NL8901578A - Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren. - Google Patents

Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren. Download PDF

Info

Publication number: NL8901578A
Authority: NL; Netherlands
Prior art keywords: process according; carbon dioxide; crude; acid; esters
Prior art date: 1989-06-22

Application number

NL8901578A

Other languages

English (en)

Dutch (nl)

Original Assignee

Suiker Unie

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1989-06-22

Filing date

1989-06-22

Publication date

1991-01-16

1989-06-22 Application filed by Suiker Unie filed Critical Suiker Unie

1989-06-22 Priority to NL8901578A priority Critical patent/NL8901578A/nl

1990-06-13 Priority to ES90201529T priority patent/ES2059993T3/es

1990-06-13 Priority to AT90201529T priority patent/ATE111475T1/de

1990-06-13 Priority to DK90201529.6T priority patent/DK0404226T3/da

1990-06-13 Priority to DE69012447T priority patent/DE69012447T2/de

1990-06-13 Priority to EP90201529A priority patent/EP0404226B1/en

1990-06-14 Priority to IE215590A priority patent/IE65355B1/en

1990-06-20 Priority to AU57656/90A priority patent/AU629951B2/en

1990-06-20 Priority to NZ234151A priority patent/NZ234151A/en

1990-06-21 Priority to FI903160A priority patent/FI95803C/sv

1990-06-22 Priority to CA002019702A priority patent/CA2019702A1/en

1990-06-22 Priority to JP2165470A priority patent/JPH0331293A/ja

1991-01-16 Publication of NL8901578A publication Critical patent/NL8901578A/nl

1993-07-14 Priority to US08/091,457 priority patent/US5378834A/en

Links

239000000194 fatty acid Substances 0.000 title claims abstract description 55
235000014113 dietary fatty acids Nutrition 0.000 title claims abstract description 51
229930195729 fatty acid Natural products 0.000 title claims abstract description 51
238000000034 method Methods 0.000 title claims abstract description 40
150000004665 fatty acids Chemical class 0.000 title claims abstract description 28
CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 109
229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 55
235000000346 sugar Nutrition 0.000 claims abstract description 47
238000000605 extraction Methods 0.000 claims abstract description 36
239000001569 carbon dioxide Substances 0.000 claims abstract description 28
238000011282 treatment Methods 0.000 claims abstract description 25
230000032050 esterification Effects 0.000 claims abstract description 19
238000005886 esterification reaction Methods 0.000 claims abstract description 19
150000002148 esters Chemical class 0.000 claims abstract description 14
235000021355 Stearic acid Nutrition 0.000 claims abstract description 11
QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 11
OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 11
239000008117 stearic acid Substances 0.000 claims abstract description 11
238000005406 washing Methods 0.000 claims abstract description 9
ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 31
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 12
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 12
POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 claims description 12
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 9
KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 9
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 8
239000005639 Lauric acid Substances 0.000 claims description 6
LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 6
ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 claims description 6
229920000728 polyester Polymers 0.000 claims description 6
239000000344 soap Substances 0.000 claims description 6
239000003960 organic solvent Substances 0.000 claims description 5
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 4
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 claims description 4
BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims description 4
229910052783 alkali metal Inorganic materials 0.000 claims description 3
150000001340 alkali metals Chemical class 0.000 claims description 3
239000007788 liquid Substances 0.000 claims description 3
BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 3
OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims description 2
KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 2
229910000147 aluminium phosphate Inorganic materials 0.000 claims description 2
KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 claims description 2
235000019253 formic acid Nutrition 0.000 claims description 2
IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims description 2
229910000041 hydrogen chloride Inorganic materials 0.000 claims description 2
239000004310 lactic acid Substances 0.000 claims description 2
235000014655 lactic acid Nutrition 0.000 claims description 2
229910000403 monosodium phosphate Inorganic materials 0.000 claims description 2
235000019799 monosodium phosphate Nutrition 0.000 claims description 2
WBHQBSYUUJJSRZ-UHFFFAOYSA-M sodium bisulfate Chemical compound [Na+].OS([O-])(=O)=O WBHQBSYUUJJSRZ-UHFFFAOYSA-M 0.000 claims description 2
229910000342 sodium bisulfate Inorganic materials 0.000 claims description 2
AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 2
239000010779 crude oil Substances 0.000 claims 2
239000003495 polar organic solvent Substances 0.000 claims 2
239000000463 material Substances 0.000 claims 1
-1 fatty acid esters Chemical class 0.000 abstract description 28
229930006000 Sucrose Natural products 0.000 abstract description 25
239000000047 product Substances 0.000 abstract description 25
239000005720 sucrose Substances 0.000 abstract description 25
150000003839 salts Chemical class 0.000 abstract description 21
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 abstract description 19
IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 abstract description 16
150000008163 sugars Chemical class 0.000 abstract description 15
239000002904 solvent Substances 0.000 abstract description 12
235000021314 Palmitic acid Nutrition 0.000 abstract description 8
WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 abstract description 8
239000012043 crude product Substances 0.000 abstract description 2
239000012467 final product Substances 0.000 abstract description 2
IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 24
239000007795 chemical reaction product Substances 0.000 description 20
ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 15
HPEUJPJOZXNMSJ-UHFFFAOYSA-N Methyl stearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC HPEUJPJOZXNMSJ-UHFFFAOYSA-N 0.000 description 12
FLIACVVOZYBSBS-UHFFFAOYSA-N Methyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC FLIACVVOZYBSBS-UHFFFAOYSA-N 0.000 description 10
WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 10
