NL7811389A - Bereiding van fructose. - Google Patents

Bereiding van fructose. Download PDF

Info

Publication number: NL7811389A
Authority: NL; Netherlands
Prior art keywords: fructose; vegetable material; inulin; preparation; activity
Prior art date: 1978-11-18

Application number

NL7811389A

Other languages

English (en)

Dutch (nl)

Original Assignee

Stamicarbon

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1978-11-18

Filing date

1978-11-18

Publication date

1980-05-20

1978-11-18 Application filed by Stamicarbon filed Critical Stamicarbon

1978-11-18 Priority to NL7811389A priority Critical patent/NL7811389A/nl

1979-11-15 Priority to EP79200672A priority patent/EP0011350A1/en

1979-11-15 Priority to DK484179A priority patent/DK484179A/da

1979-11-16 Priority to ES486027A priority patent/ES486027A1/es

1979-11-19 Priority to US06/095,680 priority patent/US4277563A/en

1980-05-20 Publication of NL7811389A publication Critical patent/NL7811389A/nl

Links

229930091371 Fructose Natural products 0.000 title claims description 31
239000005715 Fructose Substances 0.000 title claims description 31
RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 title claims description 30
238000002360 preparation method Methods 0.000 title claims description 14
229920001202 Inulin Polymers 0.000 claims description 17
JYJIGFIDKWBXDU-MNNPPOADSA-N inulin Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@]1(OC[C@]2(OC[C@]3(OC[C@]4(OC[C@]5(OC[C@]6(OC[C@]7(OC[C@]8(OC[C@]9(OC[C@]%10(OC[C@]%11(OC[C@]%12(OC[C@]%13(OC[C@]%14(OC[C@]%15(OC[C@]%16(OC[C@]%17(OC[C@]%18(OC[C@]%19(OC[C@]%20(OC[C@]%21(OC[C@]%22(OC[C@]%23(OC[C@]%24(OC[C@]%25(OC[C@]%26(OC[C@]%27(OC[C@]%28(OC[C@]%29(OC[C@]%30(OC[C@]%31(OC[C@]%32(OC[C@]%33(OC[C@]%34(OC[C@]%35(OC[C@]%36(O[C@@H]%37[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O%37)O)[C@H]([C@H](O)[C@@H](CO)O%36)O)[C@H]([C@H](O)[C@@H](CO)O%35)O)[C@H]([C@H](O)[C@@H](CO)O%34)O)[C@H]([C@H](O)[C@@H](CO)O%33)O)[C@H]([C@H](O)[C@@H](CO)O%32)O)[C@H]([C@H](O)[C@@H](CO)O%31)O)[C@H]([C@H](O)[C@@H](CO)O%30)O)[C@H]([C@H](O)[C@@H](CO)O%29)O)[C@H]([C@H](O)[C@@H](CO)O%28)O)[C@H]([C@H](O)[C@@H](CO)O%27)O)[C@H]([C@H](O)[C@@H](CO)O%26)O)[C@H]([C@H](O)[C@@H](CO)O%25)O)[C@H]([C@H](O)[C@@H](CO)O%24)O)[C@H]([C@H](O)[C@@H](CO)O%23)O)[C@H]([C@H](O)[C@@H](CO)O%22)O)[C@H]([C@H](O)[C@@H](CO)O%21)O)[C@H]([C@H](O)[C@@H](CO)O%20)O)[C@H]([C@H](O)[C@@H](CO)O%19)O)[C@H]([C@H](O)[C@@H](CO)O%18)O)[C@H]([C@H](O)[C@@H](CO)O%17)O)[C@H]([C@H](O)[C@@H](CO)O%16)O)[C@H]([C@H](O)[C@@H](CO)O%15)O)[C@H]([C@H](O)[C@@H](CO)O%14)O)[C@H]([C@H](O)[C@@H](CO)O%13)O)[C@H]([C@H](O)[C@@H](CO)O%12)O)[C@H]([C@H](O)[C@@H](CO)O%11)O)[C@H]([C@H](O)[C@@H](CO)O%10)O)[C@H]([C@H](O)[C@@H](CO)O9)O)[C@H]([C@H](O)[C@@H](CO)O8)O)[C@H]([C@H](O)[C@@H](CO)O7)O)[C@H]([C@H](O)[C@@H](CO)O6)O)[C@H]([C@H](O)[C@@H](CO)O5)O)[C@H]([C@H](O)[C@@H](CO)O4)O)[C@H]([C@H](O)[C@@H](CO)O3)O)[C@H]([C@H](O)[C@@H](CO)O2)O)[C@@H](O)[C@H](O)[C@@H](CO)O1 JYJIGFIDKWBXDU-MNNPPOADSA-N 0.000 claims description 17
