 (en)
ES (1) ES2238501T3 (en)
NO (1) NO20032335L (en)
WO (1) WO2002042524A2 (en)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10146566A1 (en) 2001-09-21 2003-07-17 Basf Ag Process for the preparation of orthocarboxylic acid trialkyl esters
DE10355087A1 (en) * 2003-11-24 2005-06-09 Basf Ag Process for the electrochemical preparation of a crystalline porous organometallic framework
FR2910784B1 (en) 2006-12-27 2009-02-20 Arkema France USE OF COMPOUNDS FOR PRESERVATION OF THE HUMAN OR ANIMAL BODY AND COMPOSITIONS COMPRISING SAME
DE102007008668A1 (en) * 2007-02-20 2008-08-21 Tesa Ag Method of marking or marking surfaces
ES2719585T3 (en) * 2010-02-12 2019-07-11 Basf Se Procedure for the preparation of 4-isopropylcyclohexylmethanol
US8889920B2 (en) * 2010-02-12 2014-11-18 Basf Se Process for preparing 4-isopropylcyclohexylmethanol
KR20150023709A (en) 2012-06-15 2015-03-05 바스프 에스이 Anodic oxidation of organic substrates in the presence of nucleophiles
CN107473945B (en) * 2016-06-08 2020-09-01 中国科学院大连化学物理研究所 Method for preparing tetramethoxymethane by catalyzing direct oxidation esterification of methanol
CN106591877A (en) * 2016-11-14 2017-04-26 江苏科技大学 Coupling agent with convertible central atoms and preparing method of coupling agent
CN109983162A (en) * 2016-11-24 2019-07-05 阿凡田知识中心有限公司 Process for processing furan-2,5-dicarboxylic acid compositions
DE102017113141A1 (en) * 2017-06-14 2018-12-20 Westfälische Wilhelms-Universität Münster Electrolyte for lithium-ion batteries
DE102017012021A1 (en) 2017-12-22 2019-06-27 Friedrich-Schiller-Universität Jena Acetal electrolyte
JP7105418B2 (en) * 2018-02-08 2022-07-25 Eneos株式会社 Apparatus and method for producing cis-disubstituted non-aromatic compound
CN108677210B (en) * 2018-04-17 2019-10-29 大连理工大学 A kind of method of ketone and carboxylic acid step hydrogenation and esterification in electrochemical hydrogen pump reactor
CN112195481B (en) * 2020-11-02 2021-12-10 上海漫关越水处理有限公司 Method for synthesizing tetramethoxyethane by membrane electrolysis

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3000243A1 (en) 1980-01-05 1981-07-09 Hoechst Ag, 6230 Frankfurt Electrochemical alkoxylation of aliphatic ether(s) - using vitreous carbon or platinum anode(s)
US4450055A (en) * 1983-03-30 1984-05-22 Celanese Corporation Electrogenerative partial oxidation of organic compounds
US4648948A (en) * 1985-05-23 1987-03-10 Meshbesher Thomas M Electrogenerative oxidation of lower alcohols to useful products
US5223102A (en) * 1992-03-03 1993-06-29 E. I. Du Pont De Nemours And Company Process for the electrooxidation of methanol to formaldehyde and methylal
DE19618854A1 (en) * 1996-05-10 1997-11-13 Basf Ag Process for the production of phthalides
DE19741423A1 (en) * 1997-09-19 1999-03-25 Basf Ag Pure phthalide or derivative preparation in high yield

Also Published As

Publication number Publication date
NO20032335L (en) 2003-07-14
JP3906153B2 (en) 2007-04-18
EP1348043B1 (en) 2005-03-09
EP1348043A2 (en) 2003-10-01
US6822124B2 (en) 2004-11-23
CN1329556C (en) 2007-08-01
AU2002224874A1 (en) 2002-06-03
CA2429450A1 (en) 2002-05-30
WO2002042524A2 (en) 2002-05-30
ES2238501T3 (en) 2005-09-01
DE50105570D1 (en) 2005-04-14
WO2002042524A3 (en) 2003-03-13
US20040026263A1 (en) 2004-02-12
JP2004514791A (en) 2004-05-20
CN1476491A (en) 2004-02-18
DE10058304A1 (en) 2002-05-29
ATE290616T1 (en) 2005-03-15

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