238000006467 substitution reaction Methods 0.000 description 8
238000006243 chemical reaction Methods 0.000 description 7
ZPVGIKNDGJGLCO-VGAMQAOUSA-N [(2s,3r,4s,5s,6r)-2-[(2s,3s,4s,5r)-3,4-dihydroxy-2,5-bis(hydroxymethyl)oxolan-2-yl]-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl] hexadecanoate Chemical compound CCCCCCCCCCCCCCCC(=O)O[C@@]1([C@]2(CO)[C@H]([C@H](O)[C@@H](CO)O2)O)O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O ZPVGIKNDGJGLCO-VGAMQAOUSA-N 0.000 description 6
CAMHHLOGFDZBBG-UHFFFAOYSA-N epoxidized methyl oleate Natural products CCCCCCCCC1OC1CCCCCCCC(=O)OC CAMHHLOGFDZBBG-UHFFFAOYSA-N 0.000 description 6
BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 6
239000000203 mixture Substances 0.000 description 5
239000001103 potassium chloride Substances 0.000 description 5
235000011164 potassium chloride Nutrition 0.000 description 5
WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 4
LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 4
QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 4
239000005642 Oleic acid Substances 0.000 description 4
ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 4
239000007957 coemulsifier Substances 0.000 description 4
QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 4
ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 4
238000000746 purification Methods 0.000 description 4
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
150000005690 diesters Chemical class 0.000 description 3
238000010309 melting process Methods 0.000 description 3
238000000593 microemulsion method Methods 0.000 description 3
VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
229910000027 potassium carbonate Inorganic materials 0.000 description 3
239000011541 reaction mixture Substances 0.000 description 3
238000007127 saponification reaction Methods 0.000 description 3
238000003815 supercritical carbon dioxide extraction Methods 0.000 description 3
DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 2
239000002253 acid Substances 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
125000004432 carbon atom Chemical group C* 0.000 description 2
238000001816 cooling Methods 0.000 description 2
238000001704 evaporation Methods 0.000 description 2
230000008020 evaporation Effects 0.000 description 2
150000002194 fatty esters Chemical class 0.000 description 2
239000000706 filtrate Substances 0.000 description 2
238000001914 filtration Methods 0.000 description 2
235000013305 food Nutrition 0.000 description 2
229910052744 lithium Inorganic materials 0.000 description 2
238000000199 molecular distillation Methods 0.000 description 2
230000020477 pH reduction Effects 0.000 description 2
229910052700 potassium Inorganic materials 0.000 description 2
239000011591 potassium Substances 0.000 description 2
238000002360 preparation method Methods 0.000 description 2
238000000926 separation method Methods 0.000 description 2
239000011734 sodium Substances 0.000 description 2
229910052708 sodium Inorganic materials 0.000 description 2
231100000331 toxic Toxicity 0.000 description 2
230000002588 toxic effect Effects 0.000 description 2
238000013022 venting Methods 0.000 description 2
238000010626 work up procedure Methods 0.000 description 2
208000035150 Hypercholesterolemia Diseases 0.000 description 1
SZYSLWCAWVWFLT-UTGHZIEOSA-N [(2s,3s,4s,5r)-3,4-dihydroxy-5-(hydroxymethyl)-2-[(2r,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxolan-2-yl]methyl octadecanoate Chemical compound O([C@@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@]1(COC(=O)CCCCCCCCCCCCCCCCC)O[C@H](CO)[C@@H](O)[C@@H]1O SZYSLWCAWVWFLT-UTGHZIEOSA-N 0.000 description 1
230000002378 acidificating effect Effects 0.000 description 1
150000001298 alcohols Chemical class 0.000 description 1
125000005907 alkyl ester group Chemical group 0.000 description 1
239000011575 calcium Substances 0.000 description 1
229910052791 calcium Inorganic materials 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
239000007810 chemical reaction solvent Substances 0.000 description 1
239000002537 cosmetic Substances 0.000 description 1
238000002425 crystallisation Methods 0.000 description 1
230000008025 crystallization Effects 0.000 description 1
230000007423 decrease Effects 0.000 description 1
238000004821 distillation Methods 0.000 description 1
QYDYPVFESGNLHU-UHFFFAOYSA-N elaidic acid methyl ester Natural products CCCCCCCCC=CCCCCCCCC(=O)OC QYDYPVFESGNLHU-UHFFFAOYSA-N 0.000 description 1
239000003995 emulsifying agent Substances 0.000 description 1
239000002360 explosive Substances 0.000 description 1
235000021588 free fatty acids Nutrition 0.000 description 1
239000004519 grease Substances 0.000 description 1
239000012535 impurity Substances 0.000 description 1
150000004702 methyl esters Chemical class 0.000 description 1
QYDYPVFESGNLHU-KHPPLWFESA-N methyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC QYDYPVFESGNLHU-KHPPLWFESA-N 0.000 description 1
229940073769 methyl oleate Drugs 0.000 description 1
150000002772 monosaccharides Chemical group 0.000 description 1
238000006386 neutralization reaction Methods 0.000 description 1
230000003472 neutralizing effect Effects 0.000 description 1
239000000825 pharmaceutical preparation Substances 0.000 description 1
MQOCIYICOGDBSG-UHFFFAOYSA-M potassium;hexadecanoate Chemical compound [K+].CCCCCCCCCCCCCCCC([O-])=O MQOCIYICOGDBSG-UHFFFAOYSA-M 0.000 description 1
238000001556 precipitation Methods 0.000 description 1
239000002994 raw material Substances 0.000 description 1
238000011084 recovery Methods 0.000 description 1
238000004064 recycling Methods 0.000 description 1
239000007787 solid Substances 0.000 description 1
238000000638 solvent extraction Methods 0.000 description 1
239000000126 substance Substances 0.000 description 1
239000004094 surface-active agent Substances 0.000 description 1
239000000725 suspension Substances 0.000 description 1
238000005809 transesterification reaction Methods 0.000 description 1
239000002699 waste material Substances 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C07H13/06—Fatty acids
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H1/00—Processes for the preparation of sugar derivatives
- C07H1/06—Separation; Purification
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/54—Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Engineering & Computer Science (AREA)
Health & Medical Sciences (AREA)
Biochemistry (AREA)
Biotechnology (AREA)
General Health & Medical Sciences (AREA)
Genetics & Genomics (AREA)
Molecular Biology (AREA)
Life Sciences & Earth Sciences (AREA)
Saccharide Compounds (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Detergent Compositions (AREA)
Extraction Or Liquid Replacement (AREA)