229940029339 inulin Drugs 0.000 claims description 17
108090000790 Enzymes Proteins 0.000 claims description 15
102000004190 Enzymes Human genes 0.000 claims description 15
108010090785 inulinase Proteins 0.000 claims description 13
238000000034 method Methods 0.000 claims description 13
239000005418 vegetable material Substances 0.000 claims description 13
238000006243 chemical reaction Methods 0.000 claims description 12
230000000694 effects Effects 0.000 claims description 12
229920000642 polymer Polymers 0.000 claims description 6
239000012736 aqueous medium Substances 0.000 claims description 4
230000002255 enzymatic effect Effects 0.000 claims description 2
238000000926 separation method Methods 0.000 claims description 2
241000196324 Embryophyta Species 0.000 description 6
LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
239000000463 material Substances 0.000 description 6
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
238000006460 hydrolysis reaction Methods 0.000 description 5
235000007542 Cichorium intybus Nutrition 0.000 description 4
240000008892 Helianthus tuberosus Species 0.000 description 4
235000003230 Helianthus tuberosus Nutrition 0.000 description 4
238000005119 centrifugation Methods 0.000 description 4
230000007062 hydrolysis Effects 0.000 description 4
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
241000723343 Cichorium Species 0.000 description 3
WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
230000002378 acidificating effect Effects 0.000 description 3
230000015572 biosynthetic process Effects 0.000 description 3
239000006227 byproduct Substances 0.000 description 3
238000000605 extraction Methods 0.000 description 3
239000008103 glucose Substances 0.000 description 3
AIHDCSAXVMAMJH-GFBKWZILSA-N levan Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)OC[C@@H]1[C@@H](O)[C@H](O)[C@](CO)(CO[C@@H]2[C@H]([C@H](O)[C@@](O)(CO)O2)O)O1 AIHDCSAXVMAMJH-GFBKWZILSA-N 0.000 description 3
239000007787 solid Substances 0.000 description 3
244000116484 Inula helenium Species 0.000 description 2
244000272264 Saussurea lappa Species 0.000 description 2
235000006784 Saussurea lappa Nutrition 0.000 description 2
239000002253 acid Substances 0.000 description 2
239000013078 crystal Substances 0.000 description 2
238000002425 crystallisation Methods 0.000 description 2
230000008025 crystallization Effects 0.000 description 2
238000001914 filtration Methods 0.000 description 2
239000000203 mixture Substances 0.000 description 2
230000007935 neutral effect Effects 0.000 description 2
238000011084 recovery Methods 0.000 description 2
239000000126 substance Substances 0.000 description 2
239000000725 suspension Substances 0.000 description 2
YZUPZGFPHUVJKC-UHFFFAOYSA-N 1-bromo-2-methoxyethane Chemical compound COCCBr YZUPZGFPHUVJKC-UHFFFAOYSA-N 0.000 description 1
241000228245 Aspergillus niger Species 0.000 description 1
241001450781 Bipolaris oryzae Species 0.000 description 1
244000298479 Cichorium intybus Species 0.000 description 1
