MX9606244A - Esterificacion de acido (met)acrilico con un alcanol. - Google Patents
Esterificacion de acido (met)acrilico con un alcanol.Info
- Publication number
- MX9606244A MX9606244A MX9606244A MX9606244A MX9606244A MX 9606244 A MX9606244 A MX 9606244A MX 9606244 A MX9606244 A MX 9606244A MX 9606244 A MX9606244 A MX 9606244A MX 9606244 A MX9606244 A MX 9606244A
- Authority
- MX
- Mexico
- Prior art keywords
- meth
- acrylic acid
- lower product
- alkanol
- separated
- Prior art date
Links
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 title abstract 6
- 230000032050 esterification Effects 0.000 title abstract 2
- 238000005886 esterification reaction Methods 0.000 title abstract 2
- 239000003377 acid catalyst Substances 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000007858 starting material Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
- C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
- C07C69/54—Acrylic acid esters; Methacrylic acid esters
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/48—Separation; Purification; Stabilisation; Use of additives
- C07C67/60—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C68/00—Preparation of esters of carbonic or haloformic acids
- C07C68/08—Purification; Separation; Stabilisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
En un proceso para esterificar ácido (met)acrílico con un alcanol en presencia de un catalizador de esterificacion en el que los compuestos de partida no reaccionados y el éster (met)acrílico formado se separan mediante destilacion y se obtiene un producto inferior que contiene ésteres oxi, el producto inferior se separa y ya sea el producto inferior se mezcla directamente con ácido (met)acrílico y los ésteres oxi presentes en el producto inferior y luego se disocia a una temperatura elevada en presencia de catalizadores ácidos diferentes al ácido (met)acrílico, o los ésteres oxi primero se separan mediante destilacion del producto inferior, el destilado se mezcla con ácido (met)acrílico y luego se disocia a una temperatura elevada en presencia de catalizadores ácidos diferentes del ácido (met)acrílico.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19547459.7 | 1995-12-19 | ||
| DE19547459A DE19547459A1 (de) | 1995-12-19 | 1995-12-19 | Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| MXPA96006244A MXPA96006244A (es) | 1998-04-01 |
| MX9606244A true MX9606244A (es) | 1998-04-30 |
Family
ID=7780580
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX9606244A MX9606244A (es) | 1995-12-19 | 1996-12-09 | Esterificacion de acido (met)acrilico con un alcanol. |
Country Status (13)
| Country | Link |
|---|---|
| EP (1) | EP0780360B1 (es) |
| JP (1) | JP4092740B2 (es) |
| KR (1) | KR100452078B1 (es) |
| CN (1) | CN1095826C (es) |
| BR (1) | BR9703406A (es) |
| CA (1) | CA2193407A1 (es) |
| CZ (1) | CZ369196A3 (es) |
| DE (2) | DE19547459A1 (es) |
| DK (1) | DK0780360T3 (es) |
| ES (1) | ES2145372T3 (es) |
| MX (1) | MX9606244A (es) |
| MY (1) | MY125609A (es) |
| SG (1) | SG79930A1 (es) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19701737A1 (de) * | 1997-01-20 | 1998-07-23 | Basf Ag | Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol |
| MY120051A (en) * | 1997-07-30 | 2005-08-30 | Mitsubishi Rayon Co | Process for purification of (meth)acrylic acid |
| DE19922722A1 (de) | 1999-05-18 | 2000-11-23 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| DE10127941A1 (de) | 2001-06-08 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| ES2387564T3 (es) | 2001-12-04 | 2012-09-26 | Mitsubishi Chemical Corporation | Procedimiento de producción de compuestos de ácido (met)acrílico |
