MXPA05011894A - Proceso para producir 1,3-propanodiol. - Google Patents
Proceso para producir 1,3-propanodiol.Info
- Publication number
- MXPA05011894A MXPA05011894A MXPA05011894A MXPA05011894A MXPA05011894A MX PA05011894 A MXPA05011894 A MX PA05011894A MX PA05011894 A MXPA05011894 A MX PA05011894A MX PA05011894 A MXPA05011894 A MX PA05011894A MX PA05011894 A MXPA05011894 A MX PA05011894A
- Authority
- MX
- Mexico
- Prior art keywords
- propanediol
- phase
- feed stream
- aqueous feed
- contaminant
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/86—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by liquid-liquid treatment
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0446—Juxtaposition of mixers-settlers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0488—Flow sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0492—Applications, solvents used
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/26—Treatment of water, waste water, or sewage by extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
Se divulgan procesos para la recuperacion de 1,3-propanediol de una corriente de alimentacion acuosa. La presente invencion involucra poner en contacto una corriente de alimentacion acuosa que comprende agua, 1,3-propanediol y por lo menos un contaminante con por lo menos un solvente para extraccion para formar una mezcla. La mezcla se separa en una primera fase y una segunda fase. La segunda fase comprende la mayoria del agua de la corriente de alimentacion acuosa. La primera fase comprende un solvente extractor y por lo menos algo del 1,3-propanediol que estaba presente en la corriente de alimentacion acuosa. La proporcion de peso en la primera fase del 1,3-propanediol con cada contaminante presente es mayor que la proporcion de peso de 1-3-propanediol con el mismo contaminante en la corriente de alimentacion acuosa antes de que la corriente de alimentacion acuosa se ponga en contacto con el solvente extractor. La primera fase puede ser removida de la segunda fase separada con el fin de recuperar el 1,3-propanediol.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/430,498 US7056439B2 (en) | 2003-05-06 | 2003-05-06 | Process for producing 1, 3-propanediol |
| PCT/US2004/013905 WO2004101437A2 (en) | 2003-05-06 | 2004-05-06 | Process for producing 1, 3-propanediol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MXPA05011894A true MXPA05011894A (es) | 2006-02-17 |
Family
ID=33416251
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MXPA05011894A MXPA05011894A (es) | 2003-05-06 | 2004-05-06 | Proceso para producir 1,3-propanodiol. |
Country Status (17)
| Country | Link |
|---|---|
| US (2) | US7056439B2 (es) |
| EP (3) | EP1620362B1 (es) |
| JP (1) | JP4808624B2 (es) |
| KR (1) | KR101094018B1 (es) |
| CN (1) | CN100430111C (es) |
| AU (1) | AU2004238804B2 (es) |
| BR (2) | BRPI0410680B1 (es) |
| CA (1) | CA2524452C (es) |
| ES (3) | ES2505541T3 (es) |
| IL (1) | IL171693A (es) |
| MX (1) | MXPA05011894A (es) |
| NO (1) | NO20055383L (es) |
| NZ (1) | NZ543388A (es) |
| RU (1) | RU2323200C2 (es) |
| UA (1) | UA84289C2 (es) |
| WO (1) | WO2004101437A2 (es) |
| ZA (1) | ZA200509090B (es) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7056439B2 (en) * | 2003-05-06 | 2006-06-06 | Tate & Lyle Ingredidents Americas, Inc. | Process for producing 1, 3-propanediol |
| JP4837949B2 (ja) * | 2005-06-22 | 2011-12-14 | パナソニック電工株式会社 | グリコールの分離方法 |
| SE531424C2 (sv) | 2007-06-18 | 2009-03-31 | Perstorp Specialty Chem Ab | Extraktionsförfarande i en process för framställning av di-, tri- och polyhydroxialkoholer |
| KR101543485B1 (ko) * | 2007-11-30 | 2015-08-10 | 메타볼릭 익스플로러 | 발효 브로쓰로부터 알콜을 정제하는 방법 |
| AR072446A1 (es) * | 2008-03-02 | 2010-09-01 | Dow Global Technologies Inc | Proceso de hidrogenacion mejorado |
