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MXPA03007012A - Proceso para la fabricacion de un epoxido. - Google Patents

Proceso para la fabricacion de un epoxido.

Info

Publication number
MXPA03007012A
MXPA03007012A MXPA03007012A MXPA03007012A MXPA03007012A MX PA03007012 A MXPA03007012 A MX PA03007012A MX PA03007012 A MXPA03007012 A MX PA03007012A MX PA03007012 A MXPA03007012 A MX PA03007012A MX PA03007012 A MXPA03007012 A MX PA03007012A
Authority
MX
Mexico
Prior art keywords
agr
double bond
product mixture
organic compound
solvent
Prior art date
Application number
MXPA03007012A
Other languages
English (en)
Inventor
Rieber Norbert
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Ag filed Critical Basf Ag
Publication of MXPA03007012A publication Critical patent/MXPA03007012A/es
Publication of MX243899B publication Critical patent/MX243899B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/19—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with organic hydroperoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/02—Synthesis of the oxirane ring
    • C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
    • C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D301/00—Preparation of oxiranes
    • C07D301/32—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Epoxy Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Un compuesto organico que tiene al menos un enlace doble C-C se epoxida por medio de peroxido de hidrogeno en presencia de al menos un compuesto con actividad catalitica y al menos un disolvente, en donde una mezcla de productos que contiene a-hidroperoxialcoholes se reduce utilizando al menos un agente reductor. El proceso consiste ventajosamente en al menos los siguientes pasos: (i) la reaccion de un compuesto organico que tenga al menos un doble enlace C-C con peroxido de hidrogeno en presencia de al menos un compuesto con actividad catalitica y al menos un disolvente para obtener una mezcla de productos P1 que contenga a-hidroperoxialcoholes; (ii) separar un epoxido formado en la reaccion del paso (i) y el compuesto organico sin reaccionar que tiene al menos un doble enlace C-C a partir de P1 o P1' para obtener una mezcla de productos P2 o P2', en donde P2 contiene los a-hidroperoxialcoholes formados como subproducto en la reaccion del paso (i), y P2' esta practicamente libre de a-hidroperoxialcoholes; iii) tratar P1 y/o P2 con al menos un agente reductor de modo que los a-hidroperoxialcoholes se conviertan en los glicoles correspondientes para obtener una mezcla de productos P1' o P3.
MXPA03007012 2001-02-07 2002-02-06 Proceso para la fabricacion de un epoxido. MX243899B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE10105527A DE10105527A1 (de) 2001-02-07 2001-02-07 Verfahren zur Herstellung eines Epoxids
PCT/EP2002/001218 WO2002062779A1 (de) 2001-02-07 2002-02-06 Verfahren zur herstellung eines epoxids

Publications (2)

Publication Number Publication Date
MXPA03007012A true MXPA03007012A (es) 2004-04-02
MX243899B MX243899B (es) 2007-02-28

Family

ID=7673158

Family Applications (1)

Application Number Title Priority Date Filing Date
MXPA03007012 MX243899B (es) 2001-02-07 2002-02-06 Proceso para la fabricacion de un epoxido.

Country Status (14)

Country Link
US (1) US7026493B2 (es)
EP (1) EP1377562B1 (es)
CN (1) CN1230428C (es)
AT (1) ATE309233T1 (es)
BR (1) BR0207063A (es)
CA (1) CA2437615A1 (es)
DE (2) DE10105527A1 (es)
MX (1) MX243899B (es)
MY (1) MY139320A (es)
RU (1) RU2314300C2 (es)
SA (1) SA02220666B1 (es)
TH (1) TH55985A (es)
WO (1) WO2002062779A1 (es)
ZA (1) ZA200306056B (es)