244000115658 Dahlia pinnata Species 0.000 description 1
235000012040 Dahlia pinnata Nutrition 0.000 description 1
229920002670 Fructan Polymers 0.000 description 1
VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
108090000604 Hydrolases Proteins 0.000 description 1
235000002598 Inula helenium Nutrition 0.000 description 1
241000209504 Poaceae Species 0.000 description 1
244000253911 Saccharomyces fragilis Species 0.000 description 1
235000018368 Saccharomyces fragilis Nutrition 0.000 description 1
229920002125 Sokalan® Polymers 0.000 description 1
229920002472 Starch Polymers 0.000 description 1
229930006000 Sucrose Natural products 0.000 description 1
CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
244000294925 Tragopogon dubius Species 0.000 description 1
235000004478 Tragopogon dubius Nutrition 0.000 description 1
235000012363 Tragopogon porrifolius Nutrition 0.000 description 1
GTDPSWPPOUPBNX-UHFFFAOYSA-N ac1mqpva Chemical compound CC12C(=O)OC(=O)C1(C)C1(C)C2(C)C(=O)OC1=O GTDPSWPPOUPBNX-UHFFFAOYSA-N 0.000 description 1
238000005882 aldol condensation reaction Methods 0.000 description 1
239000008346 aqueous phase Substances 0.000 description 1
230000001580 bacterial effect Effects 0.000 description 1
108010051210 beta-Fructofuranosidase Proteins 0.000 description 1
238000009835 boiling Methods 0.000 description 1
229910052799 carbon Inorganic materials 0.000 description 1
230000015556 catabolic process Effects 0.000 description 1
230000007073 chemical hydrolysis Effects 0.000 description 1
239000002131 composite material Substances 0.000 description 1
238000006731 degradation reaction Methods 0.000 description 1
239000003248 enzyme activator Substances 0.000 description 1
238000004108 freeze drying Methods 0.000 description 1
DKAGJZJALZXOOV-UHFFFAOYSA-N hydrate;hydrochloride Chemical compound O.Cl DKAGJZJALZXOOV-UHFFFAOYSA-N 0.000 description 1
230000003301 hydrolyzing effect Effects 0.000 description 1
239000001573 invertase Substances 0.000 description 1
235000011073 invertase Nutrition 0.000 description 1
108010005131 levanase Proteins 0.000 description 1
238000004519 manufacturing process Methods 0.000 description 1
239000002609 medium Substances 0.000 description 1
244000005700 microbiome Species 0.000 description 1
238000002156 mixing Methods 0.000 description 1
239000012452 mother liquor Substances 0.000 description 1
229930014626 natural product Natural products 0.000 description 1
238000006116 polymerization reaction Methods 0.000 description 1
239000000843 powder Substances 0.000 description 1
239000000047 product Substances 0.000 description 1
239000011541 reaction mixture Substances 0.000 description 1
238000012958 reprocessing Methods 0.000 description 1
239000008107 starch Substances 0.000 description 1
235000019698 starch Nutrition 0.000 description 1
238000003756 stirring Methods 0.000 description 1
239000005720 sucrose Substances 0.000 description 1
238000000108 ultra-filtration Methods 0.000 description 1