| WO2005007609A1 (de) | 2003-07-11 | 2005-01-27 | Basf Aktiengesellschaft | Thermisches trennverfahren zur abtrennung wenigstens eines (meth)acrylmonomere angereichert enthaltenden stoffstroms |
| DE102008054587A1 (de) | 2008-12-12 | 2010-06-17 | Basf Se | Verfahren zur Rückspaltung von in einer Flüssigkeit F enthaltenen Michael-Addukten, die bei der Herstellung von Acrylsäure oder deren Ester gebildet wurde |
| FR3008971B1 (fr) * | 2013-07-29 | 2016-08-19 | Arkema France | Procede de production en continu d'acrylates legers par esterification d'un acide acrylique de grade ester brut |
| EP4146618A1 (de) | 2020-05-04 | 2023-03-15 | Basf Se | Verfahren zur rückspaltung von in einer flüssigkeit f enthaltenen michael-addukten, die bei der herstellung von acrylsäure gebildet wurden |
| EP4015498B1 (de) | 2020-12-18 | 2024-04-24 | Basf Se | Verfahren zur kontinuierlichen herstellung von acrylsäure-n-butylester |
| TW202436407A (zh) | 2023-01-11 | 2024-09-16 | 德商贏創運營有限公司 | 巨單體及固態聚合物電解質 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB923595A (en) | 1960-12-03 | 1963-04-18 | Distillers Co Yeast Ltd | Improvements in and relating to the production of acrylic esters |
| US3868410A (en) | 1972-08-03 | 1975-02-25 | Celanese Corp | Conversion of oligomeric acrylates to acrylate monomers |
| DE2339529A1 (de) | 1973-08-03 | 1975-02-13 | Ardie Werk Gmbh | Kraftstoffeinspritzpumpenverstellvorrichtung |
| JPS5762229A (en) | 1980-10-02 | 1982-04-15 | Mitsubishi Petrochem Co Ltd | Recovery of useful component from heavy substance obtained as by-product in preparation of acrylic ester |
| CN1058390A (zh) | 1990-07-13 | 1992-02-05 | 梁效成 | 含烷氧基丙酸酯废液的处理方法 |
| JPH0768168B2 (ja) | 1991-07-12 | 1995-07-26 | 東亞合成株式会社 | アクリル酸エステルのミカエル付加物の分解方法 |
| CN1026104C (zh) | 1992-03-17 | 1994-10-05 | 侯玉里 | 丙烯酸酯类废油再生工艺 |
| JP2943523B2 (ja) | 1992-08-12 | 1999-08-30 | 東亞合成株式会社 | アクリル酸エステルのミカエル付加物から有用化合物を製造する方法 |
-
1995
- 1995-12-19 DE DE19547459A patent/DE19547459A1/de not_active Withdrawn
-
1996
- 1996-12-09 MX MX9606244A patent/MX9606244A/es unknown
- 1996-12-10 MY MYPI96005184A patent/MY125609A/en unknown
- 1996-12-13 DK DK96120076T patent/DK0780360T3/da active
- 1996-12-13 ES ES96120076T patent/ES2145372T3/es not_active Expired - Lifetime
- 1996-12-13 EP EP96120076A patent/EP0780360B1/de not_active Expired - Lifetime
- 1996-12-13 DE DE59605039T patent/DE59605039D1/de not_active Expired - Lifetime
- 1996-12-16 CZ CZ963691A patent/CZ369196A3/cs unknown
- 1996-12-17 JP JP33697796A patent/JP4092740B2/ja not_active Expired - Lifetime
- 1996-12-18 SG SG9611800A patent/SG79930A1/en unknown
- 1996-12-18 CN CN96121568A patent/CN1095826C/zh not_active Expired - Lifetime
- 1996-12-18 KR KR1019960067282A patent/KR100452078B1/ko not_active Expired - Lifetime
- 1996-12-18 CA CA002193407A patent/CA2193407A1/en not_active Abandoned
-
1997
- 1997-05-27 BR BR9703406A patent/BR9703406A/pt not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| JPH09183753A (ja) | 1997-07-15 |
| CN1095826C (zh) | 2002-12-11 |
| DE59605039D1 (de) | 2000-05-31 |
| SG79930A1 (en) | 2001-04-17 |
| MY125609A (en) | 2006-08-30 |
| CA2193407A1 (en) | 1997-06-20 |
| EP0780360B1 (de) | 2000-04-26 |
| BR9703406A (pt) | 1999-01-05 |
| EP0780360A1 (de) | 1997-06-25 |
| CN1158840A (zh) | 1997-09-10 |
| CZ369196A3 (en) | 1997-06-11 |
| ES2145372T3 (es) | 2000-07-01 |
| KR100452078B1 (ko) | 2004-11-16 |
| DE19547459A1 (de) | 1996-07-25 |
| DK0780360T3 (da) | 2000-08-07 |
| KR970042476A (ko) | 1997-07-24 |
| JP4092740B2 (ja) | 2008-05-28 |
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