[go: up one dir, main page]

NO165914C - PROCEDURE FOR THE PREPARATION OF PURE DIMETYLETS. - Google Patents

PROCEDURE FOR THE PREPARATION OF PURE DIMETYLETS.

Info

Publication number
NO165914C
NO165914C NO874787A NO874787A NO165914C NO 165914 C NO165914 C NO 165914C NO 874787 A NO874787 A NO 874787A NO 874787 A NO874787 A NO 874787A NO 165914 C NO165914 C NO 165914C
Authority
NO
Norway
Prior art keywords
dimethyl ether
pure
dimetylets
procedure
preparation
Prior art date
Application number
NO874787A
Other languages
Norwegian (no)
Other versions
NO874787D0 (en
NO165914B (en
NO874787L (en
Inventor
Horst Dornhagen
Hartmut Hammer
Ewald Meisenburg
Bernd Haas
Original Assignee
Union Rheinische Braunkohlen
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19863642845 external-priority patent/DE3642845A1/en
Application filed by Union Rheinische Braunkohlen filed Critical Union Rheinische Braunkohlen
Publication of NO874787D0 publication Critical patent/NO874787D0/en
Publication of NO874787L publication Critical patent/NO874787L/en
Publication of NO165914B publication Critical patent/NO165914B/en
Publication of NO165914C publication Critical patent/NO165914C/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/09—Preparation of ethers by dehydration of compounds containing hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Mechanical Treatment Of Semiconductor (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Pure dimethyl ether is prepared by catalytic dehydration of methanol over a gamma -Al2O3 catalyst which preferably contains small amounts of SiO2 and purification of the dehydration product by addition thereof to a distillation column to obtain pure dimethyl ether on certain plates of this column and taking off the pure dimethyl ether and impurities above certain plates of the same column.
NO874787A 1986-11-18 1987-11-17 PROCEDURE FOR THE PREPARATION OF PURE DIMETYLETS. NO165914C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
AU65506/86A AU603070B2 (en) 1986-11-18 1986-11-18 Process for the purification of dimethylether
DE19863642845 DE3642845A1 (en) 1986-12-16 1986-12-16 Process for the preparation of dimethyl ether and catalyst used for this purpose
BR8606293A BR8606293A (en) 1986-11-18 1986-12-19 PROCESS FOR PURIFICATION OF DIMETHYL ETER

Publications (4)

Publication Number Publication Date
NO874787D0 NO874787D0 (en) 1987-11-17
NO874787L NO874787L (en) 1988-05-19
NO165914B NO165914B (en) 1991-01-21
NO165914C true NO165914C (en) 1991-05-02

Family

ID=27155597

Family Applications (1)

Application Number Title Priority Date Filing Date
NO874787A NO165914C (en) 1986-11-18 1987-11-17 PROCEDURE FOR THE PREPARATION OF PURE DIMETYLETS.

Country Status (20)