Classifications

- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P19/00—Preparation of compounds containing saccharide radicals
- C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
- C13K11/00—Fructose

Landscapes

Chemical & Material Sciences (AREA)
Organic Chemistry (AREA)
Life Sciences & Earth Sciences (AREA)
Biochemistry (AREA)
Engineering & Computer Science (AREA)
Zoology (AREA)
Wood Science & Technology (AREA)
Microbiology (AREA)
General Chemical & Material Sciences (AREA)
Chemical Kinetics & Catalysis (AREA)
Biotechnology (AREA)
Health & Medical Sciences (AREA)
Bioinformatics & Cheminformatics (AREA)
General Engineering & Computer Science (AREA)
General Health & Medical Sciences (AREA)
Genetics & Genomics (AREA)
Preparation Of Compounds By Using Micro-Organisms (AREA)
Polysaccharides And Polysaccharide Derivatives (AREA)

NL7811389A 1978-11-18 1978-11-18 Bereiding van fructose. NL7811389A (nl)

Priority Applications (5)

Application Number	Priority Date	Filing Date	Title
NL7811389A NL7811389A (nl)	1978-11-18	1978-11-18	Bereiding van fructose.
EP79200672A EP0011350A1 (en)	1978-11-18	1979-11-15	Preparation of fructose
DK484179A DK484179A (da)	1978-11-18	1979-11-15	Fremstilling af fructose
ES486027A ES486027A1 (es)	1978-11-18	1979-11-16	Procedimiento para la preparacion de fructosa a partir de materia vegetal
US06/095,680 US4277563A (en)	1978-11-18	1979-11-19	Preparation of fructose

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
NL7811389		1978-11-18
NL7811389A NL7811389A (nl)	1978-11-18	1978-11-18	Bereiding van fructose.

Publications (1)

Publication Number	Publication Date
NL7811389A true NL7811389A (nl)	1980-05-20

Family

ID=19831918

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
NL7811389A NL7811389A (nl)	1978-11-18	1978-11-18	Bereiding van fructose.

Country Status (5)

Country	Link
US (1)	US4277563A (es)
EP (1)	EP0011350A1 (es)
DK (1)	DK484179A (es)
ES (1)	ES486027A1 (es)
NL (1)	NL7811389A (es)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
NL8003723A (nl) *	1980-06-27	1982-01-18	Stamicarbon	Inulinase.
DK147409C (da) *	1981-04-29	1985-03-11	Novo Industri As	Fremgangsmaade til hydrolysering af inulin ved hjaelp af et aspergillus ficuum-inulinasepraeparat
CA1170203A (en) *	1981-09-15	1984-07-03	Ernst Hoehn	Fructose syrup manufacture
DE3508387C1 (de) *	1985-03-08	1986-07-17	Günter Prof. Dr.-Ing. 1000 Berlin Bärwald	Verfahren zur Herstellung eines glukosearmen Aufschlussproduktes aus inulinhaltigen Pflanzenteilen
FR2618161B1 (fr) *	1987-07-17	1991-06-14	Roquette Freres	Procede de preparation de sirops de fructose a partir de matieres premieres vegetales contenant de l'inuline.
US4927757A (en) *	1988-07-29	1990-05-22	Idaho Research Foundation, Inc.	Production of substantially pure fructose
US5659028A (en) *	1990-02-23	1997-08-19	Raffinerie Tirlemontoise S.A.	Branched fructo-oligosaccharides, method for obtaining them and use of products containing them
EP0728213B2 (en) *	1993-11-09	2008-12-10	E.I. Du Pont De Nemours And Company	Transgenic fructan accumulating crops and methods for their production
US5846333A (en) *	1996-03-12	1998-12-08	Partida; Virgilio Zuniga	Method of producing fructose syrup from agave plants
BE1010450A3 (nl) *	1996-08-01	1998-08-04	Tiense Suikerraffinaderij Nv	Werkwijze voor het maken van een fructosestroop rijk aan fructose.
US5840361A (en) *	1997-04-09	1998-11-24	Beech-Nut Nutrition Corporation	Fructan-containing baby food compositions and methods therefor
US5952205A (en) *	1998-02-06	1999-09-14	Neose Technologies, Inc.	Process for processing sucrose into glucose and fructose
US5998177A (en) *	1998-11-19	1999-12-07	Neose Technologies, Inc.	Process for processing sucrose into glucose
FR2825898B1 (fr) *	2001-06-15	2004-11-19	Sebastien Bossard	Nouvelle farine alimentaire, son utilisation pour la fabrication d'une pate et un procede en faisant usage
EP1610623B1 (en) *	2003-03-25	2011-11-23	Aarhus Universitet	Methodologies for improving the quality of meat, health status of animals and impact on environment