NL8901578A 1989-06-22 1989-06-22 Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren. NL8901578A (nl)

Priority Applications (13)

Application Number	Priority Date	Filing Date	Title
NL8901578A NL8901578A (nl)	1989-06-22	1989-06-22	Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren.
EP90201529A EP0404226B1 (en)	1989-06-22	1990-06-13	Process for purifying products containing esters of a non-reducing sugar and one or more fatty acids
AT90201529T ATE111475T1 (de)	1989-06-22	1990-06-13	Verfahren zur reinigung von produkten, die ester eines nichtreduzierenden zuckers und eine oder mehrere fettsäuren enthalten.
DK90201529.6T DK0404226T3 (da)	1989-06-22	1990-06-13	Fremgangsmåde til rensning af produkter indeholdende estere af en ikke-reducerende sukker og en eller flere fedtsyrer
DE69012447T DE69012447T2 (de)	1989-06-22	1990-06-13	Verfahren zur Reinigung von Produkten, die Ester eines nichtreduzierenden Zuckers und eine oder mehrere Fettsäuren enthalten.
ES90201529T ES2059993T3 (es)	1989-06-22	1990-06-13	Procedimiento para la purificacion de productos que contienen esteres de un azucar no reductor y uno o mas acidos grasos.
IE215590A IE65355B1 (en)	1989-06-22	1990-06-14	Process for purifying products containing esters of a non-reducing sugar and one or more fatty acids
AU57656/90A AU629951B2 (en)	1989-06-22	1990-06-20	Process for purifying products containing esters of a non-reducing sugar and one or more fatty acids
NZ234151A NZ234151A (en)	1989-06-22	1990-06-20	Esters of a non-reducing sugar and one or more fatty acids and process for their purification and extraction
FI903160A FI95803C (sv)	1989-06-22	1990-06-21	Förfarande för rening av produkter innehållande estrar av ett icke-reducerande socker och en eller flera fettsyror
CA002019702A CA2019702A1 (en)	1989-06-22	1990-06-22	Process for purifying products containing esters of a non-reducing sugar and one or more fatty acids
JP2165470A JPH0331293A (ja)	1989-06-22	1990-06-22	非還元糖と一種類以上の脂肪酸とのエステルを含有する生成物を精製する方法
US08/091,457 US5378834A (en)	1989-06-22	1993-07-14	Process for purifying products containing esters of a non-reducing sugar and one or more fatty acids