Country Link
EP (2) EP0270852B1 (en)
JP (1) JPS63208546A (en)
CN (1) CN1036199A (en)
AT (1) ATE71354T1 (en)
AU (1) AU603070B2 (en)
BR (1) BR8606293A (en)
CA (1) CA1322767C (en)
DD (1) DD270901A1 (en)
DE (1) DE3775902D1 (en)
DK (1) DK603187A (en)
ES (1) ES2003076T3 (en)
FI (1) FI875046A7 (en)
GR (1) GR880300102T1 (en)
HU (1) HUT45956A (en)
IN (1) IN168048B (en)
NO (1) NO165914C (en)
NZ (1) NZ222597A (en)
PL (1) PL268856A1 (en)
SU (1) SU1602392A3 (en)
YU (1) YU208087A (en)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3876790D1 (en) * 1988-05-04 1993-01-28 Rwe Dea Ag IMPROVED METHOD FOR PRODUCING PURE DIMETHYL ETHER.
JP2819600B2 (en) * 1989-04-10 1998-10-30 三菱瓦斯化学株式会社 Method for producing dimethyl ether
DE4132993A1 (en) * 1991-10-04 1993-04-08 Rwe Dea Ag METHOD FOR PRODUCING DIMETHYL ETHER
DE19943219A1 (en) * 1999-09-09 2001-03-15 Axiva Gmbh Process for the preparation of dimethyl ether
JP4938941B2 (en) * 2001-08-30 2012-05-23 関西電力株式会社 Synthesis method of dimethyl ether
US6924399B2 (en) 2001-12-28 2005-08-02 Mitsubishi Heavy Industries, Ltd. Method of manufacturing dimethyl ether
KR100501922B1 (en) * 2003-02-19 2005-07-18 에스케이 주식회사 Process for preparing dimethyl ether from methanol
US7138557B2 (en) * 2003-04-22 2006-11-21 Uop Llc Selective dimethylether recovery and recycle in a methanol-to-olefin process
UA68183C2 (en) * 2003-11-07 2005-06-15 Khimtekhnolohiia State Res And Method for separation of dimethyl ether
CN1293029C (en) * 2004-03-15 2007-01-03 四川天一科技股份有限公司 Method for producing dimethyl ether from methanol
RU2282613C2 (en) * 2004-08-10 2006-08-27 Открытое акционерное общество Научно-исследовательский институт "Ярсинтез" (ОАО НИИ "Ярсинтез") High-purity dimethyl ether production process
CN1304369C (en) * 2004-10-12 2007-03-14 山东新华万博化工有限公司 Technique for preparing dimehtyl sulfate
KR100629939B1 (en) * 2004-10-15 2006-09-28 에스케이 주식회사 Method for preparing dimethyl ether from crude methanol in adiabatic reactor
CN101058534B (en) * 2006-04-18 2011-01-12 杭州林达化工技术工程有限公司 Device and method for preparing dimethyl ether from methanol
RU2315031C1 (en) * 2006-06-19 2008-01-20 Юрий Куртович Вайль Methanol processing method
KR100812099B1 (en) 2006-11-28 2008-03-12 한국가스공사 Mixed catalyst for the production of dimethyl ether, preparation method thereof and preparation method for the dimethyl ether using the same
FR2909666B1 (en) 2006-12-08 2009-03-06 Centre Nat Rech Scient DEHYDRATION OF METHANOL TO DIMETHYL ETHER EMPLOYING CATALYSTS BASED ON ZEOLITHE SUPPORTED ON SILICON CARBIDE
CN100513374C (en) * 2007-03-07 2009-07-15 中国科学院大连化学物理研究所 Method for preparing dimethyl ether by dehydration of methanol
CN101270034B (en) * 2008-05-12 2010-06-02 钱进华 Technique for preparing dimethyl ether
DE102008058931B4 (en) * 2008-11-25 2010-12-30 Lurgi Gmbh Process and apparatus for producing dimethyl ether from methanol
CN101412665B (en) * 2008-11-27 2011-01-12 何东 Apparatus for coproduction of refined methanol and dimethyl ether or production of each of refined methanol and dimethyl ether from coarse methyl alcohol
CN101550066B (en) * 2008-12-26 2013-06-05 新奥新能(北京)科技有限公司 Production method of aerosol grade dimethyl ether
CN101941891B (en) * 2009-07-06 2013-01-09 中国石油化工股份有限公司 Method for preparing dimethyl ether by dehydrating methanol
US8378150B2 (en) * 2009-08-12 2013-02-19 Catalytic Distillation Technologies Process for the production of dimethyl ether
DE102012018341A1 (en) 2012-09-15 2014-05-15 Thyssenkrupp Uhde Gmbh Process for the preparation of dimethyl ether and apparatus suitable therefor
CN103012076A (en) * 2012-12-24 2013-04-03 新奥科技发展有限公司 Method and device of rectifying dimethyl ether and recovering dimethyl ether from non-condensable gas
CN103435454B (en) * 2013-09-16 2015-04-29 凯瑞化工股份有限公司 Method for preparing dimethyl ether through methanol dehydration

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR8303437A (en) * 1982-07-01 1984-02-07 Du Pont PROCESS FOR THE PREPARATION OF DIMETHYL ETER BY CATALYTIC DEHYDRATION OF METHANOL
JPS59199648A (en) * 1983-04-27 1984-11-12 Mitsubishi Chem Ind Ltd Production of dimethyl ether

