[go: up one dir, main page]

MX2019009401A - Metodo para la purificacion de vainillina natural. - Google Patents

Metodo para la purificacion de vainillina natural.

Info

Publication number
MX2019009401A
MX2019009401A MX2019009401A MX2019009401A MX2019009401A MX 2019009401 A MX2019009401 A MX 2019009401A MX 2019009401 A MX2019009401 A MX 2019009401A MX 2019009401 A MX2019009401 A MX 2019009401A MX 2019009401 A MX2019009401 A MX 2019009401A
Authority
MX
Mexico
Prior art keywords
natural vanillin
purification
vanillin
natural
relates
Prior art date
Application number
MX2019009401A
Other languages
English (en)
Inventor
Vibert Martine
Etchebarne Alain
Original Assignee
Rhodia Operations
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodia Operations filed Critical Rhodia Operations
Publication of MX2019009401A publication Critical patent/MX2019009401A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/78—Separation; Purification; Stabilisation; Use of additives
    • C07C45/783—Separation; Purification; Stabilisation; Use of additives by gas-liquid treatment, e.g. by gas-liquid absorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/20—Unsaturated compounds containing keto groups bound to acyclic carbon atoms
    • C07C49/258—Unsaturated compounds containing keto groups bound to acyclic carbon atoms containing —CHO groups
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
    • A23L27/115—Natural spices, flavouring agents or condiments; Extracts thereof obtained by distilling, stripping, or recovering of volatiles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/001—Processes specially adapted for distillation or rectification of fermented solutions
    • B01D3/002—Processes specially adapted for distillation or rectification of fermented solutions by continuous methods
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/148—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step in combination with at least one evaporator
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/343—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances the substance being a gas
    • B01D3/346—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances the substance being a gas the gas being used for removing vapours, e.g. transport gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0059—General arrangements of crystallisation plant, e.g. flow sheets
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/20—Synthetic spices, flavouring agents or condiments
    • A23L27/24—Synthetic spices, flavouring agents or condiments prepared by fermentation
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D2009/0086—Processes or apparatus therefor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Biotechnology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Fats And Perfumes (AREA)
  • Seasonings (AREA)
  • Extraction Or Liquid Replacement (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

La presente invención se refiere a un método para la purificación de vainillina natural, que comprende un paso de implica la separación por arrastre de una corriente liquida F2 que contiene vainillina natural. La invención también se refiere a la vainillina natural que se puede obtener utilizando el método de la invención, así como un dispositivo para purificar vainillina natural.
MX2019009401A 2017-02-08 2018-02-08 Metodo para la purificacion de vainillina natural. MX2019009401A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1751021A FR3062652B1 (fr) 2017-02-08 2017-02-08 Procede de purification de la vanilline naturelle
PCT/EP2018/053207 WO2018146210A1 (fr) 2017-02-08 2018-02-08 Procede de purification de la vanilline naturelle

Publications (1)

Publication Number Publication Date
MX2019009401A true MX2019009401A (es) 2019-09-26

Family

ID=58645223

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019009401A MX2019009401A (es) 2017-02-08 2018-02-08 Metodo para la purificacion de vainillina natural.

Country Status (12)

Country Link
US (1) US10941100B2 (es)
EP (1) EP3580195B1 (es)
JP (1) JP7191835B2 (es)
CN (1) CN110312700B (es)
BR (1) BR112019014758B1 (es)
DE (2) DE202018006559U1 (es)
ES (1) ES2796558T3 (es)
FR (1) FR3062652B1 (es)
MX (1) MX2019009401A (es)
PT (1) PT3580195T (es)
SK (1) SK9324Y1 (es)
WO (1) WO2018146210A1 (es)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3099478B1 (fr) 2019-07-30 2021-07-09 Rhodia Operations Procédé de traitement d’une composition comprenant de la vanilline naturelle
FR3099477B1 (fr) 2019-07-30 2023-01-13 Rhodia Operations Compositions de vanilline naturelle
FR3114813B1 (fr) 2020-10-02 2023-11-17 Rhodia Operations Purification d’acide ferulique
EP4222137A1 (fr) 2020-10-02 2023-08-09 Rhodia Operations Purification d'acide ferulique
FR3120629B1 (fr) * 2021-03-15 2024-01-19 Rhodia Operations Procédé de purification de vanilline ou d’un dérivé de vanilline obtenus par un procédé biotechnologique
FR3125818A1 (fr) 2021-07-27 2023-02-03 Rhodia Operations Procédé d’extraction d’acide férulique et/ou ses sels comprenant une étape a) dans laquelle une biomasse est extrudée en présence d’une base
NO347003B1 (en) 2021-09-24 2023-04-03 Autostore Tech As Storage grid for vertical farming
FR3134583B1 (fr) 2022-04-15 2025-02-07 Rhodia Operations Procédé continu de croissance d’un microorganisme
FR3134582B1 (fr) 2022-04-15 2025-08-29 Rhodia Operations Procédé de préparation d’un composé de formule (I) par fermentation