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL8901578A NL8901578A (nl)	1989-06-22	1989-06-22	Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren.
NL8901578		1989-06-22

Publications (1)

Publication Number	Publication Date
NL8901578A true NL8901578A (nl)	1991-01-16

Family

ID=19854884

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL8901578A NL8901578A (nl)	1989-06-22	1989-06-22	Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren.

Country Status (13)

Country	Link
US (1)	US5378834A (sv)
EP (1)	EP0404226B1 (sv)
JP (1)	JPH0331293A (sv)
AT (1)	ATE111475T1 (sv)
AU (1)	AU629951B2 (sv)
CA (1)	CA2019702A1 (sv)
DE (1)	DE69012447T2 (sv)
DK (1)	DK0404226T3 (sv)
ES (1)	ES2059993T3 (sv)
FI (1)	FI95803C (sv)
IE (1)	IE65355B1 (sv)
NL (1)	NL8901578A (sv)
NZ (1)	NZ234151A (sv)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US5378834A (en) *	1989-06-22	1995-01-03	Cooperatieve Vereniging Suiker Unie U.A.	Process for purifying products containing esters of a non-reducing sugar and one or more fatty acids

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE4131505A1 (de) *	1991-09-21	1993-03-25	Henkel Kgaa	Verfahren zur aufbereitung des bei der herstellung von saccharose-fettsaeureestern erhaltenen reaktionsgemisches
EP0659760B1 (en) *	1993-12-24	2001-10-04	Mitsubishi Chemical Corporation	Process for producing sucrose fatty acid ester
DE59502327D1 (de) *	1994-11-18	1998-07-02	Goldschmidt Ag Th	Verfahren zur Herstellung von Alkylglycosiden
US6312528B1 (en)	1997-03-06	2001-11-06	Cri Recycling Service, Inc.	Removal of contaminants from materials
AU4210699A (en)	1998-05-27	1999-12-13	University Of Iowa Research Foundation, The	Sucrose-based surfactants and methods therefor
DE10255231B4 (de) *	2002-11-26	2006-02-02	Uhde High Pressure Technologies Gmbh	Hochdruckvorrichtung zum Verschließen eines Druckbehälters im Reinraum
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US4377686A (en) *	1981-01-08	1983-03-22	The United States Of America As Represented By The Secretary Of Agriculture	Method of purifying fatty acid ester products
EP0065390A1 (en) *	1981-05-11	1982-11-24	TATE & LYLE PUBLIC LIMITED COMPANY	Purification of sucrose esters
JPS61297A (ja) *	1984-06-12	1986-01-06	日本油脂株式会社	オレイン酸の製造法
NL8500191A (nl) *	1985-01-24	1986-08-18	Suiker Unie	Werkwijze voor het bereiden van esters van een niet-reducerende suiker en een of meer vetzuren.
US4675132A (en) *	1985-03-28	1987-06-23	The United States Of America As Represented By The Secretary Of Commerce	Polyunsaturated fatty acids from fish oils
US4749522A (en) *	1985-10-31	1988-06-07	Angio-Medical Corporation	Supercritical fluid extraction of animal derived materials
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JPH0762025B2 (ja) *	1988-10-05	1995-07-05	昭和産業株式会社	ポリオール脂肪酸ポリエステルの安定化法
NL8901578A (nl) *	1989-06-22	1991-01-16	Suiker Unie	Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren.