| US8084651B2 (en) * | 2008-03-10 | 2011-12-27 | Tate & Lyle Ingredients Americas Llc | Process for purification of glycerol |
| CA2738452C (en) | 2008-10-03 | 2016-06-21 | Metabolic Explorer | Method for purifying an alcohol from a fermentation broth using a falling film, a wiped film, a thin film or a short path evaporator |
| SG176654A1 (en) * | 2009-06-04 | 2012-01-30 | Genomatica Inc | Process of separating components of a fermentation broth |
| US8367877B2 (en) * | 2009-11-17 | 2013-02-05 | Alliant Techsystems Inc. | Methods of purifying 1,2,4-butanetriol |
| KR101134619B1 (ko) | 2009-12-10 | 2012-04-09 | 한국과학기술연구원 | 1,3-프로판다이올의 분리 방법 |
| WO2011076690A1 (en) | 2009-12-22 | 2011-06-30 | Metabolic Explorer | Method for purifying 1,2-propanediol from a fermentation broth |
| CN102140480B (zh) * | 2010-06-09 | 2013-07-17 | 河南天冠企业集团有限公司 | 一种发酵生产1,3-丙二醇的方法 |
| CN101898935A (zh) * | 2010-07-09 | 2010-12-01 | 华东理工大学 | 从发酵液中萃取分离1,3-丙二醇的方法 |
| US8466328B2 (en) | 2010-08-18 | 2013-06-18 | Eastman Chemical Company | Method for recovery and recycle of ruthenium homogeneous catalysts |
| US9227896B2 (en) | 2010-08-18 | 2016-01-05 | Eastman Chemical Company | Process for the separation and purification of a mixed diol stream |
| US8829248B2 (en) | 2010-08-18 | 2014-09-09 | Eastman Chemical Company | Method for recovery and recycle of ruthenium homogeneous catalysts |
| US8785686B2 (en) | 2010-09-23 | 2014-07-22 | Eastman Chemical Company | Process for recovering and recycling an acid catalyst |
| US8709376B2 (en) | 2010-09-23 | 2014-04-29 | Eastman Chemical Company | Process for recovering and recycling an acid catalyst |
| WO2012130316A1 (en) | 2011-03-31 | 2012-10-04 | Metabolic Explorer | Method for purifying mpg (monopropylene glycol) from a fermentation broth |
| CN103814116B (zh) * | 2011-07-29 | 2016-01-06 | 沙特阿拉伯石油公司 | 具有芳族分离的整合的加氢处理和异构化方法 |
| US8765999B2 (en) | 2012-03-27 | 2014-07-01 | Eastman Chemical Company | Hydrocarboxylation of formaldehyde in the presence of a higher order carboxylic acid and a homogeneous catalyst |
| WO2013148505A1 (en) * | 2012-03-27 | 2013-10-03 | Eastman Chemical Company | Process for the separation and purification of a mixed diol stream |
| US8927766B2 (en) | 2012-03-27 | 2015-01-06 | Eastman Chemical Company | Hydrocarboxylation of methylene dipropionate in the presence of a propionic acid and a homogeneous catalyst |
| US8703999B2 (en) | 2012-03-27 | 2014-04-22 | Eastman Chemical Company | Hydrocarboxylation of methylene dipropionate in the presence of propionic acid and a heterogeneous catalyst |
| US8829234B2 (en) | 2012-03-27 | 2014-09-09 | Eastman Chemical Company | Hydrocarboxylation of formaldehyde in the presence of a higher order carboxylic acid and heterogeneous catalyst |
| CN102816048A (zh) * | 2012-09-04 | 2012-12-12 | 华东理工大学 | 萃取分离发酵液中1,3-丙二醇的方法 |
| PL222957B1 (pl) * | 2012-09-28 | 2016-09-30 | Prochimia Surfaces Spółka Z Ograniczoną Odpowiedzialnością | Sposób izolacji propano-1,3-diolu z mieszaniny pofermentacyjnej |
| SG10201704410RA (en) * | 2012-12-21 | 2017-07-28 | Sulzer Chemtech Ag | A liquid-liquid extraction system and process for use thereof |
| CN104003844B (zh) * | 2014-05-23 | 2015-12-30 | 大连理工大学 | 萃取与发酵耦联分离发酵液中2,3-丁二醇的方法 |
| CN107001207A (zh) * | 2014-11-04 | 2017-08-01 | 国际壳牌研究有限公司 | 用于回收醇的方法 |
| US10086339B2 (en) | 2015-03-10 | 2018-10-02 | The University Of Connecticut | Polymers and membranes for separation of polar organic compounds from aqueous mixtures and methods of using |
| US10407453B2 (en) * | 2015-04-07 | 2019-09-10 | University Of Louisville Research Foundation, Inc. | Process for isolating C5 sugars from biomass hydrolyzate |
