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MX345814B - Reactor y proceso para preparar sulfuro de hidrogeno. - Google Patents

Reactor y proceso para preparar sulfuro de hidrogeno.

Info

Publication number
MX345814B
MX345814B MX2014015666A MX2014015666A MX345814B MX 345814 B MX345814 B MX 345814B MX 2014015666 A MX2014015666 A MX 2014015666A MX 2014015666 A MX2014015666 A MX 2014015666A MX 345814 B MX345814 B MX 345814B
Authority
MX
Mexico
Prior art keywords
reactor
hydrogen sulphide
preparing hydrogen
sub
hydrogen
Prior art date
Application number
MX2014015666A
Other languages
English (en)
Other versions
MX2014015666A (es
Inventor
Finkeldei Caspar-Heinrich
Körfer Martin
Kee Cheung Chiu
Maassen Ralf
Wenner Stefan
Original Assignee
Evonik Degussa Gmbh *
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Degussa Gmbh * filed Critical Evonik Degussa Gmbh *
Publication of MX2014015666A publication Critical patent/MX2014015666A/es
Publication of MX345814B publication Critical patent/MX345814B/es

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J10/00Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
    • B01J10/005Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor carried out at high temperatures in the presence of a molten material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/0285Heating or cooling the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/16Hydrogen sulfides
    • C01B17/161Preparation from elemental sulfur
    • C01B17/162Preparation from elemental sulfur from elemental sulfur and hydrogen
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00327Controlling the temperature by direct heat exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023Details
    • B01J2208/027Beds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • B01J2219/00166Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00777Baffles attached to the reactor wall horizontal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La presente invención se refiere a un reactor y a un proceso para la síntesis de sulfuro de hidrógeno a partir de azufre elemental e hidrógeno a presión elevada y temperatura elevada. La invención se refiere además al uso del reactor para la preparación de sulfuro de hidrógeno con alto rendimiento y con un bajo contenido de H2Sx.
MX2014015666A 2012-06-22 2013-05-31 Reactor y proceso para preparar sulfuro de hidrogeno. MX345814B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP12173167.3A EP2676925A1 (de) 2012-06-22 2012-06-22 Reaktor und Verfahren zur Herstellung von Schwefelwasserstoff
PCT/EP2013/061244 WO2013189719A1 (en) 2012-06-22 2013-05-31 Reactor and process for preparing hydrogen sulphide

Publications (2)

Publication Number Publication Date
MX2014015666A MX2014015666A (es) 2015-04-10
MX345814B true MX345814B (es) 2017-02-16

Family

ID=48576998

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2014015666A MX345814B (es) 2012-06-22 2013-05-31 Reactor y proceso para preparar sulfuro de hidrogeno.

Country Status (12)

Country Link
US (1) US9440208B2 (es)
EP (2) EP2676925A1 (es)
JP (1) JP6173448B2 (es)
KR (1) KR102022147B1 (es)
CN (1) CN104583116B (es)
BR (1) BR112014031947A2 (es)
ES (1) ES2717881T3 (es)
MX (1) MX345814B (es)
MY (1) MY169726A (es)
RU (1) RU2621106C2 (es)
SG (1) SG11201408546PA (es)
WO (1) WO2013189719A1 (es)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA3007925C (en) 2015-12-10 2023-05-16 Daniel M. Hasenberg Hydrogen sulfide production process and related reactor vessels
EP3464239B1 (en) 2016-05-31 2021-03-31 Novus International Inc. Process for producing methyl mercaptan from dimethyl sulfide

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2863725A (en) 1953-04-24 1958-12-09 Hooker Chemical Corp Process for making sulfur free hydrogen sulfide
US2965455A (en) * 1953-04-24 1960-12-20 Hooker Chemical Corp Apparatus for producing hydrogen sulfide
US2876070A (en) 1955-03-28 1959-03-03 Chemetron Corp Method for producing hydrogen sulfide by synthesis
US2876071A (en) * 1955-05-31 1959-03-03 Chemetron Corp Method for producing hydrogen sulfide by synthesis
US3087788A (en) * 1959-04-06 1963-04-30 Fmc Corp Combined catalytic and non-catalytic process of producing hydrogen sulfide and carbon disulfide
FR1593276A (es) * 1967-12-19 1970-05-25
DE10245164B4 (de) * 2002-09-26 2014-11-13 Evonik Degussa Gmbh Verfahren zur Umwandlung von Polysulfanen
FR2885138B1 (fr) * 2005-04-29 2007-06-15 Inst Rech Pour Le Dev I R D Et Procede de production d'acide sulfhydrique et son application, notamment a la depollution d'effluents contenant des metaux lourds
DE102006019590A1 (de) * 2006-04-27 2007-10-31 Degussa Gmbh Reaktionsbehälter für die Herstellung von Schwefelwasserstoff
JP5306231B2 (ja) * 2007-01-16 2013-10-02 ビーエーエスエフ ソシエタス・ヨーロピア 硫化水素を製造するための反応器および方法
PL2125613T3 (pl) * 2007-01-16 2017-06-30 Basf Se Sposób i urządzenie do ciągłego wytwarzania siarkowodoru
DE102008040544A1 (de) * 2008-07-18 2010-01-21 Evonik Degussa Gmbh Reaktionsbehälter und Verfahren zur Verwendung

Also Published As

Publication number Publication date
US20150209747A1 (en) 2015-07-30
CN104583116B (zh) 2017-12-12
KR20150036120A (ko) 2015-04-07
RU2621106C2 (ru) 2017-05-31
MY169726A (en) 2019-05-14
EP2676925A1 (de) 2013-12-25
BR112014031947A2 (pt) 2017-06-27
EP2864247A1 (en) 2015-04-29
EP2864247B1 (en) 2018-12-26
SG11201408546PA (en) 2015-01-29
ES2717881T3 (es) 2019-06-26
MX2014015666A (es) 2015-04-10
JP2015523957A (ja) 2015-08-20
JP6173448B2 (ja) 2017-08-02
RU2015101748A (ru) 2016-08-10
US9440208B2 (en) 2016-09-13
KR102022147B1 (ko) 2019-09-17
WO2013189719A1 (en) 2013-12-27
CN104583116A (zh) 2015-04-29

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