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DE10164348A1 (de) 2001-12-28 2003-07-17 Basf Ag Verfahren zur Herstellung von 1-Methoypropanol-2
DE10233385A1 (de) 2002-07-23 2004-02-12 Basf Ag Verfahren zur kontinuierlichen Herstellung von Propylenglykolen
DE10233382A1 (de) 2002-07-23 2004-01-29 Basf Ag Verfahren zur kontinuierlich betriebenen Reindestillation des bei der koppel-produktfreien Synthese von Propylenoxid anfallenden 1.2-Propylenglykols
DE10240129B4 (de) 2002-08-30 2004-11-11 Basf Ag Integriertes Verfahren zur Synthese von Propylenoxid
DE10307737A1 (de) * 2003-02-24 2004-09-02 Basf Ag Verfahren zur Herstellung eines Epoxids
US7273826B2 (en) * 2005-07-26 2007-09-25 Lyondell Chemical Technology, L.P. Epoxidation catalyst
ITMI20052491A1 (it) * 2005-12-27 2007-06-28 Basf Ag Un procedimento per la epossidazione del propene
EP1918248A3 (de) * 2006-10-29 2010-06-09 Silicon Fire AG Bereitstellung von H2O2 aus Schwefelsäure, die beim Verbrennen von fossilen Brennstoffen aus darin enthaltenen Schwefelrückständen entsteht, und Verwendung des H2O2 als Energieträger
WO2009092683A2 (de) * 2008-01-25 2009-07-30 Basf Se METHODE ZUR SELEKTIVEN GROßTECHNISCHEN HERSTELLUNG VON 1,5,9 CYCLODODECATRIEN
EP2103604A1 (de) 2008-03-17 2009-09-23 Evonik Degussa GmbH Verfahren zur Herstellung von Epichlorhydrin
EP2149569A1 (en) 2008-08-01 2010-02-03 Hexion Specialty Chemicals Research Belgium S.A. Process for the manufacture of a 1,2-Epoxide
EP2149570A1 (en) * 2008-08-01 2010-02-03 Hexion Specialty Chemicals Research Belgium S.A. Process for the manufacture of epichlorohydrin using hydrogen peroxide and a manganese komplex
BR112012001033B8 (pt) * 2009-07-16 2021-03-23 Basf Se método para separar acetonitrila de água, e, processo altamente integrado para a preparação de óxido de propileno
WO2012094121A1 (en) * 2011-01-05 2012-07-12 Sumitomo Chemical Company, Limited Process for producing olefin oxide
CN103298555B (zh) * 2011-01-05 2015-07-22 住友化学株式会社 生产氧化烯烃的方法
WO2012094119A1 (en) * 2011-01-05 2012-07-12 Sumitomo Chemical Company, Limited Process for producing olefin oxide
WO2012094120A1 (en) * 2011-01-05 2012-07-12 Sumitomo Chemical Company, Limited Process for producing olefin oxide
RU2456301C1 (ru) * 2011-05-24 2012-07-20 Государственное образовательное учреждение высшего профессионального образования "Башкирский государственный университет" (ГОУ ВПО БашГУ) Способ получения эпоксидированных 1,2-полибутадиенов
KR102245980B1 (ko) 2013-04-29 2021-04-29 바스프 에스이 부분-스트림 증류
RU2016101122A (ru) * 2013-06-17 2017-07-24 Басф Се Способ регенерации содержащего благородный металл катализатора на носителе
US20160107119A1 (en) * 2014-10-16 2016-04-21 Battelle Memorial Institute CATALYSTS FOR ENHANCED REDUCTION OF NOx GASES AND PROCESSES FOR MAKING AND USING SAME
MY182496A (en) 2014-10-27 2021-01-25 Dow Global Technologies Llc Part-stream distillation
EP3563927A1 (en) * 2018-04-30 2019-11-06 Hexion Research Belgium SA Purification of high performance epoxy resins via membrane filtration technology
CN110105173A (zh) * 2019-04-26 2019-08-09 江苏扬农化工集团有限公司 一种高效的hppo工艺回收溶剂的纯化方法
CA3201871A1 (en) 2020-12-10 2022-06-16 Andreas Kempter Process for the controlled decomposition of peroxo compounds
CN113058643B (zh) * 2021-03-29 2021-12-21 北京化工大学 一种改性ts-1分子筛复合催化剂及其制备方法和应用

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US3947501A (en) * 1969-11-07 1976-03-30 Halcon International, Inc. Process for treatment of reaction mixtures by hydrogenation
IT1152299B (it) * 1982-07-28 1986-12-31 Anic Spa Procedimento per l'espossidazione di composti olefinici
IT1222868B (it) 1987-10-12 1990-09-12 Montedipe Spa Metodo per la preparazione di titanio silicaliti
US5244650A (en) 1989-06-29 1993-09-14 Engelhard Corporation Large-pored molecular sieves with charged octahedral titanium and charged tetrahedral aluminum sites
GB9022003D0 (en) 1990-10-10 1990-11-21 Interox Chemicals Ltd Purification of hydrogen peroxide
US5107002A (en) 1990-12-06 1992-04-21 Arco Chemical Technology, L.P. Lower alkylene oxide purification
DE4222109A1 (de) 1992-07-06 1994-01-13 Solvay Interox Gmbh Verfahren zur Herstellung von hochreinem Wasserstoffperoxid für die Mikroelektronik
US5288882A (en) 1992-12-21 1994-02-22 Arco Chemical Technology, L.P. Process for recovering an optically active epoxy alcohol
AU714033B2 (en) 1996-07-19 1999-12-16 Nissan Chemical Industries Ltd. Method for producing purified epoxy compound
DE19636064A1 (de) 1996-09-05 1998-03-12 Basf Ag Verfahren zur Hydrierung
FR2763932B1 (fr) 1997-05-27 1999-07-30 Chemoxal Sa Procede de preparation d'une solution ultra-pure de peroxyde par echange ionique dans des lits a rapports h/d definis
DE19723949A1 (de) 1997-06-06 1998-12-10 Basf Ag Verfahren zur Regenerierung eines Zeolith-Katalysators
DE19723751A1 (de) 1997-06-06 1998-12-10 Basf Ag Formkörper und Verfahren zu dessen Herstellung
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DE10015246A1 (de) 2000-03-28 2001-10-04 Basf Ag Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid
DE10032885A1 (de) 2000-07-06 2002-01-17 Basf Ag Verfahren zur Herstellung von Propylenoxid
CA2356512C (en) * 2000-09-07 2009-03-10 Inocon Technologie Ges.M.B.H. A method for closing and/or joining a connecting joint or joining seam between two pieces of galvanized sheet metal
US6455712B1 (en) * 2000-12-13 2002-09-24 Shell Oil Company Preparation of oxirane compounds

Also Published As

Publication number Publication date
ATE309233T1 (de) 2005-11-15
EP1377562A1 (de) 2004-01-07
US7026493B2 (en) 2006-04-11
ZA200306056B (en) 2004-09-28
MX243899B (es) 2007-02-28
TH55985A (en) 2012-03-06
CN1230428C (zh) 2005-12-07
BR0207063A (pt) 2008-07-22
RU2003127385A (ru) 2005-03-27
DE50204869D1 (de) 2005-12-15
WO2002062779A1 (de) 2002-08-15
CA2437615A1 (en) 2002-08-15
MY139320A (en) 2009-09-30
SA02220666B1 (ar) 2007-01-20
DE10105527A1 (de) 2002-08-08
RU2314300C2 (ru) 2008-01-10
CN1494538A (zh) 2004-05-05
EP1377562B1 (de) 2005-11-09
US20040068128A1 (en) 2004-04-08

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