| FR3071172B1 (fr) * | 2017-09-18 | 2019-10-04 | IFP Energies Nouvelles | Procede de separation des composes furaniques, en particulier le 5- hydroxymethylfurfural, du dimethoxysulfoxyde par des extractions liquide-liquide |
| FR3073525A1 (fr) | 2017-11-13 | 2019-05-17 | Algobiotech | Procede d’extraction de carotenoides, composition et produits associes |
| US11710411B2 (en) * | 2020-05-08 | 2023-07-25 | The Travelers Indemnity Company | Systems and methods for autonomous hazardous area data collection |
| CN112920021B (zh) * | 2021-02-01 | 2022-04-29 | 大连理工大学 | 一种醇类混合溶剂萃取发酵液中1,3-丙二醇的方法 |
Family Cites Families (38)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3707188A (en) * | 1971-04-27 | 1972-12-26 | Atomic Energy Commission | Non collapse stemming of casing subjected to explosive effects |
| IL39710A (en) * | 1972-06-19 | 1975-04-25 | Imi Inst For Res & Dev | Recovery of acids from aqueous solutions by solvent extraction |
| JPS5325504A (en) * | 1976-08-20 | 1978-03-09 | Teijin Ltd | Isolation of glycols |
| JPS6267036A (ja) * | 1985-09-20 | 1987-03-26 | Jgc Corp | アルコ−ルの分離方法 |
| DE3632397A1 (de) * | 1986-09-24 | 1988-03-31 | Ruhrchemie Ag | Verfahren zur reinigung von propandiol-1,3 |
| US5254467A (en) * | 1988-09-01 | 1993-10-19 | Henkel Kommanditgesellschaft Auf Aktien | Fermentive production of 1,3-propanediol |
| ATE85813T1 (de) * | 1988-12-12 | 1993-03-15 | Unilever Nv | Verfahren zur mikrobiologischen herstellung von 1,3-propandiol aus glycerin. |
| US5356812A (en) * | 1990-08-10 | 1994-10-18 | Daicel Chemical Industries, Ltd. | Processes for production of optically active 3-phenyl-1,3-propanediol by asymmetric assimilation |
| US5412126A (en) * | 1991-04-17 | 1995-05-02 | The Regents Of The University Of California | Carboxylic acid sorption regeneration process |
| JPH05103904A (ja) * | 1991-10-21 | 1993-04-27 | Daicel Chem Ind Ltd | 分液促進方法 |
| US5304691A (en) * | 1993-07-13 | 1994-04-19 | Shell Oil Company | Process for making 1,3-propanediol and 3-hydroxypropanal |
| US5770776A (en) * | 1994-09-30 | 1998-06-23 | Shell Oil Company | Process for preparing 1,3-propanediol |
| US5463145A (en) * | 1994-09-30 | 1995-10-31 | Shell Oil Company | Process for preparing 1,3-propanediol |
| US5684214A (en) * | 1994-09-30 | 1997-11-04 | Shell Oil Company | Process for preparing 1,3-propanediol |
| RU2149156C1 (ru) * | 1994-09-30 | 2000-05-20 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. | Способ получения 1,3-алкандиолов и 3-гидроксиальдегидов |
| US5527973A (en) * | 1994-12-16 | 1996-06-18 | Kelsey; Donald R. | Purification of 1,3-propanediol |
| US5633362A (en) * | 1995-05-12 | 1997-05-27 | E. I. Du Pont De Nemours And Company | Production of 1,3-propanediol from glycerol by recombinant bacteria expressing recombinant diol dehydratase |
| US5599689A (en) * | 1995-05-12 | 1997-02-04 | E. I. Du Pont De Nemours And Company | Process for making 1,3-propanediol from carbohydrates using mixed microbial cultures |
| US6428767B1 (en) * | 1995-05-12 | 2002-08-06 | E. I. Du Pont De Nemours And Company | Method for identifying the source of carbon in 1,3-propanediol |
| US5686276A (en) * | 1995-05-12 | 1997-11-11 | E. I. Du Pont De Nemours And Company | Bioconversion of a fermentable carbon source to 1,3-propanediol by a single microorganism |
| IL118855A (en) * | 1996-07-15 | 1999-09-22 | Yissum Res Dev Co | Process for the separation of amino acids and their salts from impurities contained in an aqueous solution |
| IL129722A0 (en) * | 1996-11-13 | 2000-02-29 | Du Pont | Method for the production of 1,3-propanediol by recombinant organisms |
| KR20010013907A (ko) * | 1997-06-18 | 2001-02-26 | 메리 이. 보울러 | 3-히드록시프로피온알데히드의 수소화에 의한1,3-프로판디올의 제조 방법 |
| WO2000008198A1 (en) * | 1998-08-04 | 2000-02-17 | Metabolix, Inc. | Polyhydroxyalkanoate production from polyols |