Also Published As

Publication number Publication date
PL268856A1 (en) 1988-10-13
FI875046L (en) 1988-05-19
DE3775902D1 (en) 1992-02-20
NZ222597A (en) 1990-09-26
EP0455004A1 (en) 1991-11-06
FI875046A0 (en) 1987-11-16
AU6550686A (en) 1988-05-19
CN1036199A (en) 1989-10-11
DK603187A (en) 1988-05-19
HUT45956A (en) 1988-09-28
ES2003076A4 (en) 1988-10-16
EP0270852A2 (en) 1988-06-15
JPS63208546A (en) 1988-08-30
AU603070B2 (en) 1990-11-08
NO874787D0 (en) 1987-11-17
DD270901A1 (en) 1989-08-16
SU1602392A3 (en) 1990-10-23
DK603187D0 (en) 1987-11-17
BR8606293A (en) 1988-07-05
YU208087A (en) 1988-10-31
CA1322767C (en) 1993-10-05
NO165914B (en) 1991-01-21
ES2003076T3 (en) 1992-07-01
EP0270852A3 (en) 1988-12-28
EP0270852B1 (en) 1992-01-08
NO874787L (en) 1988-05-19
GR880300102T1 (en) 1989-06-22
ATE71354T1 (en) 1992-01-15
IN168048B (en) 1991-01-26
FI875046A7 (en) 1988-05-19

Similar Documents

Publication Publication Date Title
NO165914C (en) PROCEDURE FOR THE PREPARATION OF PURE DIMETYLETS.
FI892110A0 (en) FOERFARANDE FOER FRAMSTAELLNING AV REN DIMETYLETER (DME).
JPS5533489A (en) Heterogeneous gas phase catalytic hydrogenation of aldehyde to alchol
ATE26695T1 (en) CATALYTIC PRODUCTION OF DIMETHYL ETHER.
DK373784D0 (en) METHOD AND CATALYST FOR PRODUCING DIMETHYLETHER
ES551730A0 (en) A PROCEDURE FOR THE SYNTHESIS OF SUBSTITUTED INDINS
FR2435456B1 (en) CATALYST FOR VAPOR OXIDATION OF ISOBUTYLENE OR TERTIARY BUTYL ALCOHOL, PROCESS FOR THEIR PREPARATION AND ITS APPLICATION TO THE PRODUCTION OF METHACROLEIN
JPS6468331A (en) Distillation purification of crude secondary butyl alcohol
FI875596A0 (en) FOERFARANDE FOER FRAMSTAELLNING AV TIENYLETYLAMINER OCH AEVEN DITIENYLETYLAMINER.
JPS5528928A (en) Preparation of methoxysilane
NO170406C (en) PROCEDURE FOR THE PREPARATION OF CHLOROFULORETHANE
ATE35986T1 (en) PROCESS FOR PRODUCTION OF 2,3-DIHYDRO-2,2DIMETHYL-7-BENZOFURANOL.
ATE423T1 (en) PRODUCTION OF OLEFINS FROM CRUDE METHANOL.
ES2017675B3 (en) PROCEDURE FOR THE SYNTHESIS OF 2,2-DIALCOXIPROPANOS.
ES2020180B3 (en) PROCEDURE FOR THE SEPARATION AND PURIFICATION OF POLYGLYCERINES OR WASTE CONTAINING POLYGLYCERINES.
JPS53144534A (en) Production of styrene
ES484660A1 (en) Purificn. of crude ketone(s) prepd. by dehydrogenation of alcohol(s) - using light hydrocarbon in azeotropic dehydration stage
JPS552632A (en) Treatment of mixture
IT8521512A0 (en) CATALYST FOR THE CONVERSION OF METHANOL TO OLEFINS.
SU1277570A1 (en) METHOD FOR CLEANING HYDROCARBONS OF COT CYCLOPENTADIENE

Legal Events

Date Code Title Description
MM1K Lapsed by not paying the annual fees

Free format text: LAPSED IN MAY 2001