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MX2019006345A - Proceso para preparar microcapsulas de tamaño controlado que comprenden una etapa de fotopolimerizacion. - Google Patents

Proceso para preparar microcapsulas de tamaño controlado que comprenden una etapa de fotopolimerizacion.

Info

Publication number
MX2019006345A
MX2019006345A MX2019006345A MX2019006345A MX2019006345A MX 2019006345 A MX2019006345 A MX 2019006345A MX 2019006345 A MX2019006345 A MX 2019006345A MX 2019006345 A MX2019006345 A MX 2019006345A MX 2019006345 A MX2019006345 A MX 2019006345A
Authority
MX
Mexico
Prior art keywords
composition
emulsion
controlled size
preparing microcapsules
photopolymerization step
Prior art date
Application number
MX2019006345A
Other languages
English (en)
Inventor
WALTERS Jamie
Demoulin Damien
Original Assignee
Calyxia
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Calyxia filed Critical Calyxia
Publication of MX2019006345A publication Critical patent/MX2019006345A/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/14—Polymerisation; cross-linking
    • B01J13/18—In situ polymerisation with all reactants being present in the same phase
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/14—Polymerisation; cross-linking
    • B01J13/16—Interfacial polymerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F290/00—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups
    • C08F290/02—Macromolecular compounds obtained by polymerising monomers on to polymers modified by introduction of aliphatic unsaturated end or side groups on to polymers modified by introduction of unsaturated end groups
    • C08F290/06—Polymers provided for in subclass C08G
    • C08F290/067—Polyurethanes; Polyureas
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/26—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests in coated particulate form
    • A01N25/28—Microcapsules or nanocapsules
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/11—Encapsulated compositions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/87—Polyurethanes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/48—Preparations in capsules, e.g. of gelatin, of chocolate
    • A61K9/50—Microcapsules having a gas, liquid or semi-solid filling; Solid microparticles or pellets surrounded by a distinct coating layer, e.g. coated microspheres, coated drug crystals
    • A61K9/5005—Wall or coating material
    • A61K9/5021—Organic macromolecular compounds
    • A61K9/5026—Organic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polyvinyl pyrrolidone, poly(meth)acrylates
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/48—Preparations in capsules, e.g. of gelatin, of chocolate
    • A61K9/50—Microcapsules having a gas, liquid or semi-solid filling; Solid microparticles or pellets surrounded by a distinct coating layer, e.g. coated microspheres, coated drug crystals
    • A61K9/5089—Processes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/02—Making microcapsules or microballoons
    • B01J13/06—Making microcapsules or microballoons by phase separation
    • B01J13/14—Polymerisation; cross-linking
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/12—Polymerisation in non-solvents
    • C08F2/16—Aqueous medium
    • C08F2/22—Emulsion polymerisation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/46—Polymerisation initiated by wave energy or particle radiation
    • C08F2/48—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/46—Polymerisation initiated by wave energy or particle radiation
    • C08F2/48—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light
    • C08F2/50—Polymerisation initiated by wave energy or particle radiation by ultraviolet or visible light with sensitising agents
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/34—Silicon-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L57/00—Compositions of unspecified polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L87/00—Compositions of unspecified macromolecular compounds, obtained otherwise than by polymerisation reactions only involving unsaturated carbon-to-carbon bonds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10—General cosmetic use
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/41—Particular ingredients further characterized by their size
    • A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2500/00—Characteristics or properties of obtained polyolefins; Use thereof
    • C08F2500/17—Viscosity
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2312/00—Crosslinking
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28—HEAT EXCHANGE IN GENERAL
    • F28D—HEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D20/00—Heat storage plants or apparatus in general; Regenerative heat-exchange apparatus not covered by groups F28D17/00 or F28D19/00
    • F28D20/02—Heat storage plants or apparatus in general; Regenerative heat-exchange apparatus not covered by groups F28D17/00 or F28D19/00 using latent heat
    • F28D20/023—Heat storage plants or apparatus in general; Regenerative heat-exchange apparatus not covered by groups F28D17/00 or F28D19/00 using latent heat the latent heat storage material being enclosed in granular particles or dispersed in a porous, fibrous or cellular structure

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Engineering & Computer Science (AREA)
  • Dispersion Chemistry (AREA)
  • Birds (AREA)
  • Wood Science & Technology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Plant Pathology (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Toxicology (AREA)
  • Dentistry (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Dermatology (AREA)
  • Manufacturing Of Micro-Capsules (AREA)
  • Cosmetics (AREA)

Abstract

La presente invención se relaciona con un proceso para preparar microcápsulas sólidas que comprende las siguientes etapas: a) adicionar, con agitación, una composición C1, que comprende por lo menos un ingrediente activo, en una composición polimérica fotorreticulable C2, en la que se obtiene una emulsión (E1); b) adicionar con agitación la emulsión (E1) en una composición C3, siendo la viscosidad de la composición C3 mayor que 2,000 mPa.s a 25°C, en donde se obtiene una doble emulsión (E2); c) aplicar corte a la emulsión (E2), siendo la velocidad de corte aplicada menor de 1,000 s-1, en donde se obtiene una doble emulsión (E3); y d) la fotopolimerización de la composición C2.
MX2019006345A 2016-12-01 2017-12-01 Proceso para preparar microcapsulas de tamaño controlado que comprenden una etapa de fotopolimerizacion. MX2019006345A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1661787A FR3059666B1 (fr) 2016-12-01 2016-12-01 Procede de preparation de microcapsules de taille controlee comprenant une etape de photopolymerisation.
PCT/EP2017/081227 WO2018100179A1 (fr) 2016-12-01 2017-12-01 Procédé de préparation de microcapsules de taille contrôlée comprenant une étape de photopolymérisation

Publications (1)

Publication Number Publication Date
MX2019006345A true MX2019006345A (es) 2019-11-07

Family

ID=57796705

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019006345A MX2019006345A (es) 2016-12-01 2017-12-01 Proceso para preparar microcapsulas de tamaño controlado que comprenden una etapa de fotopolimerizacion.

