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MX2018005803A - Forma novedosa de espirodiclofeno, procedimiento de preparacion y uso de la misma. - Google Patents

Forma novedosa de espirodiclofeno, procedimiento de preparacion y uso de la misma.

Info

Publication number
MX2018005803A
MX2018005803A MX2018005803A MX2018005803A MX2018005803A MX 2018005803 A MX2018005803 A MX 2018005803A MX 2018005803 A MX2018005803 A MX 2018005803A MX 2018005803 A MX2018005803 A MX 2018005803A MX 2018005803 A MX2018005803 A MX 2018005803A
Authority
MX
Mexico
Prior art keywords
spirodiclofen
preparation
crystal
novel form
crystalline form
Prior art date
Application number
MX2018005803A
Other languages
English (en)
Inventor
Timothy Bristow James
Original Assignee
Rotam Agrochem Int Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rotam Agrochem Int Co Ltd filed Critical Rotam Agrochem Int Co Ltd
Publication of MX2018005803A publication Critical patent/MX2018005803A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/94—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom spiro-condensed with carbocyclic rings or ring systems, e.g. griseofulvins
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
    • A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
    • A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/06—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings
    • A01N43/12—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom five-membered rings condensed with a carbocyclic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Environmental Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Toxicology (AREA)
  • Dispersion Chemistry (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)

Abstract

Una nueva forma cristalina de espirodiclofeno de fórmula (I), el procedimiento de preparación del cristal, los análisis del cristal mediante diversos procedimientos analíticos y el uso del cristal para preparar una formulación agroquímica estable. También se describe el uso de diversos disolventes para las condiciones de preparación de la forma cristalina.
MX2018005803A 2015-12-14 2016-08-31 Forma novedosa de espirodiclofeno, procedimiento de preparacion y uso de la misma. MX2018005803A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14/967,950 US10005754B2 (en) 2015-12-14 2015-12-14 Form of spirodiclofen, a process for its preparation and use the same
PCT/CN2016/097608 WO2017101515A1 (en) 2015-12-14 2016-08-31 Novel form of spirodiclofen, process for preparation and use thereof

Publications (1)

Publication Number Publication Date
MX2018005803A true MX2018005803A (es) 2018-09-17

Family

ID=59018915

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2018005803A MX2018005803A (es) 2015-12-14 2016-08-31 Forma novedosa de espirodiclofeno, procedimiento de preparacion y uso de la misma.

Country Status (6)

Country Link
US (1) US10005754B2 (es)
CN (1) CN107922368A (es)
BR (1) BR112017023291A2 (es)
MX (1) MX2018005803A (es)
TW (1) TWI742024B (es)
WO (1) WO2017101515A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102695684B1 (ko) 2018-04-13 2024-08-19 바이엘 악티엔게젤샤프트 점적 및 관주 적용에 사용하기 위한 케토엔올 부류의 살곤충제를 갖는 고도로 로딩된 제제
CN108658913A (zh) * 2018-06-13 2018-10-16 石家庄市绿丰化工有限公司 一种合成农药螺螨酯关键中间体的方法
CN109053410A (zh) * 2018-08-06 2018-12-21 兰博尔开封科技有限公司 一种合成1-羟基环己基甲酸的新工艺及应用
CN108840846A (zh) * 2018-08-20 2018-11-20 山东康乔生物科技有限公司 一种螺螨酯及其中间体的制备方法
CN109369587A (zh) * 2018-12-13 2019-02-22 新沂市永诚化工有限公司 一种高纯度高收率螺螨酯的生产工艺
CN119462478A (zh) * 2023-08-09 2025-02-18 天津大学 螺虫乙酯晶型ⅱ及其制备方法和农药组合物及其应用

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4216814A1 (de) 1991-07-16 1993-01-21 Bayer Ag 3-aryl-4-hydroxy-(delta)(pfeil hoch)3(pfeil hoch)-dihydrofuranon- und 3-aryl-4-hydroxy-(delta)(pfeil hoch)3(pfeil hoch)-dihydrothiophenon-derivate
DE10012825B4 (de) * 2000-03-16 2004-04-15 Bayer Corp. Verfahren zur Herstellung von spirocyclischen Tetronsäurederivaten
CN101235023B (zh) * 2008-03-04 2010-06-02 浙江大学 一种螺螨酯的合成方法
CN102372687A (zh) * 2010-08-12 2012-03-14 南通德益化工有限公司 一种螺螨酯的生产方法
CN104292197B (zh) * 2014-09-19 2016-07-06 江苏安邦电化有限公司 一种螺螨酯的合成方法

Also Published As

Publication number Publication date
CN107922368A (zh) 2018-04-17
US10005754B2 (en) 2018-06-26
BR112017023291A2 (pt) 2018-08-14
US20170166546A1 (en) 2017-06-15
TW201726640A (zh) 2017-08-01
WO2017101515A1 (en) 2017-06-22
TWI742024B (zh) 2021-10-11

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