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2745796A (en) * 1953-10-21 1956-05-15 Aschaffenburger Zellstoffwerke Method of recovering vanillin
DE1132113B (de) * 1959-07-09 1962-06-28 Aschaffenburger Zellstoffwerke Verfahren zur Reinigung von Vanillin
AT236357B (de) * 1962-08-16 1964-10-26 Chemie Linz Ag Verfahren zur Reinigung von Acrylnitril
DE3920039A1 (de) * 1989-06-20 1991-01-03 Haarmann & Reimer Gmbh Verfahren zur herstellung von natuerlichem vanillin
US5582692A (en) * 1994-10-07 1996-12-10 Artisan Industries, Inc. Method for the purification of vitamin E
CA2238215A1 (en) 1997-06-19 1998-12-19 Markus Wetli Process for the production of vanillin
FR2984314B1 (fr) 2011-12-15 2014-01-17 Rhodia Operations Procede de purification de la vanilline par extraction liquide-liquide
ES2796555T3 (es) * 2013-01-24 2022-08-11 Rhodia Operations Procedimiento de purificación de la vainillina natural

Also Published As

Publication number Publication date
SK500042021U1 (sk) 2021-05-26
EP3580195B1 (fr) 2022-02-23
US20190389792A1 (en) 2019-12-26
WO2018146210A1 (fr) 2018-08-16
SK9324Y1 (sk) 2021-09-29
FR3062652B1 (fr) 2020-10-16
PT3580195T (pt) 2022-04-04
CN110312700B (zh) 2022-11-11
JP2020506194A (ja) 2020-02-27
EP3580195A1 (fr) 2019-12-18
ES2796558T3 (es) 2022-05-10
BR112019014758A2 (pt) 2020-03-03
ES2796558T1 (es) 2020-11-27
FR3062652A1 (fr) 2018-08-10
US10941100B2 (en) 2021-03-09
CN110312700A (zh) 2019-10-08
BR112019014758B1 (pt) 2022-11-16
DE18702741T1 (de) 2021-01-07
JP7191835B2 (ja) 2022-12-19
DE202018006559U1 (de) 2021-03-08

Similar Documents

Publication Publication Date Title
MX2019009401A (es) Metodo para la purificacion de vainillina natural.
PH12018501378A1 (en) Compositions and methods for the treatment of hemoglobinopathies
MX2025006476A (es) Composiciones y metodos para oncologia inmunologica
MX2016014515A (es) Composicion topica de crema gel.
NZ749360A (en) Hydrophobic interaction chromatography for purification of oligonucleotides
MX2016004837A (es) Formulaciones de solventes hibridos para la remocion total de azufre organico y la remocion de gas acido total.
MX378847B (es) Nuevos derivados de gamma-amanitina
MY182267A (en) Polishing composition and polishing method
PH12018501013A1 (en) Purified silicon, devices and systems for producing same
MY176465A (en) Synthetic route to 2?-deoxy-2?,2?-difluorotetrahydrouridines
EA201890938A1 (ru) Способ удаления соединений серы из технологических потоков
MX2019002778A (es) Procedimiento de hidrogenacion.
MX2023009431A (es) Metodo para crear un compuesto a base de mercurio, compuesto a base de mercurio, metodos de uso del compuesto a base de mercurio y usos del compuesto a base de mercurio.
MX2019004024A (es) Metodo para preparar acetofenonas sustituidas con ciclopropilo.
PL3775108T3 (pl) Sposób wytwarzania biometanu z odpadów
MX2018008193A (es) Procedimientos para la recuperacion del acido acetico precedente de corrientes acuosas.
MY178981A (en) Method for purifying refined lipid phases
MX2016009073A (es) Acido (s)-3'-metil-abscisico y esteres del mismo.
MX2016009325A (es) Metodo para la preparacion de 1-alquil-3-difluorometil-5-fluor-1h- pirazol-4-carbaldehidos y 1-alquil-3-difluorometil-5-fluor-1h-pira zol-4-carboxilatos.
PH12017501869A1 (en) (s)-2'-vinyl-abscisic acid derivatives
EA201692246A1 (ru) Способ получения 2,6-диметилбензохинона
SG10201803880TA (en) Stable compositions of neuroactive peptides
MX2015010325A (es) Metodo para purificar un compuesto de pnpnh en bruto.
MX2020010343A (es) Proceso para la purificacion de biocomposiciones complejas.
PL3571166T3 (pl) Sposób oczyszczania wody