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE1042364B (de) *	1954-12-01	1958-10-30	Keimdiaet G M B H	Verfahren zur Herstellung von Fruktosesirup
JPS5649117B2 (es) *	1974-06-22	1981-11-19
JPS52136928A (en) *	1976-05-11	1977-11-16	Sankyo Co	Process for preparing fructose from jerusalem artichoke by enzymatic method
JPS52136929A (en) *	1976-05-11	1977-11-16	Sankyo Co	Process for preparing fructose from jerusalem artichoke by enzymatic method

1978
- 1978-11-18 NL NL7811389A patent/NL7811389A/nl not_active Application Discontinuation
1979
- 1979-11-15 DK DK484179A patent/DK484179A/da unknown
- 1979-11-15 EP EP79200672A patent/EP0011350A1/en not_active Withdrawn
- 1979-11-16 ES ES486027A patent/ES486027A1/es not_active Expired
- 1979-11-19 US US06/095,680 patent/US4277563A/en not_active Expired - Lifetime

Also Published As

Publication number	Publication date
US4277563A (en)	1981-07-07
DK484179A (da)	1980-05-19
ES486027A1 (es)	1980-05-16
EP0011350A1 (en)	1980-05-28

Publication	Publication Date	Title
NL7811389A (nl)	1980-05-20	Bereiding van fructose.
CA1230592A (en)	1987-12-22	Organosolv process for hydrolytic decomposition of lignocellulosic and starch materials
US5478732A (en)	1995-12-26	Process for the preparation of long-chain inulin with inulinase
US4448790A (en)	1984-05-15	Process for fractioning grain flour into components of food quality
US4431737A (en)	1984-02-14	Process for the production of alpha-galactosidase and uses of the enzyme thus obtained
JP5322150B2 (ja)	2013-10-23	セルロースを含むバイオマスの糖化方法
US4547226A (en)	1985-10-15	Preparation of high fructose syrups from citrus residues
EP0822262A1 (en)	1998-02-04	Process for producing a fructose syrup rich in fructose
CN103717622A (zh)	2014-04-09	一种从玉米纤维中提取半纤维素的方法
US5578335A (en)	1996-11-26	Process for the production of juices from fruits and vegetables
SU1024014A3 (ru)	1983-06-15	Способ получени ферментного препарата глюкоизомеразы
EP0043169B1 (en)	1983-10-12	Inulinase
US20100024810A1 (en)	2010-02-04	Decrystallization of cellulosic biomass with an acid mixture comprising phosphoric and sulfuric acids
US20130149761A1 (en)	2013-06-13	Method to recover sugars of pre-treated lignocellulosic biomass liquids
Park et al.	1998	Enzymatic production of inulo-oligosaccharides from chicory juice
US4488912A (en)	1984-12-18	Preparation of high fructose syrups from citrus residues
US4612284A (en)	1986-09-16	Process for the enzymatic hydrolysis of non-gelatinized granular starch material directly to glucose
EP0126513B1 (en)	1986-12-03	Process for the recovery of monosaccharides from poly-, oligo- and/or disaccharides containing plants by means of ultrafiltration
US10138505B2 (en)	2018-11-27	Process for the production of organic compounds from plant species
US4544558A (en)	1985-10-01	Process for preparing carbohydrates from vegetal juice
CA2604328C (en)	2011-12-06	Purification method and production method for cellobiose
Isbell et al.	1944	Preparation of salts of galacturonic acid from beet pulp
WO2002085950A1 (en)	2002-10-31	A method of isolation of immunostimulating glucan from oyster mushroom
WO2018099877A1 (en)	2018-06-07	Process for preparing soluble fibre
WO2000056268A2 (en)	2000-09-28	Beta glucan extraction from cereals

Legal Events

Date	Code	Title	Description
1980-06-10	A1B	A search report has been drawn up
1983-07-01	BV	The patent application has lapsed