| US5945570A (en) * | 1998-10-29 | 1999-08-31 | Arhancet; Juan Pedro | Catalyst and process for preparing 1,3-propanediol |
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| US6514733B1 (en) * | 1999-08-18 | 2003-02-04 | E. I. Du Pont De Nemours And Company | Process for the biological production of 1,3-propanediol with high titer |
| US6361983B1 (en) * | 1999-09-30 | 2002-03-26 | E. I. Du Pont De Nemours And Company | Process for the isolation of 1,3-propanediol from fermentation broth |
| FR2800751B1 (fr) * | 1999-11-09 | 2003-08-29 | Roquette Freres | Procede de production de 1,3 propanediol par voie fermentaire |
| FR2801058B1 (fr) * | 1999-11-16 | 2002-01-18 | Roquette Freres | Procede de purification du 1,3-propanediol a partir d'un milieu de fermentation |
| US6469222B2 (en) * | 2000-03-27 | 2002-10-22 | Shell Oil Company | One step process for preparing A 1,3-diol |
| US6479716B2 (en) * | 2000-03-29 | 2002-11-12 | Archer-Daniels-Midland Company | Method of recovering 1,3-propanediol from fermentation broth |
| AU2001245737A1 (en) | 2000-03-29 | 2001-10-08 | Archer Daniels Midland Company | Method of recovering 1,3-propanediol from fermentation broth |
| EP1305439B1 (en) * | 2000-07-21 | 2006-06-07 | Metabolix, Inc. | Production of polyhydroxyalkanoates from polyols |
| CN1204260C (zh) * | 2001-04-27 | 2005-06-01 | 大连理工大学 | 一种微生物微氧发酵生产1,3－丙二醇的方法 |
| DE50209503D1 (de) * | 2001-11-13 | 2007-03-29 | Metanomics Gmbh | Verfahren zur extraktion und analyse von inhaltsstoffen aus organischem material |
| US6641734B2 (en) * | 2002-01-03 | 2003-11-04 | A. E. Staley Manufacturing Co. | Process for purifying an organic acid |
| US7056439B2 (en) * | 2003-05-06 | 2006-06-06 | Tate & Lyle Ingredidents Americas, Inc. | Process for producing 1, 3-propanediol |
-
2003
- 2003-05-06 US US10/430,498 patent/US7056439B2/en not_active Expired - Lifetime
-
2004
- 2004-05-06 WO PCT/US2004/013905 patent/WO2004101437A2/en not_active Ceased
- 2004-05-06 CN CNB2004800184635A patent/CN100430111C/zh not_active Expired - Fee Related
- 2004-05-06 RU RU2005137867/04A patent/RU2323200C2/ru active
- 2004-05-06 EP EP04751324.7A patent/EP1620362B1/en not_active Expired - Lifetime
- 2004-05-06 ES ES11158110.4T patent/ES2505541T3/es not_active Expired - Lifetime
- 2004-05-06 ES ES04751324T patent/ES2408344T3/es not_active Expired - Lifetime
- 2004-05-06 MX MXPA05011894A patent/MXPA05011894A/es active IP Right Grant
- 2004-05-06 EP EP11158110.4A patent/EP2327465B1/en not_active Expired - Lifetime
- 2004-05-06 EP EP11158112A patent/EP2327464B1/en not_active Expired - Lifetime
- 2004-05-06 JP JP2006532567A patent/JP4808624B2/ja not_active Expired - Fee Related
- 2004-05-06 BR BRPI0410680-6B1A patent/BRPI0410680B1/pt not_active IP Right Cessation
- 2004-05-06 KR KR1020057021149A patent/KR101094018B1/ko not_active Expired - Fee Related
- 2004-05-06 BR BR122014002952A patent/BR122014002952B1/pt not_active IP Right Cessation
- 2004-05-06 CA CA2524452A patent/CA2524452C/en not_active Expired - Lifetime
- 2004-05-06 AU AU2004238804A patent/AU2004238804B2/en not_active Ceased
- 2004-05-06 NZ NZ543388A patent/NZ543388A/en not_active IP Right Cessation
- 2004-05-06 UA UAA200511455A patent/UA84289C2/ru unknown
- 2004-05-06 ES ES11158112T patent/ES2410057T3/es not_active Expired - Lifetime
-
2005
- 2005-10-31 IL IL171693A patent/IL171693A/en active IP Right Grant
- 2005-11-10 ZA ZA200509090A patent/ZA200509090B/en unknown
- 2005-11-14 NO NO20055383A patent/NO20055383L/no not_active Application Discontinuation
-
2006
- 2006-02-13 US US11/352,593 patent/US7572376B2/en not_active Expired - Lifetime
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Legal Events
| Date | Code | Title | Description |
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| FG | Grant or registration |