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MX2019002204A - Proceso para preparar bifenilos sustituidos. - Google Patents

Proceso para preparar bifenilos sustituidos.

Info

Publication number
MX2019002204A
MX2019002204A MX2019002204A MX2019002204A MX2019002204A MX 2019002204 A MX2019002204 A MX 2019002204A MX 2019002204 A MX2019002204 A MX 2019002204A MX 2019002204 A MX2019002204 A MX 2019002204A MX 2019002204 A MX2019002204 A MX 2019002204A
Authority
MX
Mexico
Prior art keywords
preparing substituted
substituted biphenyls
solvent
biphenyls
disclosed
Prior art date
Application number
MX2019002204A
Other languages
English (en)
Inventor
Xu Xiaoming
Frassetto Timo
Huang Chao
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2019002204A publication Critical patent/MX2019002204A/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B37/00—Reactions without formation or introduction of functional groups containing hetero atoms, involving either the formation of a carbon-to-carbon bond between two carbon atoms not directly linked already or the disconnection of two directly linked carbon atoms
    • C07B37/04—Substitution
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/12—Preparation of nitro compounds by reactions not involving the formation of nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/07—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms
    • C07C205/11—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms having nitro groups bound to carbon atoms of six-membered aromatic rings
    • C07C205/12—Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by halogen atoms having nitro groups bound to carbon atoms of six-membered aromatic rings the six-membered aromatic ring or a condensed ring system containing that ring being substituted by halogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6568—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus atoms as the only ring hetero atoms
    • C07F9/65683—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus atoms as the only ring hetero atoms the ring phosphorus atom being part of a phosphine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/40—Substitution reactions at carbon centres, e.g. C-C or C-X, i.e. carbon-hetero atom, cross-coupling, C-H activation or ring-opening reactions
    • B01J2231/42—Catalytic cross-coupling, i.e. connection of previously not connected C-atoms or C- and X-atoms without rearrangement
    • B01J2231/4205—C-C cross-coupling, e.g. metal catalyzed or Friedel-Crafts type
    • B01J2231/4211—Suzuki-type, i.e. RY + R'B(OR)2, in which R, R' are optionally substituted alkyl, alkenyl, aryl, acyl and Y is the leaving group
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/824—Palladium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
    • B01J31/2404—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring
    • B01J31/2419—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising P as ring member
    • B01J31/2438—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising P as ring member and further hetero atoms as ring members, excluding the positions adjacent to P

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Se divulga un proceso para preparar bifenilos sustituidos por medio de acoplamiento de Suzuki usando ligandos de fosforo específicos y una mezcla solvente que contiene agua, un solvente orgánico no polar y un cosolvente aprotico polar.
MX2019002204A 2016-08-22 2016-08-22 Proceso para preparar bifenilos sustituidos. MX2019002204A (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2016/096260 WO2018035685A1 (en) 2016-08-22 2016-08-22 Process for preparing substituted biphenyls

Publications (1)

Publication Number Publication Date
MX2019002204A true MX2019002204A (es) 2019-09-19

Family

ID=61246624

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019002204A MX2019002204A (es) 2016-08-22 2016-08-22 Proceso para preparar bifenilos sustituidos.

Country Status (8)

Country Link
US (1) US10683256B2 (es)
EP (1) EP3500551B1 (es)
KR (1) KR102550878B1 (es)
CN (1) CN109563023B (es)
ES (1) ES2906251T3 (es)
IL (1) IL264681B (es)
MX (1) MX2019002204A (es)
WO (1) WO2018035685A1 (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3541788B1 (en) 2016-11-17 2020-09-02 Basf Se Process for the purification of 1-(4-chlorophenyl)pyrazol-3-ol
CN109942433B (zh) * 2019-04-11 2022-03-25 浙江工业大学 一种3’,4’,5’-三氟-2-氨基联苯的化学合成方法
WO2021014437A1 (en) 2019-07-19 2021-01-28 Adama Makhteshim Ltd. Process for the preparation of biphenylamines
KR102231991B1 (ko) * 2019-10-30 2021-03-25 주식회사 서연이화 테일게이트 인너 판넬용 폴리프로필렌 수지 조성물 및 이의 성형품
EP4378929A1 (en) 2022-11-29 2024-06-05 Adama Makhteshim Ltd. Synthesis of aromatic boronic acids
CN117430516A (zh) * 2023-10-16 2024-01-23 江苏中旗科技股份有限公司 一种一锅法合成氟唑菌酰胺联苯胺中间体的工业化方法
CN119591501A (zh) * 2024-12-25 2025-03-11 江苏广域化学有限公司 一锅法制备含氟联苯化合物的合成方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE502005005420D1 (de) * 2004-09-16 2008-10-30 Basf Se Benzoylsubstituierte serin-amide
PE20060721A1 (es) * 2004-09-16 2006-08-24 Basf Ag Serinamidas sustituidas por heteroaroilo
EP2119697A1 (en) * 2008-05-09 2009-11-18 Bayer CropScience AG Process for preparing substituted biphenylanilides
EP2303828B1 (de) 2008-06-25 2014-07-30 Basf Se Verfahren zur herstellung von substituierten biphenylen
WO2010102980A1 (en) * 2009-03-09 2010-09-16 Basf Se Process for preparing substituted 2-nitrobiphenyls
US9096626B2 (en) * 2010-04-05 2015-08-04 Boehringer Ingelheim International Gmbh Monophosphorus ligands and their use in cross-coupling reactions
AU2012342564A1 (en) * 2011-11-21 2014-06-12 Basf Se Process for preparing N-substituted 1H-pyrazole-5-carboxylate compounds and derivatives thereof
EP2978315A1 (en) * 2013-03-28 2016-02-03 Basf Se Process for preparing sulfimines and their in-situ conversion into n-(2-amino-benzoyl)-sulfimines
CN105392791B (zh) 2013-07-23 2019-02-22 拜耳作物科学股份公司 制备氯代酰联苯胺和联苯胺的改进方法
WO2016094489A1 (en) * 2014-12-10 2016-06-16 The Regents Of The University Of California Phosphorus ligands and methods of use
CN104529786B (zh) * 2014-12-16 2019-10-11 上海生农生化制品股份有限公司 3,4,5-三氟-2’-硝基联苯的合成方法
WO2017025377A1 (en) 2015-08-10 2017-02-16 Basf Se A novel process for preparing crystalline methyl N-[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]-N-methoxycarbamate
CN105399635B (zh) * 2015-12-15 2017-07-28 上海师范大学 微波合成2‑硝基‑3’,4’,5’‑三氟‑1,1’‑联苯的方法

Also Published As

Publication number Publication date
EP3500551A4 (en) 2020-03-25
CN109563023B (zh) 2022-10-28
US20190210954A1 (en) 2019-07-11
IL264681B (en) 2021-10-31
KR102550878B1 (ko) 2023-07-04
KR20190039280A (ko) 2019-04-10
EP3500551B1 (en) 2021-11-10
EP3500551A1 (en) 2019-06-26
CN109563023A (zh) 2019-04-02
ES2906251T3 (es) 2022-04-13
WO2018035685A1 (en) 2018-03-01
US10683256B2 (en) 2020-06-16

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