Country Status (11)

Country Link
US (2) US20190388861A1 (es)
EP (1) EP3548529B1 (es)
JP (1) JP7010965B2 (es)
KR (1) KR102458011B1 (es)
CN (1) CN110062779B (es)
AU (1) AU2017367182B2 (es)
BR (1) BR112019011248B1 (es)
ES (1) ES2834874T3 (es)
FR (1) FR3059666B1 (es)
MX (1) MX2019006345A (es)
WO (1) WO2018100179A1 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112969552B (zh) 2018-10-31 2024-03-22 索尔维特殊聚合物意大利有限公司 自润滑涂料组合物
EP3873985A1 (en) 2018-10-31 2021-09-08 Solvay Specialty Polymers Italy S.p.A. Curable composition of elastomers
US10793686B2 (en) * 2018-12-07 2020-10-06 National Chung-Shan Institute Of Science And Technology Preparation method of vinyl ester resin for optimizing heat-release during curing
JP7603602B2 (ja) * 2019-08-05 2024-12-20 フイルメニツヒ ソシエテ アノニム 開裂性多価アルコール系マイクロカプセル
US11713367B2 (en) * 2019-12-23 2023-08-01 Carbon, Inc. Inhibition of crystallization in polyurethane resins
KR102440764B1 (ko) * 2020-03-30 2022-09-06 경희대학교 산학협력단 습도 및 pH 민감형 항균 나노 캡슐 및 그 제조방법
KR102492946B1 (ko) * 2020-11-17 2023-01-30 경희대학교 산학협력단 습도 및 pH 민감형 다공성 나노 캡슐 및 그 제조방법
EP4008312A1 (en) * 2020-12-01 2022-06-08 Calyxia Emulsion comprising size-controlled droplets
EP4608548A1 (en) * 2022-10-27 2025-09-03 Calyxia SAS Process for the manufacture of microcapsules and microcapsules
WO2024133458A1 (en) 2022-12-20 2024-06-27 Calyxia Sas A plurality of microcapsules and use thereof in polymers
EP4552734A1 (en) 2023-11-07 2025-05-14 Calyxia Microcapsules containing volatile ingredients
WO2025132932A1 (en) 2023-12-20 2025-06-26 Calyxia Sas A plurality of microcapsules and use thereof in polymers
WO2025132982A2 (en) 2023-12-22 2025-06-26 Calyxia Sas A plurality of microcapsules and use thereof in polymers
WO2026003221A1 (en) 2024-06-27 2026-01-02 Calyxia Plurality of microcapsules and polymer dispersions comprising the same

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AR006355A1 (es) 1996-03-22 1999-08-25 Procter & Gamble Activo suavizante biodegradable y composicion que lo contiene
CA2269293C (en) 1996-10-21 2003-07-15 The Procter & Gamble Company Concentrated fabric softening composition
DE10000223A1 (de) 2000-01-05 2001-07-12 Basf Ag Mikrokapselzubereitungen und Mikrokapseln enthaltende Wasch- und Reinigungsmittel
EP1404516A2 (en) * 2000-12-13 2004-04-07 Purdue Research Foundation Microencapsulation of drugs by solvent exchange
JP2007528286A (ja) * 2003-07-03 2007-10-11 エルジー・ケム・リミテッド ミニエマルジョン重合を通じたマイクロカプセルの製造方法
EP1502646B1 (en) 2003-08-01 2016-07-13 The Procter & Gamble Company Microcapsules
FR2867075B1 (fr) 2004-03-03 2006-07-14 Ethypharm Sa Procede de preparation de microspheres biodegradables calibrees
CN101362069B (zh) * 2008-10-08 2011-06-01 中国科学院过程工程研究所 一种中空多孔微胶囊及其制备方法
EP2442901A2 (de) 2009-06-15 2012-04-25 Basf Se Mikrokapseln mit hochverzweigten polymeren als vernetzer
CN102702449B (zh) * 2012-06-13 2013-09-18 福建省锦浪精细化工有限公司 一种耐热性发泡微胶囊的制备方法
EP3144058A1 (en) 2015-09-16 2017-03-22 Calyxia Method for preparing microcapsules by double emulsion

Also Published As

Publication number Publication date
JP2020500707A (ja) 2020-01-16
KR20190126048A (ko) 2019-11-08
CN110062779B (zh) 2021-12-31
FR3059666B1 (fr) 2019-05-17
US20200094214A1 (en) 2020-03-26
US20190388861A1 (en) 2019-12-26
JP7010965B2 (ja) 2022-02-10
BR112019011248A2 (pt) 2019-10-15
WO2018100179A1 (fr) 2018-06-07
AU2017367182B2 (en) 2022-03-17
FR3059666A1 (fr) 2018-06-08
CA3045215A1 (fr) 2018-06-07
AU2017367182A1 (en) 2019-06-20
ES2834874T3 (es) 2021-06-21
EP3548529A1 (fr) 2019-10-09
US10850247B2 (en) 2020-12-01
EP3548529B1 (fr) 2020-10-14
CN110062779A (zh) 2019-07-26
BR112019011248B1 (pt) 2023-01-24
KR102458011B1 (ko) 2022-10-21

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