1989
- 1989-06-22 NL NL8901578A patent/NL8901578A/nl not_active Application Discontinuation
1990
- 1990-06-13 AT AT90201529T patent/ATE111475T1/de active
- 1990-06-13 DE DE69012447T patent/DE69012447T2/de not_active Expired - Fee Related
- 1990-06-13 DK DK90201529.6T patent/DK0404226T3/da active
- 1990-06-13 ES ES90201529T patent/ES2059993T3/es not_active Expired - Lifetime
- 1990-06-13 EP EP90201529A patent/EP0404226B1/en not_active Expired - Lifetime
- 1990-06-14 IE IE215590A patent/IE65355B1/en not_active IP Right Cessation
- 1990-06-20 AU AU57656/90A patent/AU629951B2/en not_active Ceased
- 1990-06-20 NZ NZ234151A patent/NZ234151A/en unknown
- 1990-06-21 FI FI903160A patent/FI95803C/sv not_active IP Right Cessation
- 1990-06-22 CA CA002019702A patent/CA2019702A1/en not_active Abandoned
- 1990-06-22 JP JP2165470A patent/JPH0331293A/ja active Pending
1993
- 1993-07-14 US US08/091,457 patent/US5378834A/en not_active Expired - Fee Related

Cited By (1)

* Cited by examiner, † Cited by third party
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US5378834A (en) *	1989-06-22	1995-01-03	Cooperatieve Vereniging Suiker Unie U.A.	Process for purifying products containing esters of a non-reducing sugar and one or more fatty acids

Also Published As

Publication number	Publication date
CA2019702A1 (en)	1990-12-22
NZ234151A (en)	1992-02-25
FI95803B (sv)	1995-12-15
FI903160A0 (sv)	1990-06-21
IE902155L (en)	1990-12-22
DK0404226T3 (da)	1994-10-17
US5378834A (en)	1995-01-03
IE65355B1 (en)	1995-10-18
AU629951B2 (en)	1992-10-15
FI95803C (sv)	1996-03-25
AU5765690A (en)	1991-01-03
DE69012447D1 (de)	1994-10-20
ES2059993T3 (es)	1994-11-16
JPH0331293A (ja)	1991-02-12
ATE111475T1 (de)	1994-09-15
EP0404226B1 (en)	1994-09-14
EP0404226A1 (en)	1990-12-27
DE69012447T2 (de)	1995-02-02
IE902155A1 (en)	1991-01-02

Publication	Publication Date	Title
NL8901578A (nl)	1991-01-16	Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren.
EP0255824B1 (en)	1990-01-24	A process for the production of refined fish oil concentrate
US3748324A (en)	1973-07-24	Method for the purification of sucrose esters of fatty acids
DE68906525T2 (de)	1993-09-23	Verfahren zur herstellung von estern der beta-hydroxybuttersaeure.
DK142148B (da)	1980-09-08	Fremgangsmåde til fremstilling af estere af sucrose med fedtsyrer.
US4104464A (en)	1978-08-01	Purification of sucrose esters
AU670723B2 (en)	1996-07-25	A process for separating lipophilic compounds
US4256875A (en)	1981-03-17	Extraction of sennosides
JP2004307476A (ja)	2004-11-04	Ｏ−アシル化グルコース誘導体の調製方法
US3249600A (en)	1966-05-03	Process for the preparation of purified sucrose esters and products obtained thereby
JPH0641007A (ja)	1994-02-15	高純度ポリグリセリン脂肪酸エステルの製造方法
JPH07118285A (ja)	1995-05-09	ショ糖脂肪酸エステルの製造方法
US5811563A (en)	1998-09-22	Process for the fractionation of wool wax acid mixtures
US1880677A (en)	1932-10-04	Recovery of organic acids
NL9201041A (nl)	1993-01-04	Werkwijze voor de bereiding van sucrose-vetzuuresters.
EP0274887A1 (en)	1988-07-20	Process for the recovery of succinic acid from its mixtures with other carboxylic acids
EP0448996B1 (en)	1998-08-19	Process for removing soaps and fatty acids from sucrose fatty acid esters
DE60301672T9 (de)	2006-12-07	Herstellung von ascorbinsäureestern
CN119923456A (zh)	2025-05-02	从鱼油残余物中回收胆固醇
KR19990058544A (ko)	1999-07-15	자당 지방산 에스테르의 제조방법
US1766715A (en)	1930-06-24	Production of lactic acid and its derivatives
JPH0592102A (ja)	1993-04-16	有機酸または有機酸エステルの晶析方法
IL34245A (en)	1970-08-19	Process for the preparation of a-) 1 - noble - 3 - indolyl (low elliptical carboxyls
US2488559A (en)	1949-11-22	Penicillin extraction process
CS219401B1 (cs)	1983-03-25	Způsob dělení směsi D-threo-chloramfenikolového esteru kyseliny palmitové s volnou kyselinou palmitovou

Legal Events

Date	Code	Title	Description
1991-01-16	A1B	A search report has been drawn up
1992-02-03	BV	The patent application has lapsed

NL8901578A - Werkwijze voor het zuiveren van produkten met esters van een niet-reducerende suiker en een of meer vetzuren. - Google Patents

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